Optimization of Preparation Process of Essential Oil of Baokening Granule-β-Cyclodextrin Inclusion by Orthogonal Test

2014 ◽  
Vol 937 ◽  
pp. 118-121
Author(s):  
Fang Luo ◽  
Shun Bin Qiao
Keyword(s):  
Essential Oil ◽  
Orthogonal Design ◽  
Process Condition ◽  
Phase Method ◽  
Optimum Process ◽  
Process Conditions ◽  
Inclusion Process ◽  
Preparation Conditions ◽  
Liquid Phase Method ◽  
Inclusion Rate

To study optimum inclusion process conditions for essential oil from perilla and Pericarpium Citri Reticulatae in Baokening granule,the utilization ratio of volatile and the inclusion rate were determined to evaluate process conditions, and the condition was optimized with orthogonal design by the liquid-phase method in aqueous solution. The experiment results showed that the optimum preparation conditions for inclusion were established as: oil: ß-CD was 1:8, and ratio of amount of water to ß –CD was 10. The inclusion temperature and time were at 40°C and for 180 min. The yield is high in such optimum process condition and the inclusion effect is good.

Study on Preparation Technology Optimization of Sultamicillin Tosilate-β-Cyclodextrin

2015 ◽  
Vol 1120-1121 ◽  
pp. 873-876
Author(s):  
Xiang Qun Xu ◽  
Nian Hong ◽  
Jie Yang ◽  
You Quan Zhong ◽  
Lin Cheng
Keyword(s):  
Orthogonal Experiment ◽  
Process Condition ◽  
Molar Ratio ◽  
Process Conditions ◽  
Preparation Technology ◽  
Inclusion Process ◽  
Cyclodextrin Inclusion ◽  
Main Factors ◽  
Time Of Reaction

To study the process conditions for preparing sultamicillin tosilate β-cyclodextrin inclusion.Method: Choose the usage ration of sultamicillin tosilate with β-cyclodextrin, the inclusion temperature and the time of reaction as the main factors, and use the inclusion yield as evaluated indicators and the process condition to conduct the L9 (34) orthogonal experiment Optimization Pack sultamicillin tosilate.Outcome: The optimum inclusion process condition: molar ratio of the sultamicillin tosilate with β-cyclodextrin is 1:8, inclusion temperature is 47°C, inclusion time is 40 minutes.Conclusion: The process condition of using β-cyclodextrin inclusion to inconcluse sultamicillin tosilate is feasible, effective, and of applicative value.

Study on Direct Reduction of Vanadium Slag

2015 ◽  
Vol 815 ◽  
pp. 254-262
Author(s):  
Neng Wei Wang ◽  
Guo Wei Li ◽  
Min Xian Fang
Keyword(s):  
Sodium Carbonate ◽  
Direct Reduction ◽  
Process Condition ◽  
Optimum Process ◽  
Process Conditions ◽  
Vanadium Slag ◽  
Anhydrous Sodium Carbonate ◽  
Factors Affecting ◽  
Roasting Temperature ◽  
Slag Reduction

In this paper the process of direct reduction of vanadium slag was adopted. The main factor was determined by uniform experimental design and single factor analysis, and then the optimum process condition was drawn by the test. The test results showed that the regression equation curve fitting of the experiment data was very significant, the main factors affecting the vanadium slag reduction (according to the primary and secondary order) was the content of anhydrous sodium carbonate, roasting temperature, roasting time and reduction of carbon content. The factors for the reduction of the optimum process conditions are the carbon coefficient 1.04, roasting temperature 1100°C, roasting reduction time 4h, 4% mass percent of anhydrous sodium carbonate and slag. Under the optimum conditions, the actual rate of weight loss and theory rate of weight were close to 0, the results could be reproduced, and the vanadium slag metallization rate was 75%~83%.

scholarly journals Direct Bioconversion of Oil Palm Empty Fruit Bunches for Bioethanol Production By Solid State Bioconversion

2010 ◽  
Vol 8 (2) ◽  
pp. 25-36
Author(s):  
Nassereldeen Ahmed Kabbashi ◽  
Md Zahangir Alam ◽  
M. Fahrurrazi Tompang
Keyword(s):  
Solid State ◽  
Moisture Content ◽  
Wheat Flour ◽  
Process Condition ◽  
Inoculum Size ◽  
Optimum Process ◽  
Process Conditions ◽  
Bioethanol Production ◽  
Maximum Production ◽  
Empty Fruit Bunches

The bioethanol production was conducted by utilizing agriculture waste, palm oil empty fruit bunches (EFB) with the aid of T. harzianum and yeast, Saccharomyces cerevisiae using solid state bioconversion method. The compatibility of various fungal strains was done as to develop the direct bioconversion process of compatible mixed culture. Analyzes such ethanol estimation, reducing sugar and glucosamine as growth indicator were conducted in order to select the best experimented run for optimization. The optimization of process conditions, by using central composite design (CCD) was carried out. Optimization of process condition was done with varied level of moisture content, pH, inoculum size, concentration of co-substrate (wheat flour) and mineral solutions. Statistical analysis showed that the optimum process condition for moisture content was 50% (v/w), pH of 4, inoculum size of 10% (v/v), concentration of wheat flour of 1% (v/v) and mineral solutions 1%(v/v). In this study, the application levels of the methods of environmental management in regards to the maximum production were determined. The final optimization with the developed process conditions indicated that the maximum production was increased from 14.315 (v/v) to 34.785(v/v).

