Effect of SiC Nanoparticles Dispersion on the Microstructure and Mechanical Properties of Electroplated Sn-Bi Solder Alloy

2010 ◽  
Vol 11 ◽  
pp. 113-118 ◽  
Author(s):  
Chang Woo Lee ◽  
Y.S. Shin ◽  
S.H. Yoo
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Solder Alloy ◽  
High Reliability ◽  
Nanoparticle Dispersion ◽  
Sic Nanoparticles ◽  
Microstructure And Mechanical Properties ◽  
Nanoparticles Dispersion ◽  
Average Grain Size ◽  
Joining Strength

The effect of SiC nanoparticle dispersion was investigated for microstructure change and mechanical properties of Sn-Bi electroplated alloys. The diameters of SiC nanoparticle in this study were 45-55 nm. The SiC nanoparticles were mixed with Sn-Bi electroplating and then the nanoparticles were dispersed with ultrasonic vibrator. After the dispersion, the SiC dispersed Sn-Bi alloys were electroplated on Cu deposited Si wafer. The microstructure and mechanical properties of the sample were evaluated by FE-TEM, FE-SEM, EDS, and shear tester. For TEM observation, the specimens were prepared by ultramicrotome and FIB. The SiC nanoparticles were well-dispersed in Sn-Bi alloy. SiC particles were located near grain boundaries or grain inside. The average grain size of the solder alloy was decrease about 30% compared with the grain size of Sn-Bi alloy prepared in the same condition. Due to the grain refinement and dispersion hardening by SiC nanoparticles, the SiC dispersed Sn-Bi alloy is expected to obtain high reliability and joining strength when it applied to interconnection materials.

Influence of Annealing on the Microstructure and Mechanical Properties of Electrodeposited Nanocrystalline Nickel

2011 ◽  
Vol 683 ◽  
pp. 103-112 ◽  
Author(s):  
B. Yang
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Elastic Modulus ◽  
Grain Boundary ◽  
Boundary Structure ◽  
Boundary State ◽  
Microstructure And Mechanical Properties ◽  
Grain Boundary Structure ◽  
Average Grain Size ◽  
Different Grain Size

The evolution of the microstructure and mechanical properties of electrodeposited nanocrystalline Ni with different annealing procedures was studied systematically. For the annealed specimens hardness decreases with increasing average grain size but the dependence changes at different grain size ranges. The specimens annealed at a low temperature show higher hardness compared to the as-deposited nanocrystalline Ni, despite an increased measured average grain size. In association with this hardening an increase in elastic modulus and a decrease in microstrain was observed after annealing. With increasing annealing temperature both the tensile strength and the fracture strain were observed to decrease, this is companied with a transition from ductile to brittle in the fracture surfaces. These results indicated that the mechanical behaviour of nanocrystalline Ni depends not only on the average grain size but also on the grain boundary structure. A change in the grain boundary state arising from annealing may be responsible for the observed increase in hardness and elastic modulus as well as the deterioration of tensile properties.

Effect of Bi on Microstructure and Mechanical Properties of Extruded AZ80-2Sn Magnesium Alloy

2018 ◽  
Vol 37 (1) ◽  
pp. 97-103 ◽  
Author(s):  
Hansong Xue ◽  
Xinyu Li ◽  
Weina Zhang ◽  
Zhihui Xing ◽  
Jinsong Rao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Magnesium Alloy ◽  
Ultimate Tensile Strength ◽  
Yield Strength ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

AbstractThe effects of Bi on the microstructure and mechanical properties of AZ80-2Sn alloy were investigated. The results show that the addition of Bi within the as-cast AZ80-2Sn alloy promotes the formation of Mg3Bi2 phase, which can refine the grains and make the eutectic phases discontinuous. The addition of 0.5 % Bi within the as-extruded AZ80-2Sn alloy, the average grain size decreases to 12 μm and the fine granular Mg17Al12 and Mg3Bi2 phases are dispersed in the α-Mg matrix. With an increase in Bi content, the Mg17Al12 and Mg3Bi2 phases become coarsened and the grain size increases. The as-extruded AZ80-2Sn-0.5 %Bi alloy has the optimal properties, and the ultimate tensile strength, yield strength and elongation are 379.6 MPa, 247.1 MPa and 14.8 %, respectively.

Investigation of Microstructure and Mechanical Properties of Friction Stir Lap Jointed Ni Base Superalloy

2012 ◽  
Vol 724 ◽  
pp. 481-485
Author(s):  
Kuk Hyun Song ◽  
Kazuhiro Nakata
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Friction Stir Welding ◽  
Base Material ◽  
Lap Joints ◽  
Stir Zone ◽  
Inconel 600 ◽  
Friction Stir ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

This study evaluated the microstructure and mechanical properties of friction stir welded lap joints. Inconel 600 and SS 400 as experimental materials were selected, and friction stir welding was carried out at tool rotation speed of 200 rpm and welding speed of 100 mm/min. Applying the friction stir welding was notably effective to reduce the grain size of the stir zone, as a result, the average grain size of Inconel 600 was reduced from 20 μm in the base material to 8.5 μm in the stir zone. Joint interface between Inconel 600 and SS 400 showed a sound weld without voids and cracks. Also, the hook, along the Inconel 600 alloy from SS 400, was formed at advancing side, which directly affected an increase in peel strength. In this study, we systematically discussed the evolution on microstructure and mechanical properties of friction stir lap jointed Inconel 600 and SS 400.

