scholarly journals Microencapsulation of Lemongrass (Cymbopogon citratus) Essential Oil Via Spray Drying: Effects of Feed Emulsion Parameters

Processes ◽  
2020 ◽  
Vol 8 (1) ◽  
pp. 40 ◽  
Author(s):  
Nguyen Phu Thuong Nhan ◽  
Vo Tan Thanh ◽  
Mai Huynh Cang ◽  
Tri Duc Lam ◽  
Nguyen Cam Huong ◽  
...  
Keyword(s):  
Essential Oil ◽  
Essential Oils ◽  
Spray Drying ◽  
Gum Arabic ◽  
Core Material ◽  
Wall Material ◽  
Cymbopogon Citratus ◽  
Encapsulation Process ◽  
Wall Materials ◽  
Lemongrass Essential Oil

The purpose of this study was to attempt the encapsulation of lemongrass (Cymbopogon citratus) essential oil utilizing spray drying technique. An array of process parameters including concentration of wall (15–30%), type of wall materials (maltodextrin, maltodextrin and gum Arabic mixture), and concentration of essential oil (0.5–2.0%) were thoroughly investigated. The results show that the use of sole maltodextrin as encapsulant gave microcapsules characteristics comparable to that of powder produced using maltodextrin and gum Arabic mixture. The encapsulation process that was performed with maltodextrin at the concentration of 30% as wall material and lemongrass essential oil at the concentration of 1.5% as core material showed highest drying yield (84.49%), microencapsulation yield (89.31%) and microencapsulation efficiency (84.75%). Encapsulated essential oils retained most of their major constituents in comparison with the bare essential oils without any significant compromise in product quality.

scholarly journals Encapsulation efficiency and thermal stability of lemongrass (Cymbopogon citratus) essential oil microencapsulated by the spray-drying process

Food Research ◽  
2020 ◽  
Vol 5 (1) ◽  
pp. 195-202
Author(s):  
P.T.N. Nguyen ◽  
T.T. Vo ◽  
T.Y.N. Tran ◽  
T.H.N. Le ◽  
H.C. Mai ◽  
...  
Keyword(s):  
Essential Oil ◽  
Spray Drying ◽  
Treatment Time ◽  
Heating Temperature ◽  
Core Material ◽  
Wall Material ◽  
Cymbopogon Citratus ◽  
Liquid Form ◽  
The Stability ◽  
Lemongrass Essential Oil

Encapsulation is a potential technique that is widely studied and applied in the preservation of biological compounds and living cells. Lemongrass (Cymbopogon citratus) essential oil is a biological compound that emits a strong aroma and contains robust antibacterial compounds, hence its applications in various areas such as food, pharmaceuticals and cosmetics. However, lemongrass essential oil is in a liquid form, so it is easy to evaporate and oxidize when being exposed to temperature variations, oxygen, and light. Hence, the present study was aimed to determine the effects of heating temperature and time on the stability of microencapsulated lemongrass essential oil powder. In this research, microencapsulated powder was produced by the spray-drying method using maltodextrin (30%, w/w) as the wall material and lemongrass (1.5%, w/w) as the core material. Thereafter, the effects of heat during processing, including temperature (60°C to 180°C) and treatment time (from 20 to 80 mins) were evaluated. The results showed that when the temperature and the time increased, the color of powder became darker and OR values were rapidly reduced. The selected optimal temperature and time was 100°C and 20 mins. The encapsulated essential oil maintained its main components including nerol, citral a, citral b, and geraniol, even after being heated.

scholarly journals Ultrasound-assisted emulsions with biopolymers for spray-drying of lemongrass essential oil

2021 ◽  
Vol 56 ◽  
Author(s):  
Gabriel Ribeiro Carvalho ◽  
Amanda Maria Teixeira Lago ◽  
Maria Cecília Evangelista Vasconcelos Schiassi ◽  
Priscila de Castro e Silva ◽  
Soraia Vilela Borges ◽  
...  
Keyword(s):  
Essential Oil ◽  
Spray Drying ◽  
Gum Arabic ◽  
Partial Substitution ◽  
Partial Replacement ◽  
Wall Material ◽  
Drying Process ◽  
Osa Starch ◽  
Ultrasound Assisted ◽  
Lemongrass Essential Oil

Abstract The objective of this work was to evaluate the partial replacement of gum arabic by modified starches on the spray-drying microencapsulation of lemongrass (Cymbopogon flexuosus) essential oil. The ultrasound-assisted emulsions were prepared with 30% (w/w) of wall material, 7.5% (w/w) of oil load, and 1:1 (w/w) replacement ratio for all treatments. After 16 hours, the incompatibility observed between gum arabic and octenyl succinic anhydride (OSA) starch did not affect the obtained microparticles, since the treatment with OSA starch, partially replacing gum arabic, showed the best results for the process yield and for the oil charge retention after spray-drying process, and the treatment showed Newtonian viscosity close to that of the treatment prepared with gum arabic. Maltodextrin dextrose equivalent 10 (10DE) shows an oil load similar to that of the treatment with gum arabic, while the presence of maize maltodextrin DE20 reduces the content of encapsulated oil and the efficiency of the drying process due to the adherence of particles to the chamber. Therefore, the partial substitution of gum arabic is an alternative for the formation of emulsions, for the spray-drying microencapsulation of lemongrass essential oil.