Preparation of Aspirin-β-Cyclodextrin Inclusion Complex by Grinding Method

2015 ◽  
Vol 1120-1121 ◽  
pp. 882-885 ◽  
Author(s):  
Xiang Qun Xu ◽  
Nian Hong ◽  
Jing Wen Zheng ◽  
Bing Bing Guo ◽  
Lin Cheng
Keyword(s):  
Orthogonal Experiment ◽  
Process Condition ◽  
Molar Ratio ◽  
Process Conditions ◽  
Inclusion Process ◽  
Grinding Method ◽  
Cyclodextrin Inclusion ◽  
Main Factors ◽  
Cyclodextrin Inclusion Complex ◽  
Time Of Reaction

To study the process conditions for preparing aspirin β-cyclodextrin inclusion.Method: Choose the usage ration of aspirin with β-cyclodextrin and the time of reaction as the main factors, and use the inclusion yield as evaluated indicators and the process condition to conduct orthogonal experiment Optimization Pack aspirin.Outcome: The optimum inclusion process condition: molar ratio of the aspirin with β-cyclodextrin is 1:3, inclusion time is 60 minutes.Conclusion: The process condition of using β-cyclodextrin inclusion to inconcluse aspirin is feasible, effective, and of applicative value.

Optimization of Process Parameters for Injection Molding Based on Taguchi Technique

2012 ◽  
Vol 538-541 ◽  
pp. 1170-1174
Author(s):  
Shi Jun Fu
Keyword(s):  
Injection Molding ◽  
Process Parameters ◽  
Orthogonal Design ◽  
Mold Temperature ◽  
Optimum Process ◽  
Process Conditions ◽  
Injection Time ◽  
Melt Temperature ◽  
Injection Process ◽  
Packing Pressure

In this paper, Taguchi and CAE technique are combined to study the influence of process conditions on the warpage of injection molding parts through twice orthogonal design experiments, and the injection process parameters are optimized according to the warpage. For the parameters selected, melt temperature and packing pressure have effects on the warpage of injection molding parts are highly significant, injection time is significant, other parameters have little effects. Within the range of experiments, the warpage decreased with the rise of the melt temperature and packing pressure. At last, the optimum process parameters of injection are that the mold temperature is 60°C, packing time is 10s, melt temperature is240°C, packing pressure is 115MPa and injection time is 0.4s.

scholarly journals Optimization of Glass Edge Sealing Process Using Microwaves for Fabrication of Vacuum Glazing

2019 ◽  
Vol 9 (5) ◽  
pp. 874 ◽  
Author(s):  
Jae Kim ◽  
Young Kim ◽  
Euy Jeon
Keyword(s):  
Process Condition ◽  
Step Height ◽  
Optimum Process ◽  
Process Conditions ◽  
Main Process ◽  
Height Measurement ◽  
Effect Analysis ◽  
Response Optimization ◽  
Vacuum Glazing ◽  
Glass Edge

Among the various methods used for glass edge sealing, this study uses microwaves to seal glass edges. Through basic experiments, the main process conditions for edge sealing of glass were derived, and the experimental plan and analysis were carried out using the Box-Behnken method of response-surface analysis based on 3 factors and 3 levels. The step height which influences sealing was set as a response variable. If the step height becomes too large, the glass can be damaged, and if the step height is too small, the edge sealing will not be performed. Accordingly, process optimization that edge sealing is possible while minimizing the step height was carried out. A predictable regression equation was derived for the step height of edge sealing and the main-effect analysis was performed for the step height. Using the response-optimization tool, we derived the optimum process condition that minimized the step height of the edge sealing and verified that it matched the error value of 4.1% compared with the target value of the step height measurement result confirmed through the verification experiment.

Synthesis and conformational investigation of β-turn forming tetra- and hexapeptides

1982 ◽  
Vol 47 (7) ◽  
pp. 1884-1892
Author(s):  
A. N. Abdel Rahman ◽  
S. Abdel Rahman
Keyword(s):  
Energy Transfer ◽  
Phase Method ◽  
Conformational Study ◽  
Poly Ethylene Glycol ◽  
High Solubility ◽  
Liquid Phase Method ◽  
Conformational Investigation ◽  
Transfer Method ◽  
Poly Ethylene ◽  
Good Agreement

Tetra- and hexapeptides containing Pro-Gly or Gly-Pro or Aib-Pro in their sequences were synthesized using the liquid-phase method. The high solubility of the poly(ethylene glycol) bound peptides in water and in organic solvents enables the application of the singlet-singlet energy transfer method for conformational investigation of these peptides. The conformational study in solid state by IR and in solution by CD were carried out in parallel to the energy transfer method. The qualitative results generated by IR and CD were found to be in good agreement with the quantitative end-to-end distances given by the energy transfer method.

