Colloidal Process of Magnesia-Carbon Refractory and Its Sintering Characteristic

2007 ◽  
Vol 280-283 ◽  
pp. 1675-1678 ◽  
Author(s):  
Li Hua Xu ◽  
Zhi Fei Cheng ◽  
Fang Lian ◽  
Ti Zhuang Wang ◽  
Yun Yao
Keyword(s):  
High Performance ◽  
Ph Value ◽  
Compaction Pressure ◽  
Slip Casting ◽  
Metallurgical Industry ◽  
Green Density ◽  
Structural Ceramics ◽  
Dry Pressing ◽  
Excellent Thermal Property ◽  
Selection Of

Carbon-containing refractories are widely used in metallurgical industry due to their excellent thermal property and resistance to corrosion by molten iron. In the present work, slip casting colloidal process, which is used to fabricate high performance structural ceramics, has been introduced into the preparation for magnesia-carbon refractory with selection of suitable dispersant. The results indicated that the curve of zeta-potential of magnesia was similar with that of carbon just containing dispersant and the homogenized mixtures were attained under a controlling of low pH value. Three kinds of preparing routes for green bodies were designed, and all of the final densities and the resultant hardness of sintered bodies using colloidal process were superior to these of the specimen using conventional dry pressing, whereas its high green density can be plausibly observed in dry pressing body because of high compaction pressure used.

Preparation of Sialon from Solid Wastes by Colloidal Process

2007 ◽  
Vol 336-338 ◽  
pp. 1927-1929 ◽  
Author(s):  
Yun Yao ◽  
Li Hua Xu ◽  
Jin Qiu
Keyword(s):  
Fly Ash ◽  
Compaction Pressure ◽  
Slip Casting ◽  
Green Density ◽  
Sintering Process ◽  
Final Density ◽  
Dry Pressing ◽  
Pickling Process ◽  
Dispersant Additive ◽  
Properties Of Materials

Based on the slip casting and the preparation of sialon synthesized from clay, fly ash and gangue by the carbothermal reduction nitridation, the influences of compositions, dispersant additive and sintering process on the properties of materials have been investigated in present work. The experimental results indicate that disposal of fly ash via a pickling process can greatly reduce the content of iron, and the effect is obvious with increasing the concentrations of hydrochloric acid and pickling temperature. Therefore the component of the final product can be purified. It is also noted that the final density of the sintered body using colloidal process is superior to that of using conventional dry pressing, although the slightly higher green density is observed in dry pressing body because of high compaction pressure.

Study on Preparation and Property of Carbon Fiber/HA Composites by Centrifugal Slip Casting Method

2014 ◽  
Vol 1058 ◽  
pp. 180-184
Author(s):  
Qiang Li ◽  
Jing Yuan Yu ◽  
Xiu Juan Meng
Keyword(s):  
Fracture Toughness ◽  
Carbon Fiber ◽  
Carbon Fibers ◽  
Bending Strength ◽  
Slip Casting ◽  
Rheological Characteristic ◽  
Green Density ◽  
Aminobenzoic Acid ◽  
Casting Method ◽  
Dry Pressing

In this paper, centrifugal slip casting method was use to prepare carbon fiber/HA composites using the nanoHA particles and carbon fibers as initial materials. The morphology of the carbon fiber after modification of p-aminobenzoic acid was observed. The rheological characteristic of the carbon fibers/HA slurries was studied. The effects of the centrifugal acceleration on green density uniformity of carbon fiber/HA composites were analyzed. The bending strength and fracture toughness of carbon fiber/HA composites were measured. The results show the roughness of carbon fibers treated by p-aminobenzoic acid increases. At the pH of 10 and 5 wt% dispersant, the HA slurries with 3 vol% carbon fibers have good fluidity. After centrifuged at 2860 G for 30 min, the green compacts of HA composites have high and uniform the green density. After sintered at 1100°C for 1h, compared with carbon fiber/HA composites prepared by dry pressing, the modified carbon fiber/HA composites prepared by centrifugal slip casting have higher bending strength and fracture toughness of 89.4 MPa and 1.92MPa1/2, respectively.

