scholarly journals Single-Sided Portable NMR Investigation to Assess and Monitor Cleaning Action of PVA-Borax Hydrogel in Travertine and Lecce Stone

Molecules ◽  
2021 ◽  
Vol 26 (12) ◽  
pp. 3697
Author(s):  
Valeria Stagno ◽  
Chiara Genova ◽  
Nicole Zoratto ◽  
Gabriele Favero ◽  
Silvia Capuani
Keyword(s):  
Pore Size ◽  
Experimental Conditions ◽  
Non Invasive ◽  
Bedding Planes ◽  
Paramagnetic Impurities ◽  
Two Samples ◽  
Action Time ◽  
Paramagnetic Agents ◽  
Portable Nmr ◽  
Non Destructive

In this work, we investigated the potential of PVA-borax hydrogel for cleaning limestones and the dependence of the cleaning on the porosity of the rock and on the action time of the hydrogel treatment. Towards this goal, we used a nuclear magnetic resonance (NMR) spectrometer, developed for non-invasive and non-destructive applications on cultural heritage. T2-NMR parameters were quantified on different samples of Lecce stone and Travertine cut perpendicular (Pe) and parallel (Pa) to the bedding planes under different experimental conditions: untreated samples, treated with Paraloid B72 and cleaned with PVA-PEO-borax hydrogel applied for 4 min and 2 h. The T2 results suggest that the effectiveness of the cleaning strongly depended on the porosity of the stones. In Lecce stone, the hydrogel seemed to eliminate both the paramagnetic impurities (in equal measure with 4 min and 2 h treatment) and Paraloid B72. In Travertine Pe, characterized by a smaller pore size compared to Lecce stone, no significant effects were found regarding both the cleaning and the treatment with Paraloid B72. In Travertine Pa, characterized by a larger pore size than the other two samples, the hydrogel seemed to clean the paramagnetic agents (it worked better if applied for a longer time) but it did not appear to have any effect on Paraloid B72 removal.

scholarly journals Non-invasive skin sampling of tryptophan/kynurenine ratio in vitro towards a skin cancer biomarker

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Skaidre Jankovskaja ◽  
Johan Engblom ◽  
Melinda Rezeli ◽  
György Marko-Varga ◽  
Tautgirdas Ruzgas ◽  
...  
Keyword(s):  
Skin Cancer ◽  
Relative Increase ◽  
Cancer Biomarker ◽  
Cancer Diagnostics ◽  
Sampling Time ◽  
Skin Permeability ◽  
Experimental Conditions ◽  
Non Invasive

AbstractThe tryptophan to kynurenine ratio (Trp/Kyn) has been proposed as a cancer biomarker. Non-invasive topical sampling of Trp/Kyn can therefore serve as a promising concept for skin cancer diagnostics. By performing in vitro pig skin permeability studies, we conclude that non-invasive topical sampling of Trp and Kyn is feasible. We explore the influence of different experimental conditions, which are relevant for the clinical in vivo setting, such as pH variations, sampling time, and microbial degradation of Trp and Kyn. The permeabilities of Trp and Kyn are overall similar. However, the permeated Trp/Kyn ratio is generally higher than unity due to endogenous Trp, which should be taken into account to obtain a non-biased Trp/Kyn ratio accurately reflecting systemic concentrations. Additionally, prolonged sampling time is associated with bacterial Trp and Kyn degradation and should be considered in a clinical setting. Finally, the experimental results are supported by the four permeation pathways model, predicting that the hydrophilic Trp and Kyn molecules mainly permeate through lipid defects (i.e., the porous pathway). However, the hydrophobic indole ring of Trp is suggested to result in a small but noticeable relative increase of Trp diffusion via pathways across the SC lipid lamellae, while the shunt pathway is proposed to slightly favor permeation of Kyn relative to Trp.

scholarly journals Non-Invasive Testing of Physical Systems Using Topological Sensitivity