Effects of Sr and B addition on microstructure and mechanical properties of AZ91 magnesium alloy

2007 ◽  
Vol 22 (9) ◽  
pp. 2423-2428 ◽  
Author(s):  
H.L. Zhao ◽  
S.K. Guan ◽  
F.Y. Zheng
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Tensile Strength ◽  
Az91 Alloy ◽  
Az91 Magnesium Alloy ◽  
Solidification Range ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size ◽  
B Additions ◽  
Az91 Magnesium

The effects of Sr and B addition on the microstructure and mechanical properties of AZ91 alloy were studied. The results of this work show that a small amount of Sr addition to AZ91 refined the grain size. The highest tensile strength was obtained from the alloy with the optimal composition of 0.5% Sr and 0.09% B added, in which the average grain size was 42 μm. The tensile strength and elongation of the AZ91–0.5%Sr–0.09%B alloy were 151 MPa and 1.62%, respectively. Some needle-shaped Al4Sr particles distributed mainly at grain boundaries have been observed in the alloys with Sr and B additions. The fluidity is improved significantly, and the solidification range decreased by adding Sr and B. The liquidus of AZ91 alloy decreased markedly with the addition of Sr and B, but the solidus hardly changed. Therefore, the solidification range can be decreased, which will improve the die-casting properties.

Synergetic Effect of ECAP and Friction Stir Welding on Microstructure and Mechanical Properties of Aluminium Sheets

2010 ◽  
Vol 667-669 ◽  
pp. 505-510
Author(s):  
Ilya Nikulin ◽  
Alla Kipelova ◽  
Sergey Malopheyev ◽  
Rustam Kaibyshev
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Friction Stir Welding ◽  
Base Metal ◽  
Synergetic Effect ◽  
Aluminum Matrix ◽  
Friction Stir ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

Friction stir welding (FSW) was used to join the submicrocrystalline (SMC) grained Al-Cu-Mg-Ag sheets produced by equal channel angular pressing (ECAP) followed by hot rolling (HR). The effect of SPD and FSW on the microstructure and mechanical properties in the zone of base metal, as well as in the stirred zone (SZ) were examined. In addition, effect of standard heat treatment on microstructure and mechanical properties in these zones was considered. A refined microstructure with an average grain size of ~ 0.6 m and a portion of high-angle grain boundaries (HAGBs) of ~0.67 was produced in sheets by ECAP followed by HR at 250°C. The microcrystalline grained structure with average grain size of ~2.3 mm was found in joint weld. The moderate mechanical properties were revealed in SMC sheets and joint welds. Heat treatment considerably increases strength of the base metal as well as the joint welds. The higher strength of the alloy after T6 temper is attributed to the dense precipitations of  dispersoids having plate-like shape which are uniformly distributed within aluminum matrix. It was observed that FSW can produce full strength weld both in the tempered and in the un-tempered conditions.

Effects of Thermo-Mechanical Process on the Microstructure and Mechanical Properties of Low Carbon HSLA Steels

2006 ◽  
Vol 15-17 ◽  
pp. 786-791 ◽  
Author(s):  
J.S. Kang ◽  
Y. Huang ◽  
C.W. Lee ◽  
Chan Gyung Park
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Cooling Rate ◽  
High Strength ◽  
Nucleation Site ◽  
Polygonal Ferrite ◽  
Low Alloy Steels ◽  
Low Carbon ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

Effects of deformation at austenite region and cooling rate on the microstructure and mechanical properties of low carbon (0.06 wt. % C) high strength low alloy steels have been investigated. Average grain size decreased and polygonal ferrite transformation promoted with increasing deformation amount at austenite region due to increase of ferrite nucleation site. Microstructure was also influenced by cooling rate resulting in the development of a mixture of fine polygonal ferrite and acicular ferrite at 10°C/s cooling rate. Discontinuous yielding occurred in highly deformed specimen due to the formation of polygonal ferrite. However, small grain size of highly deformed specimen caused lower ductile-to-brittle transition temperature than slightly deformed specimen.

