scholarly journals Mechanical Behaviors of Microalloyed TRIP-Assisted Annealed Martensitic Steels under Hydrogen Charging

Materials ◽  
2021 ◽  
Vol 14 (24) ◽  
pp. 7752
Author(s):  
Xiongfei Yang ◽  
Hao Yu ◽  
Chenghao Song ◽  
Lili Li
Keyword(s):  
Tensile Strength ◽  
Volume Fraction ◽  
Hydrogen Desorption ◽  
Total Elongation ◽  
Microalloyed Steels ◽  
Steel Matrix ◽  
Hydrogen Trapping ◽  
Martensitic Steels ◽  
Hydrogen Charging ◽  
Trapping Effect

Transformation Induced Plasticity (TRIP)-assisted annealed martensitic (TAM) steel sheets with various microalloying additions such as niobium, vanadium, or titanium were prepared on laboratory scale and subjected to a double-quenching and austempering heat treatment cycle. Slow strain rate tensile (SSRT) was tested on the investigated TAM steels with and without hydrogen charging to reveal their tensile behaviors and hydrogen induced embrittlement effects. Microstructure observations by scanning electron microscope (SEM) are composed of a principal annealed martensitic matrix and 11.0–13.0% volume fraction of retained austenite, depending on the type of microalloying addition in the different steels. SSRT results show that these TRIP-assisted annealed martensitic steels under air media conditions combine high tensile strength (>1000 MPa) and good ductility (~25%), while under hydrogen charging condition, both tensile strength and ductility decrease where tensile strength ranges between 680 and 760 MPa, down from 1000–1100 MPa, and ductility loss ratio is between 78.8% and 91.1%, along with a total elongation of less than 5%. Hydrogen charged into steel matrix leads to the appearance of cleavage fractures, implying the occurrence of hydrogen induced embrittlement effect in TAM steels. Thermal hydrogen desorption results show that there are double-peak hydrogen desorption temperature ranges for these microalloyed steels, where the first peak corresponds to a high-density dislocation trapping effect, and the second peak corresponds to a hydrogen trapping effect exerted by microalloying precipitates. Thermal desorption analysis (TDS) in combination with SSRT results demonstrate that microalloying precipitates act as irreversible traps to fix hydrogen and, thus, retard diffusive hydrogen motion towards defects, such as grain boundaries and dislocations in microstructure matrix, and eventually reduce the hydrogen induced embrittlement tendency.

The Influence of Quenching Temperature on the Mechanical Properties of a Dual-Phase Steel with 0.094% C and 0.53% Mn

2015 ◽  
Vol 808 ◽  
pp. 28-33 ◽  
Author(s):  
Constantin Dulucheanu ◽  
Nicolai Bancescu ◽  
Traian Severin
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Dual Phase Steel ◽  
Volume Fraction ◽  
Total Elongation ◽  
Metallographic Analysis ◽  
Dual Phase ◽  
Quenching Temperature ◽  
Offset Yield Strength ◽  
Martensite Structure

In this article, the authors have analysed the influence of quenching temperature (TQ) on the mechanical properties of a dual-phase steel with 0.094 % C and 0.53% Mn. In order to obtain a ferrite-martensite structure, specimens of this material have been the subjected to intercritical quenching that consisted of heating at 750, 770, 790, 810 and 830 °C, maintaining for 30 minutes and cooling in water. These specimens have then been subjected to metallographic analysis and tensile test in order to determine the volume fraction of martensite (VM) in the structure, ultimate tensile strength (Rm), the 0.2% offset yield strength (Rp0.2), the total elongation (A5) and the Rp0.2/Rm ratio.

Study on Microstructures and Mechanical Properties of Cold-Rolled C-Mn-Si-Al TRIP Steel

2010 ◽  
Vol 146-147 ◽  
pp. 678-681
Author(s):  
Zheng You Tang ◽  
Hua Ding
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Trip Steel ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Total Elongation ◽  
Partial Substitution ◽  
Cold Rolled ◽  
Microstructures And Mechanical Properties

The effect of the partial substitution of Si by Al on the microstructures and the mechanical properties of cold rolled C-Mn-Si TRIP steel was investigated. The results show that the partial substitution of Si by Al could refine the microstructures, increase the volume fraction of ferrite and retained austenite. In addition, the excellent mechanical properties of the Al partial substituted TRIP steel could be obtained, the tensile strength, total elongation and strength-ductility of C-Mn-Si-Al TRIP steel are 739MPa, 38% and 28082MPa%, respectively.