2021 ◽  
Vol 11 (3) ◽  
pp. 1341
Author(s):  
María Higuera ◽  
José M. Perales ◽  
María-Luisa Rapún ◽  
José M. Vega
Keyword(s):  
Lamb Waves ◽  
General Purpose ◽  
Mathematical Tool ◽  
Non Destructive Testing ◽  
Destructive Testing ◽  
Topological Sensitivity ◽  
Physical Systems ◽  
Non Invasive ◽  
Active Infrared Thermography ◽  
Non Destructive

A review of available results on non-destructive testing of physical systems, using the concept of topological sensitivity, is presented. This mathematical tool estimates the sensitivity of a set of measurements in some given sensors, distributed along the system, to defects/flaws that produce a degradation of the system. Such degradation manifests itself on the properties of the system. The good performance of this general purpose post-processing method is reviewed and illustrated in some applications involving non-destructive testing. These applications include structural health monitoring, considering both elastodynamic ultrasonic guided Lamb waves and active infrared thermography. Related methods can also be used in other fields, such as diagnosis/prognosis of engineering devices, which is also considered.

scholarly journals Prevalence and Photobiology of Photosynthetic Dinoflagellate Endosymbionts in the Nudibranch Berghia stephanieae

Animals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 2200
Author(s):  
Ruben X. G. Silva ◽  
Paulo Cartaxana ◽  
Ricardo Calado
Keyword(s):  
Food Deprivation ◽  
Photosynthetic Efficiency ◽  
Rapid Decrease ◽  
Complete Loss ◽  
Symbiotic Association ◽  
Non Invasive ◽  
Sea Slugs ◽  
Non Destructive ◽  
Over Time

Berghia stephanieae is a stenophagous sea slug that preys upon glass anemones, such as Exaiptasia diaphana. Glass anemones host photosynthetic dinoflagellate endosymbionts that sea slugs ingest when consuming E. diaphana. However, the prevalence of these photosynthetic dinoflagellate endosymbionts in sea slugs appears to be short-lived, particularly if B.stephanieae is deprived of prey that host these microalgae (e.g., during bleaching events impacting glass anemones). In the present study, we investigated this scenario, along with food deprivation, and validated the use of a non-invasive and non-destructive approach employing chlorophyll fluorescence as a proxy to monitor the persistence of the association between sea slugs and endosymbiotic photosynthetic dinoflagellates acquired through the consumption of glass anemones. Berghia stephanieae deprived of a trophic source hosting photosynthetic dinoflagellate endosymbionts (e.g., through food deprivation or by feeding on bleached E. diaphana) showed a rapid decrease in minimum fluorescence (Fo) and photosynthetic efficiency (Fv/Fm) when compared to sea slugs fed with symbiotic anemones. A complete loss of endosymbionts was observed within 8 days, confirming that no true symbiotic association was established. The present work opens a new window of opportunity to rapidly monitor in vivo and over time the prevalence of associations between sea slugs and photosynthetic dinoflagellate endosymbionts, particularly during bleaching events that prevent sea slugs from incorporating new microalgae through trophic interactions.

scholarly journals The grades and freshness assessment of eggs based on density detection using machine vision and weighing sensor

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Supakorn Harnsoongnoen ◽  
Nuananong Jaroensuk
Keyword(s):  
Machine Vision ◽  
Vision System ◽  
Low Cost ◽  
Measuring System ◽  
Coefficient Of Determination ◽  
Water Displacement ◽  
Non Invasive ◽  
Future Potential ◽  
Non Destructive ◽  
Egg Freshness

AbstractThe water displacement and flotation are two of the most accurate and rapid methods for grading and assessing freshness of agricultural products based on density determination. However, these techniques are still not suitable for use in agricultural inspections of products such as eggs that absorb water which can be considered intrusive or destructive and can affect the result of measurements. Here we present a novel proposal for a method of non-destructive, non-invasive, low cost, simple and real—time monitoring of the grading and freshness assessment of eggs based on density detection using machine vision and a weighing sensor. This is the first proposal that divides egg freshness into intervals through density measurements. The machine vision system was developed for the measurement of external physical characteristics (length and breadth) of eggs for evaluating their volume. The weighing system was developed for the measurement of the weight of the egg. Egg weight and volume were used to calculate density for grading and egg freshness assessment. The proposed system could measure the weight, volume and density with an accuracy of 99.88%, 98.26% and 99.02%, respectively. The results showed that the weight and freshness of eggs stored at room temperature decreased with storage time. The relationship between density and percentage of freshness was linear for the all sizes of eggs, the coefficient of determination (R2) of 0.9982, 0.9999, 0.9996, 0.9996 and 0.9994 for classified egg size classified 0, 1, 2, 3 and 4, respectively. This study shows that egg freshness can be determined through density without using water to test for water displacement or egg flotation which has future potential as a measuring system important for the poultry industry.