Selection of Insulating Elastomers for High-Performance Intrinsically Stretchable Transistors

2021 ◽  
Author(s):  
Hang Ren ◽  
Junmo Zhang ◽  
Yanhong Tong ◽  
Mingxin Zhang ◽  
Xiaoli Zhao ◽  
...  
Keyword(s):  
High Performance ◽  
Selection Of

Realizing Stable High‐Performance and Low‐Energy‐Loss Ternary Photovoltaics through Judicious Selection of the Third Component

Solar RRL ◽  
2021 ◽  
pp. 2100450
Author(s):  
Bing-Huang Jiang ◽  
Yi-Peng Wang ◽  
Yu-Wei Su ◽  
Jia-Fu Chang ◽  
Chu-Chen Chueh ◽  
...  
Keyword(s):  
Energy Loss ◽  
High Performance ◽  
Low Energy ◽  
The Third ◽  
Selection Of

scholarly journals An Overview of Molecular Dynamic Simulation for Corrosion Inhibition of Ferrous Metals

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 46
Author(s):  
Nur Izzah Nabilah Haris ◽  
Shafreeza Sobri ◽  
Yus Aniza Yusof ◽  
Nur Kartinee Kassim
Keyword(s):  
Molecular Dynamic ◽  
Corrosion Inhibition ◽  
High Performance ◽  
Md Simulation ◽  
Ferrous Metal ◽  
Working Mechanism ◽  
Inhibitor Molecule ◽  
As Adsorption ◽  
Inhibition Studies ◽  
Selection Of

Molecular dynamics (MD) simulation is a powerful tool to study the molecular level working mechanism of corrosion inhibitors in mitigating corrosion. In the past decades, MD simulation has emerged as an instrument to investigate the interactions at the interface between the inhibitor molecule and the metal surface. Combined with experimental measurement, theoretical examination from MD simulation delivers useful information on the adsorption ability and orientation of the molecule on the surface. It relates the microscopic characteristics to the macroscopic properties which enables researchers to develop high performance inhibitors. Although there has been vast growth in the number of studies that use molecular dynamic evaluation, there is still lack of comprehensive review specifically for corrosion inhibition of organic inhibitors on ferrous metal in acidic solution. Much uncertainty still exists on the approaches and steps in performing MD simulation for corrosion system. This paper reviews the basic principle of MD simulation along with methods, selection of parameters, expected result such as adsorption energy, binding energy and inhibitor orientation, and recent publications in corrosion inhibition studies.

scholarly journals Bioactive Glass as a Nanoporous Drug Delivery System for Teicoplanin

2020 ◽  
Vol 10 (7) ◽  
pp. 2595 ◽  
Author(s):  
Chih-Ling Huang ◽  
Wei Fang ◽  
Bo-Rui Huang ◽  
Yan-Hsiung Wang ◽  
Guo-Chung Dong ◽  
...  
Keyword(s):  
Drug Delivery ◽  
Bioactive Glass ◽  
Drug Delivery System ◽  
Delivery System ◽  
Inductively Coupled Plasma ◽  
High Performance ◽  
Ph Value ◽  
Sol Gel ◽  
Phase Identification ◽  
Bet Analysis