Response Surface Optimization on Microencapsulation of Lemongrass Essential Oil Using Spray Drying

2020 ◽  
Vol 859 ◽  
pp. 271-276
Author(s):  
Teerawat Boonsom ◽  
Ekachai Dumkliang
Keyword(s):  
Essential Oil ◽  
Response Surface ◽  
Spray Drying ◽  
Encapsulation Efficiency ◽  
Food Additives ◽  
Gum Arabic ◽  
Cassava Starch ◽  
Wall Material ◽  
Mass Ratio ◽  
Lemongrass Essential Oil

Microencapsulation by spray drying is offered to prevent volatilization or degradation of lemongrass essential oil as food additives and ingredients in traditional medicines. In this process, oil is contained in microcapsules by enclosing with wall material. Although gum arabic is commonly used according to its encapsulation efficiency and stability, its cost is more expensive. This experiment used cassava starch for wall material because it was cheaper than gum and could get optimized condition for microencapsulation of lemongrass essential oil. The 3 factors of microcapsulation consisting of the mass ratio of CS:GA, mass ratio of wall: core materials, and inlet temperatures were optimized for maximum response, the process yield (PY) and encapsulation efficiency (EE) using response surface methodology. The results concluded that the highest weight replacement of cassava starch and gum arabic at 2.4:1, wall:core ratio 3.4-4.0:1 with inlet air temperature about 180 °C for spray drying was the optimal condition for was higher than 70 % PY and 85 % EE.

scholarly journals Development of bioactive/active additives based on essential oils: A review

2020 ◽  
Vol 3 (4) ◽  
pp. 60-67
Author(s):  
Jessica Alarcón-Moyano ◽  
◽  
Silvia Matiacevich ◽  
Keyword(s):  
Medicinal Plants ◽  
Essential Oil ◽  
Essential Oils ◽  
Freeze Drying ◽  
The Other ◽  
Wall Material ◽  
Oil Oxidation ◽  
Active Additive ◽  
Wall Materials ◽  
Selection For

The use of bioactive/active additives has been increasing in recent years, especially those derived from medicinal plants such as essential oils. However, due to essential oil oxidation it is necessary to protect it by encapsulation techniques such as: emulsion, spray- and/or freeze-drying as the most economical techniques. On the other hand, an important factor is to determine the appropriate wall material to obtain a prolonged or controlled release in the food or in the organism. Therefore, several factors affect the release of the compounds such as the type, amount of wall material and/or combination of wall materials. Therefore, the knowledge of all the aforementioned factors is important in order to make an adequate selection for the development of a bioactive/active additive based on essential oils.

Preparation and Characterization of Naturally Scented Candles Using the Lemongrass (Cymbopogon citratus) Essential Oil

2020 ◽  
Vol 977 ◽  
pp. 212-217
Author(s):  
Hoang Danh Pham ◽  
Tri Nhut Pham ◽  
Do Thi Kim Nga ◽  
Ngan Thi Thu Nhung ◽  
Tri Duc Lam ◽  
...  
Keyword(s):  
Citric Acid ◽  
Essential Oil ◽  
Essential Oils ◽  
Health Effects ◽  
Low Cost ◽  
Cymbopogon Citratus ◽  
Natural Sources ◽  
The Common ◽  
Lemongrass Essential Oil

At present, there are many different forms of relaxation and aromatic candles are one of the common forms. Scented candles not only provide background lighting but also help promoting a feeling of wellness. This study attempts to produce scented candles from natural sources such as soy wax, beeswax, and natural essential oils to bring the most practical benefits to the users. The produced candle should be long lasting, low cost and causes no health effects. The composition of scented candles included 60% beeswax, 30% soy wax, 8% lemongrass essential oil, 1% citric acid, and 1% ethanol.