scholarly journals Phenotyping plants: genes, phenes and machines

2012 ◽  
Vol 39 (11) ◽  
pp. 813 ◽  
Author(s):  
Roland Pieruschka ◽  
Hendrik Poorter
Keyword(s):  
Structural Information ◽  
Plant Phenotyping ◽  
Phenotypic Traits ◽  
Special Issue ◽  
Non Invasive ◽  
The Core ◽  
The Relationship ◽  
Non Destructive ◽  
Major Progress ◽  
Meaningful Data

No matter how fascinating the discoveries in the field of molecular biology are, in the end it is the phenotype that matters. In this paper we pay attention to various aspects of plant phenotyping. The challenges to unravel the relationship between genotype and phenotype are discussed, as well as the case where ‘plants do not have a phenotype’. More emphasis has to be placed on automation to match the increased output in the molecular sciences with analysis of relevant traits under laboratory, greenhouse and field conditions. Currently, non-destructive measurements with cameras are becoming widely used to assess plant structural properties, but a wider range of non-invasive approaches and evaluation tools has to be developed to combine physiologically meaningful data with structural information of plants. Another field requiring major progress is the handling and processing of data. A better e-infrastructure will enable easier establishment of links between phenotypic traits and genetic data. In the final part of this paper we briefly introduce the range of contributions that form the core of a special issue of this journal on plant phenotyping.

Determination of the pore size of woven structures through image analysis

2012 ◽  
Vol 2 (1) ◽  
Author(s):  
R. Angelova
Keyword(s):  
Pore Size ◽  
Single Layer ◽  
Woven Fabric ◽  
Virtual Model ◽  
Experimental Procedure ◽  
Porosity And Permeability ◽  
Woven Structures ◽  
Woven Structure ◽  
Non Destructive

AbstractThe paper presents an experimental procedure developed for determination of the pore size, shape and distribution in a single layer woven fabric, for the construction of a virtual model to be incorporated in a future CFD software package. The procedure is based on non-destructive observation and analysis of woven samples. 14 different samples of gray fabrics of 100 % cotton in plain and twill weaves are investigated. The results obtained allow the creation of reality more realistic virtual model of the woven structure, and theoretical investigation of its porosity and permeability through computer simulation.

Microplasma synthesized gold nanoparticles for surface enhanced Raman spectroscopic detection of methylene blue

2021 ◽  
Author(s):  
Xuanhe Li ◽  
Liangliang Lin ◽  
Wei-Hung Chiang ◽  
Kuan Chang ◽  
Hujun Xu
Keyword(s):  
Rapid Detection ◽  
Chemical Species ◽  
Spectroscopic Technique ◽  
Trace Level ◽  
Raman Spectroscopic ◽  
Non Invasive ◽  
Surface Enhanced ◽  
Surface Enhanced Raman ◽  
Enhanced Raman Scattering ◽  
Non Destructive

Surface enhanced Raman scattering (SERS) is a powerful and sensitive spectroscopic technique that allows for rapid detection of trace-level chemical species in a non-invasive and non-destructive manner. In the present...