scholarly journals Hydrogen Trapping Behavior in Vanadium Microalloyed TRIP-Assisted Annealed Martensitic Steel

Metals ◽  
2019 ◽  
Vol 9 (7) ◽  
pp. 741
Author(s):  
Yang ◽  
Yu ◽  
Li
Keyword(s):  
Vanadium Carbide ◽  
Hydrogen Diffusion ◽  
Martensitic Steel ◽  
Tensile Tests ◽  
Test Results ◽  
Hydrogen Trapping ◽  
Martensitic Steels ◽  
Transformation Induced Plasticity ◽  
Hydrogen Charging ◽  
Transmission Electron

Transformation induced plasticity (TRIP)-assisted annealed martensitic (TAM) steel combines higher tensile strength and elogangtion, and has been increasingly used but appears to bemore prone to hydrogen embrittlement (HE). In this paper, the hydrogen trapping behavior and HE of TRIP-assisted annealed martensitic steels with different vanadium additions had been investigated by means of hydrogen charging and slow strain rate tensile tests (SSRT), microstructral observartion, and thermal desorption mass spectroscope (TDS). Hydrogen charging test results indicates that apparent hydrogen diffusive index Da is 1.94 × 10−7/cm2·s−1 for 0.21wt.% vanadium steel, while the value is 8.05×10−7/cm2·s−1 for V-free steel. SSRT results show that the hydrogen induced ductility loss ID is 76.2% for 0.21wt.%V steel, compared with 86.5% for V-free steel. The trapping mechanism of the steel containing different V contents is analyzed by means of TDS and Transmission electron microscope (TEM) observations. It is found out that the steel containing 0.21wt.%V can create much more traps for hydrogen trapping compared with lower V steel, which is due to vanadium carbide (VC) precipitates acting as traps capturing hydrogen atoms.The relationship between hydrogen diffusion and hydrogentrapping mechanism is discussed in details.

Microstructure and Mechanical Properties of TRIP-Aided Steels with Different Heat Treatments

2015 ◽  
Vol 817 ◽  
pp. 439-443 ◽  
Author(s):  
Rui Dong ◽  
Ai Min Zhao ◽  
Ran Ding ◽  
Jian Guo He ◽  
Han Jiang Hu
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Total Elongation ◽  
Heat Treatments ◽  
Second Phase ◽  
Soft Matrix ◽  
Significant Difference

The microstructures, mechanical properties and retained austenite characteristics of TRIP-aided steels with three different heat treatments were studied in this paper. The results indicated that the designed annealing treatments resulted in completely different matrices and the morphologies of second phase, and a significant difference in mechanical properties. The TAM steel was found to have fine annealed martensite lath matrix and inter lath acicular retained austenite, and possessed an excellent combination of strength and elongation which attributed to the highest retained austenite volume fraction and carbon concentration. For TPF steel, the higher instability and lower carbon content of retained austenite and the soft matrix resulted in the lowest ultimate tensile strength and total elongation. While in TBF steel, the stability of retained austenite was lower than that in TAM steel but higher than that in TPF steel. The ultimate tensile strength of TBF was significantly higher than the TAM and TPF steels, but the ductility of TBF steel was lower than TAM steel.

scholarly journals Microstructure and mechanical properties of Mo-Nb microalloyed medium Manganese trip Steel by cyclic quenching

10.30544/426 ◽  
2019 ◽  
Vol 25 (2) ◽  
pp. 139-146 ◽  
Author(s):  
Chunquan Liu ◽  
Qichun Peng ◽  
Zhengliang Xue
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Ultimate Tensile Strength ◽  
Trip Steel ◽  
Volume Fraction ◽  
Total Elongation ◽  
Reverse Transformation ◽  
Comprehensive Properties ◽  
Cyclic Quenching ◽  
Strength And Ductility

A novel cyclic quenching (CQ) and austenite reverse transformation (ART) was proposed for a Fe-0.25C-3.98Mn-1.22Al-0.20Si-0.19Mo-0.03Nb (wt.%) Mo-Nb microalloyed medium-Mn TRIP steel to improve strength and ductility. The results show that after twice cyclic quenching and ART exhibited optimum comprehensive properties, characterized by an ultimate tensile strength of 838 MPa, a total elongation of 90.8%, a product of strength and elongation (PSE) of 76.1 GPa·%, and the volume fraction of austenite of approximately 62 vol.%.

scholarly journals Optimal Design of High-Strength Ti‒Al‒V‒Zr Alloys through a Combinatorial Approach