Influence of Different Wall Materials on the Microencapsulation of Virgin Coconut Oil by Spray Drying

2015 ◽  
Vol 11 (1) ◽  
pp. 61-69 ◽  
Author(s):  
Yen Yi Hee ◽  
Chin Ping Tan ◽  
Russly Abdul Rahman ◽  
Noranizan Mohd Adzahan ◽  
Wee Ting Lai ◽  
...  
Keyword(s):  
Oxidative Stability ◽  
Spray Drying ◽  
Encapsulation Efficiency ◽  
Coconut Oil ◽  
Gum Arabic ◽  
Sodium Caseinate ◽  
Whey Protein Concentrate ◽  
Wall Material ◽  
Virgin Coconut Oil ◽  
Wall Materials

Abstract The main objective of this study was to evaluate the influence of the different wall material combinations on the microencapsulation of virgin coconut oil (VCO) by spray drying. Maltodextrin (MD) and sodium caseinate (SC) were used as the basic wall materials and mixed with gum Arabic (GA), whey protein concentrate (WPC) and gelatin (G). The stability, viscosity and droplet size of the feed emulsions were measured. MD:SC showed the best encapsulation efficiency (80.51%) and oxidative stability while MD:SC:GA presented the lowest encapsulation efficiency (62.93%) but better oxidative stability than the other two combinations. Microcapsules produced were sphere in shape with no apparent fissures and cracks, low moisture content (2.35–2.85%) and high bulk density (0.23–0.29 g/cm3). All the particles showed relatively low peroxide value (0.34–0.82 meq peroxide/kg of oil) and good oxidative stability during storage. MD:SC:GA microencapsulated VCO had the highest antioxidant activity in both of the 2,2-diphenyl-1-picrylhydrazyl (DPPH) (0.22 mmol butylated hydroxyanisole (BHA)/kg of oil) and 2,2-azinobis (3-ethylbenzothiazoline-6-sulfonic acid) (ABTS) assays (1.35 mmol trolox/kg of oil).

scholarly journals Microencapsulation of Camelina sativa Oil Using Selected Soluble Fractions of Dietary Fiber as the Wall Material

Foods ◽  
2019 ◽  
Vol 8 (12) ◽  
pp. 681 ◽  
Author(s):  
Kanclerz ◽  
Drozińska ◽  
Kurek
Keyword(s):  
Dietary Fiber ◽  
High Efficiency ◽  
Gum Arabic ◽  
Camelina Sativa ◽  
Core Material ◽  
Wall Material ◽  
The Core ◽  
Wall Materials ◽  
Low Efficiency

The aim of the study was to prove the usefulness of microencapsulation of Camelina sativa oil regarding its vulnerability to oxidation caused by oxygen, temperature, and other factors. Pectin, inulin, gum arabic, and β-glucan, each of them mixed with maltodextrin, were used as wall materials and their appropriability to reduce oxidation of the core material was examined. Microcapsules were prepared by spray drying, which is the most commonly used and very effective method. The research confirmed results known from literature, that gum arabic and inulin are most proper wall materials, because they ensure small oxidation increase during storage (4.59 and 5.92 eq/kg after seven days respectively) and also provide high efficiency of process (83.93% and 91.74%, respectively). Pectin turned out to be the least appropriate polysaccharide because it is not able to assure sufficient protection for the core material, in this case Camelina sativa oil, due to low efficiency (61.36%) and high oxidation (16.11 eq/kg after seven days). β-glucan occurred to be the coating material with relatively high encapsulation efficiency (79.26%) but high humidity (4.97%) which could negatively influence the storage of microcapsules. The use of polysaccharides in microencapsulation, except performing the role of wall material, has the advantage of increasing the amount of dietary fiber in human diet.

scholarly journals Influence of wall materials on the microencapsulation of pequi oil by spray drying

2020 ◽  
Vol 23 ◽  
Author(s):  
Fabiana Helen dos Santos ◽  
Bianca Marise Pereira e Silveira ◽  
Lourena Lopes de Souza ◽  
Anna Karolina Cruz Duarte ◽  
Milton Cosme Ribeiro ◽  
...  
Keyword(s):  
Moisture Content ◽  
Antioxidant Capacity ◽  
Size Distribution ◽  
Spray Drying ◽  
Water Activity ◽  
Droplet Size ◽  
Encapsulation Efficiency ◽  
Gum Arabic ◽  
Wall Material ◽  
Wall Materials