Fertilization state ofAscaris suumdetermined by electrorotation

2006 ◽  
Vol 80 (1) ◽  
pp. 25-31 ◽  
Author(s):  
C. Dalton ◽  
A.D. Goater ◽  
H.V. Smith
Keyword(s):  
Dielectric Properties ◽  
Physicochemical Properties ◽  
Parasitic Nematode ◽  
Invasive Technique ◽  
Non Invasive ◽  
Egg Morphology ◽  
Parasite Biology ◽  
Response Modelling ◽  
Non Destructive ◽  
Insight Into

AbstractElectrorotation is a non-invasive technique that is capable of detecting changes in the morphology and physicochemical properties of microorganisms. The first detailed electrorotation study of the egg (ovum) of a parasitic nematode, namelyAscaris suumis described to show that electrorotation can rapidly differentiate between fertilized and non-fertilized eggs. Support for this conclusion is by optical microscopy of egg morphology, and also from modelling of the electrorotational response. Modelling was used to determine differences in the dielectric properties of the unfertilized and fertilized eggs, and also to investigate specific differences in the spectra of fertilized eggs only, potentially reflecting embryogenesis. The potential of electrorotation as an investigative tool is shown, as undamaged eggs can be subjected to further non-destructive and destructive techniques, which could provide further insight into parasite biology and epidemiology.

Nondestructive Extraction of Parameters of Multilayered Media Using Terahertz Pulse Technique

Frequenz ◽  
2019 ◽  
Vol 73 (1-2) ◽  
pp. 63-70
Author(s):  
Surya Prakash Singh ◽  
Nilesh K. Tiwari ◽  
M. Jaleel Akhtar
Keyword(s):  
Refractive Index ◽  
Complex Refractive Index ◽  
Multilayered Structure ◽  
Terahertz Pulse ◽  
Destructive Testing ◽  
Multilayered Media ◽  
Pulse Technique ◽  
Non Invasive ◽  
Full Wave ◽  
Non Destructive

Abstract In this work, an efficient non-invasive terahertz pulse technique is proposed and investigated to determine the thickness and refractive index of each layer in an optically thick stratified media. A closed form formulations are derived for simultaneous extraction of the thickness and complex refractive index of each layer with the help of primary reflected signals from the multilayered structure. The proposed technique is numerically tested using a full wave electromagnetic simulator and is experimental verified in the millimeter wave frequency range by utilizing the power peaks corresponding to the primary reflected signals. The numerical and measured results of multilayered samples under test are in good agreement with the reference data. The proposed terahertz pulse technique can be used for non-destructive testing of the multilayered system existing in various industries.

scholarly journals Qualitative terpene profiling of Cannabis varieties cultivated for medical purposes

Rodriguésia ◽  
2020 ◽  
Vol 71 ◽  
Author(s):  
Ernesto Diaz Rocha ◽  
Vitória EA Silva ◽  
Fernanda CS Pereira ◽  
Valery M Jean ◽  
Fabio L Costa Souza ◽  
...  
Keyword(s):  
Raw Material ◽  
Control Methods ◽  
Intermediate Type ◽  
Spectral Library ◽  
Medical Cannabis ◽  
Two Samples ◽  
Different Strains ◽  
Main Component ◽  
Non Destructive

Abstract With the upcoming medical Cannabis regulation, quality control methods on raw material will be required. Besides testing for contaminants and potency, there are also pharmaceutical and forensic interests in the determination of the terpene profile in different strains of Cannabis as complementary identification methods. A simple non-destructive HS-SPME GC-MS method was used to identify the terpene content in twelve Cannabis samples, four of them were of the hemp type (Harle-tsu), seven from various marihuana types and one of the intermediate type. They all were previously analyzed by HPLC to determine the potency (THC and CBD content). Spectral library matching was used to identify the terpenes compounds. Thirty terpenes compounds were detected, nine of them were present in all Cannabis samples and used to find their terpene profile: α-pinene, β-pinene, β-myrcene, D-limonene, terpinolene, linalool, caryophyllene, α-bergamotene and humulene. Three of them, caryophyllene, α-pinene and β-myrcene were found as larger components in most of samples. A principal components analyses (PCA) was performed. The four hemp type samples showed two different profiles, two samples showed caryophyllene as main component and the others two with β-myrcene as such. The marihuana type samples showed wider profiles with no clear patterns at all, which is not surprising because of the low number of samples. The simple methodology shows viable to set the terpenes profile for analyses of raw Cannabis material. Suitability for differentiation between different sorts of types needs more studies, with increasing numbers of samples.

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