Materials ◽  
2018 ◽  
Vol 11 (9) ◽  
pp. 1603
Author(s):  
Di Wu ◽  
Yueyan Tian ◽  
Ligang Zhang ◽  
Zhenyu Wang ◽  
Jinwen Sheng ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Volume Fraction ◽  
High Strength ◽  
Total Elongation ◽  
Peak Hardness ◽  
Combinatorial Approach ◽  
Α Phase ◽  
Lamella Thickness ◽  
Major Factors

The influence of various Zr contents (0–45 wt.%) on the microstructure and mechanical properties of Ti6Al4V alloy was investigated through a combinatorial approach. The diffusion multiples of Ti6Al4V–Ti6Al4V20Fe–Ti6Al4V20Cr–Ti6Al4V20Mo–Ti6Al4V45Zr were manufactured and diffusion-annealed to obtain a large composition space. Scanning electron microscopy, electron probe micro-analysis, and a microhardness system were combined to determine the relationships among the composition, microstructure, and hardness of these alloys. The Ti–6Al–4V–30Zr alloy was found to contain the thinnest α lath and showed peak hardness. X-ray diffraction and transmission electron microscope results indicated that after quenching from the β-field, the metastable α″-phase formed; moreover, at the secondary aging stage, the metastable α″-phase acted as precursor nucleation sites for the stable α-phase. The bulk Ti6Al4V30Zr alloy was manufactured. After aging at 550 °C, the alloy showed excellent balance of strength and ductility, and the tensile strength was 1464 MPa with a moderate elongation (8.3%). As the aging temperature increased, the tensile strength and yield strength of the alloys rose, but the total elongation decreased. The lamella thickness and volume fraction of the α-phase were the major factors that had great impacts on the mechanical properties.

scholarly journals A Novel Cyclic-Quenching-ART for Stabilizing Austenite in Nb–Mo Micro-Alloyed Medium-Mn Steel

Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1090 ◽  
Author(s):  
Chunquan Liu ◽  
Qichun Peng ◽  
Zhengliang Xue ◽  
Chengwei Yang
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Total Elongation ◽  
Practical Significance ◽  
Strengthening Effect ◽  
Medium Mn Steel ◽  
Cyclic Quenching ◽  
Mn Steel

In the context of obtaining an excellent elongation and tensile-strength combination in the third generation of advanced high strength steel, we emphasized the practical significance of adjusting the retained austenite fraction and stability in medium-Mn steel to obtain better mechanical properties. A novel cyclic quenching and austenite reverse transformation (CQ-ART) was used to obtain a large retained austenite content in Fe-0.25C-3.98Mn-1.22Al-0.20Si-0.19Mo-0.03Nb (wt.%) Nb–Mo micro-alloyed medium-Mn steel. The results show that after twice cyclic quenching and ART, the alloy exhibited optimum comprehensive properties, characterized by an ultimate tensile strength of 838 MPa, a total elongation of 90.8%, a product of strength and elongation of 76.1 GPa%, and the volume fraction of austenite of approximately 62 vol.%. The stability of retained austenite was significantly improved with the increasing of the number of cyclic quenching. Moreover, the effects of CQ-ART on the microstructure evolution, mechanical properties, C/Mn partitioning behavior, and austenite stability were investigated. Further, the strengthening effect of microalloying elements Nb–Mo was also discussed.

scholarly journals Low-carbon cast microalloyed steel intercritically heat-treated at different temperatures: microstructure and mechanical properties

2021 ◽  
Vol 21 (2) ◽  
Author(s):  
Hadi Torkamani ◽  
Shahram Raygan ◽  
Carlos Garcia Mateo ◽  
Yahya Palizdar ◽  
Jafar Rassizadehghani ◽  
...  
Keyword(s):  
Carbon Content ◽  
Volume Fraction ◽  
Block Size ◽  
Tensile Tests ◽  
Total Elongation ◽  
Martensite Phase ◽  
Low Carbon ◽  
Steel Increase ◽  
Different Temperatures ◽  
The Impact