Bioactive glass (BG) was made by the sol–gel method and doped with boron (B) to increase its bioactivity. Microstructures of BG and B-doped BG were observed by scanning electron microscopy, and phase identification was performed using an X-ray diffraction diffractometer. The ion concentrations released after soaking in simulated body fluid (SBF) for 1, 4, and 7 days were measured by inductively coupled plasma mass spectrometry, and the pH value of the SBF was measured after soaking samples to determine the variation in the environment. Brunauer–Emmett–Teller (BET) analysis was performed to further verify the characteristics of mesoporous structures. High performance liquid chromatography was used to evaluate the drug delivery ability of teicoplanin. Results demonstrated that B-doped BG performed significantly better than BG in parameters assessed by the BET analysis. B-doped BG has nanopores and more rough structures, which is advantageous for drug delivery as there are more porous structures available for drug adsorption. Moreover, B-doped BG was shown to be effective for keeping pH values stable and releasing B ions during soaking in SBF. The cumulative release of teicoplanin from BG and B-doped BG reached 20.09% and 3.17% on the first day, respectively. The drug release gradually slowed, reaching 29.43% and 4.83% after 7 days, respectively. The results demonstrate that the proposed bioactive glass has potential as a drug delivery system.

Mechanism of the Transition From In-Plane Buckling to Helical Buckling for a Stiff Nanowire on an Elastomeric Substrate

2016 ◽  
Vol 83 (4) ◽  
Author(s):  
Youlong Chen ◽  
Yong Zhu ◽  
Xi Chen ◽  
Yilun Liu
Keyword(s):  
High Performance ◽  
Three Dimensional ◽  
Stretchable Electronics ◽  
Buckling Mode ◽  
Design And Optimization ◽  
Out Of Plane ◽  
Plane Direction ◽  
Plane Displacement ◽  
Helical Buckling ◽  
Selection Of

In this work, the compressive buckling of a nanowire partially bonded to an elastomeric substrate is studied via finite-element method (FEM) simulations and experiments. The buckling profile of the nanowire can be divided into three regimes, i.e., the in-plane buckling, the disordered buckling in the out-of-plane direction, and the helical buckling, depending on the constraint density between the nanowire and the substrate. The selection of the buckling mode depends on the ratio d/h, where d is the distance between adjacent constraint points and h is the helical buckling spacing of a perfectly bonded nanowire. For d/h > 0.5, buckling is in-plane with wavelength λ = 2d. For 0.27 < d/h < 0.5, buckling is disordered with irregular out-of-plane displacement. While, for d/h < 0.27, buckling is helical and the buckling spacing gradually approaches to the theoretical value of a perfectly bonded nanowire. Generally, the in-plane buckling induces smaller strain in the nanowire, but consumes the largest space. Whereas the helical mode induces moderate strain in the nanowire, but takes the smallest space. The study may shed useful insights on the design and optimization of high-performance stretchable electronics and three-dimensional complex nanostructures.

The Formation of Plasma Acid at Atmospheric Pressure and its Application in Hydrolysis of Microcrystalline Cellulose

2013 ◽  
Vol 750-752 ◽  
pp. 1626-1629
Author(s):  
Bo Yuan ◽  
Ying Wang ◽  
Ying Chao Ji ◽  
Qiu Hong Wang
Keyword(s):  
Microcrystalline Cellulose ◽  
Atmospheric Pressure ◽  
High Performance ◽  
Barrier Discharge ◽  
Ph Value ◽  
Reducing Sugar ◽  
Dielectric Barrier ◽  
Integrated Optical ◽  
Hydrolysis Of ◽  
Single Factor Experiment

In this paper, plasma acid was obtained by treating distilled water with dielectric barrier discharge at atmospheric pressure in order to hydrolyze cellulose. The acidity of plasma acid was studied through a single factor experiment. A plasma acid with pH value of 1.42 was obtained and used to hydrolyze microcrystalline cellulose at 80°C for 60min. Under this condition, the integrated optical density (IOD) of the hydrolysis sample was 0.589. Based on standard glucose curve, the total reducing sugar (TRS) was calculated to be 53.75mg and the TRS yield was 53.75%. The filtrate was evaporated to get the solid hydrolysis sample to be analyzed by High-performance liquid chromatography (HPLC). The results showed that the sample mainly consisted of glucose, which proved that microcrystalline cellulose could be hydrolyzed by plasma acid. Therefore, it could be concluded that it was an environmentally friendly and economical method to hydrolyze the microcrystalline cellulose by plasma acid.