scholarly journals Identification of VOCs in essential oils extracted using ultrasound- and microwave-assisted methods from sweet cherry flower

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Huimin Zhang ◽  
Hongguang Yan ◽  
Quan Li ◽  
Hui Lin ◽  
Xiaopeng Wen
Keyword(s):  
Essential Oil ◽  
Sweet Cherry ◽  
Dimethyl Sulfide ◽  
Solid Phase ◽  
Oil Yield ◽  
Gas Chromatography Mass Spectrometry ◽  
Process Conditions ◽  
Important Indicator ◽  
Microwave Assisted ◽  
Essential Oil Yield

AbstractThe floral fragrance of plants is an important indicator in their evaluation. The aroma of sweet cherry flowers is mainly derived from their essential oil. In this study, based on the results of a single-factor experiment, a Box–Behnken design was adopted for ultrasound- and microwave-assisted extraction of essential oil from sweet cherry flowers of the Brooks cultivar. With the objective of extracting the maximum essential oil yield (w/w), the optimal extraction process conditions were a liquid–solid ratio of 52 mL g−1, an extraction time of 27 min, and a microwave power of 435 W. The essential oil yield was 1.23%, which was close to the theoretical prediction. The volatile organic compounds (VOCs) of the sweet cherry flowers of four cultivars (Brooks, Black Pearl, Tieton and Summit) were identified via headspace solid phase microextraction (SPME) and gas chromatography–mass spectrometry (GC–MS). The results showed that a total of 155 VOCs were identified and classified in the essential oil from sweet cherry flowers of four cultivars, 65 of which were shared among the cultivars. The highest contents of VOCs were aldehydes, alcohols, ketones and esters. Ethanol, linalool, lilac alcohol, acetaldehyde, (E)-2-hexenal, benzaldehyde and dimethyl sulfide were the major volatiles, which were mainly responsible for the characteristic aroma of sweet cherry flowers. It was concluded that the VOCs of sweet cherry flowers were qualitatively similar; however, relative content differences were observed in the four cultivars. This study provides a theoretical basis for the metabolism and regulation of the VOCs of sweet cherry flowers.

scholarly journals Indicative Marker Microbiome Structures Deduced from the Taxonomic Inventory of 67 Full-Scale Anaerobic Digesters of 49 Agricultural Biogas Plants

2021 ◽  
Vol 9 (7) ◽  
pp. 1457
Author(s):  
Julia Hassa ◽  
Johanna Klang ◽  
Dirk Benndorf ◽  
Marcel Pohl ◽  
Benedikt Hülsemann ◽  
...  
Keyword(s):  
Stable Process ◽  
Process Condition ◽  
Full Scale ◽  
Process Models ◽  
Process Efficiency ◽  
Process Conditions ◽  
Rrna Gene ◽  
General Process ◽  
Specific Distribution ◽  
Biogas Plants

There are almost 9500 biogas plants in Germany, which are predominantly operated with energy crops and residues from livestock husbandry over the last two decades. In the future, biogas plants must be enabled to use a much broader range of input materials in a flexible and demand-oriented manner. Hence, the microbial communities will be exposed to frequently varying process conditions, while an overall stable process must be ensured. To accompany this transition, there is the need to better understand how biogas microbiomes respond to management measures and how these responses affect the process efficiency. Therefore, 67 microbiomes originating from 49 agricultural, full-scale biogas plants were taxonomically investigated by 16S rRNA gene amplicon sequencing. These microbiomes were separated into three distinct clusters and one group of outliers, which are characterized by a specific distribution of 253 indicative taxa and their relative abundances. These indicative taxa seem to be adapted to specific process conditions which result from a different biogas plant operation. Based on these results, it seems to be possible to deduce/assess the general process condition of a biogas digester based solely on the microbiome structure, in particular on the distribution of specific indicative taxa, and without knowing the corresponding operational and chemical process parameters. Perspectively, this could allow the development of detection systems and advanced process models considering the microbial diversity.

Analyzing the Effect of Fiber, Yarn and Fabric Variables on Bagging Behavior of Single Jersey Weft Knitted Fabrics

2013 ◽  
Vol 8 (3) ◽  
pp. 155892501300800 ◽  
Author(s):  
Mitra Karimian ◽  
Hossein Hasani ◽  
Saeed Ajeli
Keyword(s):  
Optimum Process ◽  
Process Conditions ◽  
Knitted Fabrics ◽  
Yarn Twist ◽  
Fabric Density ◽  
Fabric Structure ◽  
Controllable Factors ◽  
Yarn Count ◽  
The Individual ◽  
Single Jersey

This research investigates the effect of fiber, yarn and fabric variables on the bagging behavior of single jersey weft knitted fabrics interpreted in terms of bagging fatigue percentage. In order to estimate the optimum process conditions and to examine the individual effects of each controllable factor on a particular response, Taguchi's experimental design was used. The controllable factors considered in this research are blending ratio, yarn twist and count, fabric structure and fabric density. The findings show that fabric structure has the largest effect on the fabric bagging. Factor yarn twist is second and is followed by fabric density, blend ratio and yarn count. The optimum conditions to achieve the least bagging fatigue ratio were determined.

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