Abstract The aim of this study was to assess the influence of the wall materials on the microencapsulation of pequi oil. An emulsion containing pequi oil in the oil phase was microencapsulated by spray drying process at 120 °C using gum Arabic, maltodextrin, or a 25:75 (w/w) mixture of gum Arabic and maltodextrin as wall material. The emulsions were characterized for droplet size, Polydispersity Index (PDI), and zeta potential. Pequi oil microparticles were analyzed for moisture content, water activity, wettability, encapsulation efficiency, antioxidant capacity, and color. Ultrastructural examination was performed by Scanning Electron Microscopy (SEM). The Droplet Size Distribution (DSD) of the emulsions exhibited a relatively wide size distribution (2.67 to 8.96 μm) and high PDI (> 0.3). Smooth microparticles with high encapsulation efficiency (79.17% to 84.20%), and good antioxidant capacity (28.20 to 28.71 μmol Trolox equivalents/g dry extract) were obtained. Microparticles prepared using gum Arabic as wall material had higher antioxidant capacity than that prepared with maltodextrin. All microparticles had satisfactory encapsulation efficiency, water activity, moisture content, and wettability. These results indicate that pequi oil microparticles have characteristics that can contribute to good stability during storage and handling of encapsulated oil. Therefore, pequi oil can be successfully encapsulated by spray drying using gum Arabic, maltodextrin, or 25:75 (w/w) mixture of gum Arabic and maltodextrin as wall materials, but the physicochemical properties of microparticles vary with wall material composition.

scholarly journals Perbandingan randemen minyak atsiri sereh (cymbopogon citratus) yang umur panennya 6 bulan Dan 9 bulan dengan metode destilasi air)

2019 ◽  
Vol 10 (3) ◽  
pp. 66-71
Author(s):  
Rani Prabandari
Keyword(s):  
Essential Oil ◽  
Soil Fertility ◽  
Essential Oils ◽  
Test Sample ◽  
Distillation Method ◽  
Average Yield ◽  
Cymbopogon Citratus ◽  
Water Distillation ◽  
Significant Difference ◽  
Lemongrass Essential Oil

AbstractIndonesian nature is very rich in plants containing essential oils. Essential oils can be produced from various parts of plants such as roots, stems, leaves, flowers, or fruit. There are 50-200 species of essential oil producing plants. In Indonesia there are around 40 types of essential oils producing plants. One of the essential oils producing plants is lemongrass (Taufiq, Tuhana, 2008 p: 2). This study aims to determine the comparison of essential oils in Lemongrass (Cymbopogon citratus) which are harvested at 6 months and 9 months with a water distillation method. The procedure for selecting samples and research samples, directly with the object of research, is the citronella plant whose harvest age is 6 months taken from 1 clump and 9 months taken from 1 clump. The results of this study indicate that lemongrass plants with a harvest age of 6 months produce more essential oils compared to lemongrass plants with a harvest age of 9 months. This is influenced by several factors, including climate, harvest age. Lemongrass plants aged 6 months are the optimal age to be harvested, so that they get a higher yield of essential oils, besides that the factors of soil fertility and the intensity of sunlight also affect the content of essential oils of lemongrass.From the results of the research that has been done on the test sample, it can be concluded that the results of the essential oil ration on citronella (Cymbopogon citratus), which has 6 months of harvest age, obtained an average yield of 0.46% v / b and 9 months. 0.35% v / b with the results of the t-test obtained by the price t-count (2.984)> t-table (2.776). So that H0 is rejected and Ha is accepted and it can be concluded that there is a significant difference between lemongrass with 6 months and 9 months of harvest. Keywords: lemongrass, essential oil, age of harvest, water distillation

scholarly journals Extraction and Formulation of Perfume from Cymbopogon citratus (Lemongrass)

2021 ◽  
Vol 25 (8) ◽  
pp. 1461-1463
Author(s):  
O.E. Ameh ◽  
J.I. Achika ◽  
N.M. Bello ◽  
A.J. Owolaja
Keyword(s):  
Solvent Extraction ◽  
Essential Oil ◽  
Essential Oils ◽  
Boiling Point ◽  
Extraction Method ◽  
Extraction Methods ◽  
Suitable Method ◽  
Oil Yield ◽  
Cymbopogon Citratus ◽  
Solvent Extraction Method

This work aimed to extract perfume from the leaves of Cymbopogon citratus using three extraction methods viz: distillation, solvent extraction and expression or effleurage. About 150 g of dried lemons grass were extracted using ethanol as the solvent to obtain essential oils required for the formulation of perfumes. The result of the hydrodistillation process showed that 1.23 g of essential oil per 130g of dry lemongrass produce 0.95% oil at 78 °C, while the effleurage method was 2.55 g of essential oil per 130 g of dry lemongrass sample thereby producing 1.96% oil yield. The solvent extraction method gave 2.7 g of essential oil per 130 g of dry lemongrass sample. This gives about 2.08 % yield of essential oil at a temperature of 78°C i.e. the boiling point of ethanol. The solvent extraction method yielded 2.08%, the effleuragemethod yielded 1.96% and the hydrodistillation method yielded 0.95% essential oil respectively. In conclusion, solvent extraction gave the highest yield because of less exposure to air and heat, which is highly recommended as the most suitable method for the extraction of essential oil.

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