Synthesis and Application of Itaconic Acid Water-Coke Slurry Dispersant

2017 ◽  
Vol 896 ◽  
pp. 167-174 ◽  
Author(s):  
Zhi Yuan Yang ◽  
Zhuo Yue Meng ◽  
Zhi Hua Li ◽  
Si Tong Wang
Keyword(s):  
Surface Tension ◽  
Polyethylene Glycol ◽  
Itaconic Acid ◽  
High Performance ◽  
Ph Value ◽  
Raw Materials ◽  
Esterification Reaction ◽  
Solution Ph ◽  
Powder Surface ◽  
Coke Powder

Polyethylene glycol (PEG-200) and itaconic acid (IA) were used as raw materials to compound macromer through esterification reaction. A new type of specialized water-coke slurry dispersant was synthesized by copolymerization of microware, sodium methallyl sulfonate (SMAS) and maleic anhydride (MA). The experiment showed that the concentration of slurry could be reached to 63% with the dosage of 0.2%, and the apparent viscosity was 1140.3 mPa∙s. Through the analysis of the infrared, the dispersant was confirmed to have polyethylene glycol branched chain and hydrophilic functional groups such as carboxyl or sulfonic group. When the concentration of dispersant was 30 g/L, the surface tension of water could be decreased from 72.70 mN/m to 45.50 mN/m. Furthermore, when the solution pH value was 9, the Zeta potential of semi-coke powder surface could also be decreased from-13.38 mV to-25 mV with the addition of dispersant. Thus, this dispersant could increase electronegativity of semi-coke powder surface, enhance steric-hindrance effect and prevent the phenomenon of powder flocculation and gather. Meantime, it also could reinforce the semi-coke hydrophilic by reducing the surface tension of water effectively. And then, the high performance water-coke slurry could be obtained.

scholarly journals Regeneration and Reuse of Immunoaffinity Column for Highly Efficient Clean-Up and Economic Detection of Ochratoxin A in Malt and Ginger

Toxins ◽  
2018 ◽  
Vol 10 (11) ◽  
pp. 462 ◽  
Author(s):  
Xi Liu ◽  
Xiaofei Liu ◽  
Pinxuan Huang ◽  
Fang Wei ◽  
Guangyao Ying ◽  
...  
Keyword(s):  
Ochratoxin A ◽  
High Performance ◽  
Ph Value ◽  
Low Cost ◽  
Herbal Medicines ◽  
Preparation Procedure ◽  
Preservation Solution ◽  
Traditional Procedure ◽  
Sample Extraction ◽  
Sample Preparation Procedure

Immunoaffinity columns (IACs) are most popularly used for mycotoxin clean-up in complex matrices prior to chromatographic analysis. But, their high cost has limited their wide application and the regeneration of IACs for multiple instances of reuse is important. This study aimed to investigate the feasibility of regeneration and reuse of IACs for purification of ochratoxin A (OTA) in spiked raw malt and dried ginger samples followed by high performance liquid chromatography-fluorescence detection. After each use, the IACs were filled with phosphate buffer saline (PBS) as the preservation solution and stored at 8 °C overnight for regeneration and reuse until the recovery rate was <70%. The results showed that matrix type, preparation procedure, and pH value of sample extraction exhibited major effects on the reuse of IACs for OTA clean-up. While, after modifying the sample preparation procedure using water as the diluent and the solution at a pH of 7 to 8, the IACs could be used eight and three times for the spiked raw malt and dried ginger samples with OTA after regeneration. Regarding the traditional procedure recommended in Chinese Pharmacopoeia (2015 edition), the IACs could be used for three and two times for the spiked raw malt and dried ginger samples with OTA, respectively. Therefore, the corresponding experimental cost could be reduced to one-eighth and one-third of the original cost. This is the first study on the regeneration and reuse of IACs for OTA clean-up in complex Chinese herbal medicines, providing a green and economical tool for a large number of samples analysis with low cost.

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