AbstractIn this study, dual-phase (DP, ferrite + martensite) microstructures were obtained by performing intercritical heat treatments (IHT) at 750 and 800 °C followed by quenching. Decreasing the IHT temperature from 800 to 750 °C leads to: (i) a decrease in the volume fraction of austenite (martensite after quenching) from 0.68 to 0.36; (ii) ~ 100 °C decrease in martensite start temperature (Ms), mainly due to the higher carbon content of austenite and its smaller grains at 750 °C; (iii) a reduction in the block size of martensite from 1.9 to 1.2 μm as measured by EBSD. Having a higher carbon content and a finer block size, the localized microhardness of martensite islands increases from 380 HV (800 °C) to 504 HV (750 °C). Moreover, despite the different volume fractions of martensite obtained in DP microstructures, the hardness of the steels remained unchanged by changing the IHT temperature (~ 234 to 238 HV). Applying lower IHT temperature (lower fraction of martensite), the impact energy even decreased from 12 to 9 J due to the brittleness of the martensite phase. The results of the tensile tests indicate that by increasing the IHT temperature, the yield and ultimate tensile strengths of the DP steel increase from 493 to 770 MPa, and from 908 to 1080 MPa, respectively, while the total elongation decreases from 9.8 to 4.5%. In contrast to the normalized sample, formation of martensite in the DP steels could eliminate the yield point phenomenon in the tensile curves, as it generates free dislocations in adjacent ferrite.

scholarly journals Continuous Cooling Transformation Behaviour and Bainite Transformation Kinetics of 23CrNi3Mo Carburised Steel

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 48
Author(s):  
Wenjun Song ◽  
Min Lei ◽  
Mingpan Wan ◽  
Chaowen Huang
Keyword(s):  
Phase Transformation ◽  
Volume Fraction ◽  
Austenite Formation ◽  
Steel Matrix ◽  
Transformation Kinetics ◽  
Bainite Transformation ◽  
Continuous Cooling ◽  
The Matrix ◽  
Dimensional Growth ◽  
Kinetics Of

In this study, the phase transformation behaviour of the carburised layer and the matrix of 23CrNi3Mo steel was comparatively investigated by constructing continuous cooling transformation (CCT) diagram, determining the volume fraction of retained austenite (RA) and plotting dilatometric curves. The results indicated that Austenite formation start temperature (Ac1) and Austenite formation finish temperature (Ac3) of the carburised layer decreased compared to the matrix, and the critical cooling rate (0.05 °C/s) of martensite transformation is significantly lower than that (0.8 °C/s) of the matrix. The main products of phase transformation in both the carburised layer and the matrix were martensite and bainite microstructures. Moreover, an increase in carbon content resulted in the formation of lamellar martensite in the carburised layer, whereas the martensite in the matrix was still lath. Furthermore, the volume fraction of RA in the carburised layer was higher than that in the matrix. Moreover, the bainite transformation kinetics of the 23CrNi3Mo steel matrix during the continuous cooling process indicated that the mian mechanism of bainite transformation of the 23CrNi3Mo steel matrix is two-dimensional growth and one-dimensional growth.

scholarly journals Heat Treatment Evaluation for the Camshafts Production of ADI Low Alloyed with Vanadium

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1036
Author(s):  
Eduardo Colin García ◽  
Alejandro Cruz Ramírez ◽  
Guillermo Reyes Castellanos ◽  
José Federico Chávez Alcalá ◽  
Jaime Téllez Ramírez ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Tensile Strength ◽  
Ductile Iron ◽  
Volume Fraction ◽  
Energy Impact ◽  
Treatment Conditions ◽  
Mold Casting ◽  
Grade 3 ◽  
Good Agreement

Ductile iron camshafts low alloyed with 0.2 and 0.3 wt % vanadium were produced by one of the largest manufacturers of the ductile iron camshafts in México “ARBOMEX S.A de C.V” by a phenolic urethane no-bake sand mold casting method. During functioning, camshafts are subject to bending and torsional stresses, and the lobe surfaces are highly loaded. Thus, high toughness and wear resistance are essential for this component. In this work, two austempering ductile iron heat treatments were evaluated to increase the mechanical properties of tensile strength, hardness, and toughness of the ductile iron camshaft low alloyed with vanadium. The austempering process was held at 265 and 305 °C and austempering times of 30, 60, 90, and 120 min. The volume fraction of high-carbon austenite was determined for the heat treatment conditions by XRD measurements. The ausferritic matrix was determined in 90 min for both austempering temperatures, having a good agreement with the microstructural and hardness evolution as the austempering time increased. The mechanical properties of tensile strength, hardness, and toughness were evaluated from samples obtained from the camshaft and the standard Keel block. The highest mechanical properties were obtained for the austempering heat treatment of 265 °C for 90 min for the ADI containing 0.3 wt % V. The tensile and yield strength were 1200 and 1051 MPa, respectively, while the hardness and the energy impact values were of 47 HRC and 26 J; these values are in the range expected for an ADI grade 3.

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