Effect of Cooling Speed on the Microstructure and Mechanical Properties of Sn-0.7Cu-0.05Ni Solder Alloy

2018 ◽  
Vol 934 ◽  
pp. 73-78
Author(s):  
Phairote Sungkhaphaitoon
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Melting Point ◽  
Cooling Rate ◽  
Solder Alloy ◽  
Testing Machine ◽  
Solder Alloys ◽  
Scanning Calorimetry ◽  
Microstructure And Mechanical Properties ◽  
Cooling Speed

To study the effect of cooling speed on the microstructure and mechanical properties of Sn-0.7Cu-0.05Ni solder alloy, molten alloys were cooled at two different rates, using water-cooling and mold-cooling. The mechanical properties of the obtained alloys were analyzed with a universal testing machine (UTM) and by Vickers microhardness testing (HV). The microstructures were characterized using an optical microscope (OM) and energy dispersive X-ray spectroscopy (EDX).The melting point was ascertained by differential scanning calorimetry (DSC). The cooling rate of the water-cooled system (0.28 o C/s) was faster than the cooling rate of the mold-cooled system (0.05 °C/s). The grain size of the alloy produced by the faster cooling rate was finer than that of the alloy obtained from the slower cooling rate. This finer grain size gave the alloy superior ultimate tensile strength (UTS) and hardness but inferior ductility (%EL). The microstructure of both Sn-0.7Cu-0.05Ni solder alloys exhibited three phases of β-Sn, Cu6Sn5 and (Cu,Ni)6Sn5 intermetallic compounds. The melting point and undercooling of the solder alloys was 233.8 °C and 35.7 °C, respectively.

scholarly journals Microstructure and Properties of Ultrafine Cemented Carbides Prepared by Microwave Sintering of Nanocomposites

Crystals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 507
Author(s):  
Yanju Qian ◽  
Zhiwei Zhao
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Grain Size ◽  
Vickers Hardness ◽  
Sintering Temperature ◽  
Microwave Sintering ◽  
Raw Material ◽  
Cemented Carbides ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

Ultrafine cemented carbides were prepared by microwave sintering, using WC-V8C7-Cr3C2-Co nanocomposites as a raw material. The effects of sintering temperature and holding time on the microstructure and mechanical properties of cemented carbides were studied. The results show that the ultrafine cemented carbides prepared at 1300 °C for 60 min have good mechanical properties and a good microstructure. The relative density, Vickers hardness, and fracture toughness of the specimen reach the maximum values of 99.79%, 1842 kg/mm2 and 12.6 MPa·m1/2, respectively. Tungsten carbide (WC) grains are fine and uniformly distributed, with an average grain size of 300–500 nm. The combination of nanocomposites, secondary pressing, and microwave sintering can significantly reduce the sintering temperature and inhibit the growth of WC grains, thus producing superfine cemented carbides with good microstructure and mechanical properties.

scholarly journals Effect of ECAP on the Microstructure and Mechanical Properties of a Rolled Mg-2Y-0.6Nd-0.6Zr Magnesium Alloy

Crystals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 586 ◽  
Author(s):  
Shi ◽  
Li ◽  
Hu ◽  
Tan ◽  
Zhang ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Room Temperature ◽  
High Strength ◽  
Electron Backscattered Diffraction ◽  
Bar Rolling ◽  
Fine Grained ◽  
Angular Pressing ◽  
Microstructure And Mechanical Properties ◽  
Average Grain Size

A fine-grained Mg-2Y-0.6Nd-0.6Zr alloy was processed by bar-rolling and equal-channel angular pressing (ECAP). The effect of ECAP on the microstructure and mechanical properties of rolled Mg-2Y-0.6Nd-0.6Zr alloy was investigated by optical microscopy, scanning electron microscopy, electron backscattered diffraction and a room temperature tensile test. The results show that the Mg-2Y-0.6Nd-0.6Zr alloy obtained high strength and poor plasticity after rolling. As the number of ECAP passes increased, the grain size of the alloy gradually reduced and the texture of the basal plane gradually weakened. The ultimate tensile strength of the alloy first increased and then decreased, the yield strength gradually decreased, and the plasticity continuously increased. After four passes of ECAP, the average grain size decreased from 11.2 µm to 1.87 µm, and the alloy obtained excellent comprehensive mechanical properties. Its strength was slightly reduced compared to the as-rolled alloy, but the plasticity was greatly increased.

Microstructure and Mechanical Properties of Rheo-Extruded AZ31 Mg Alloy

2008 ◽  
Vol 141-143 ◽  
pp. 713-718 ◽  
Author(s):  
Jun Xu ◽  
Shao Ming Zhang ◽  
Bi Cheng Yang ◽  
Li Kai Shi ◽  
Z. Fan
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Hot Extrusion ◽  
Solid Particles ◽  
Microstructure And Mechanical Properties ◽  
Az31 Mg Alloy ◽  
Average Grain Size ◽  
Twin Screw ◽  
Inner Diameter ◽  
Screw Mechanism

A new rheo-extrusion technique has been developed to produce extruded profiles. The AZ31 slurry is fabricated by a twin-screw mechanism, and has spheroidal solid particles with a grain size of about 50 to 80μm. The slurry was introduced into an extrusion container with an inner diameter of 95mm, and then squeezed to a billet before extruding into a round bar with a diameter of 22mm using a 500kN extrusion machine. It is found that the new technique has a lower deformation resistance than that of the conventionally hot extrusion technique in the same extrusion velocity. The microstructure and mechanical properties of the rheo-extruded bars were examined in detail. The results illustrated that grains of the bar were very fine with the average grain size about 2.3μm，and the mechanical properties were improved substantially compared with those of the same alloy produced by the conventional hot extrusion.

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