Preparation and Thermal Properties of Pressureless Sintered AIN/SiC Composites

2015 ◽  
Vol 655 ◽  
pp. 78-81
Author(s):  
Shu He Ai ◽  
Yu Jun Zhang ◽  
Hong Yu Gong ◽  
Qi Song Li
Keyword(s):  
Thermal Conductivity ◽  
Mechanical Property ◽  
Thermal Properties ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Pressureless Sintering ◽  
Temperature Range ◽  
Sic Composites

AlN/SiC composites with 5 wt.% Y2O3addition were fabricated by pressureless sintering at 1700-1950 oC. The influences of sintering temperature and SiC content on the relative density, mechanical property and thermal conductivity were studied. With sintering temperature increasing from 1700 oC to 1750 oC, the relative density increased significantly to about 98.0%, without evident changes from 1750 oC to 1900 oC, and then decreased slightly at 1950 oC. As SiC content increased, the flexural strength of composites sintered at 1750 oC increased firstly, and then decreased, obtaining a maximum flexural strength of 337 MPa at 20 wt.% SiC content. Meanwhile, the thermal conductivity decreased from 60 W/(m∙K) to 40 W/(m∙K) with SiC content increasing from 0 wt.% to 30 wt.%. Moreover, in the sintering temperature range from 1750 oC to 1950 oC, the thermal conductivity increased from 45 W/(m∙K) to 55 W/(m∙K) for AlN-10 wt.% SiC composites, but decreased from 40 W/(m∙K) to 36 W/(m∙K) for AlN-30 wt.% SiC composites.

The Effect of Sintering Temperature to the Properties of Zinc Oxide

2013 ◽  
Vol 795 ◽  
pp. 419-423 ◽  
Author(s):  
J.H. Lim ◽  
C.K. Yeoh ◽  
Pei Leng Teh ◽  
W.M. Arif ◽  
A. Chik
Keyword(s):  
Thermal Conductivity ◽  
Zinc Oxide ◽  
Thermal Properties ◽  
Solid State ◽  
Sintering Temperature ◽  
Solid State Method ◽  
Influence Of Temperature ◽  
Temperature Range ◽  
Influence Of Temperature On ◽  
State Method

In this paper, different sintering temperature used to study the influence of temperature on the structural and thermal properties of zinc oxide (ZnO). On this research, the sample was prepared by solid-state method for zinc oxide (ZnO) at different sintering temperature which was 700°C, 800°C and 900°C. It was observed that the density of bulk ZnO that sintering at 900°C had the higher value of density 5.03 g/cm3. The microhardness of the bulk ZnO had a higher measurement 397.3 Hv after sintered at 900°C. ZnO that sintering at 900°C had been observed that had thermal conductivity 1.1611W/cm-K in the sintering temperature range 700°C to 900°C.

Preparation of 10B Enriched B4C Ceramics by Pressureless Sintering

2014 ◽  
Vol 602-603 ◽  
pp. 540-543
Author(s):  
Yu Jun Zhang ◽  
Sha Li Tan ◽  
Ru Bin Wei ◽  
Shu He Ai ◽  
Hai Bin Sun
Keyword(s):  
Flexural Strength ◽  
Boron Carbide ◽  
Relative Density ◽  
Sintering Temperature ◽  
Raw Material ◽  
Carbide Powder ◽  
Average Particle ◽  
Strength Increase ◽  
Pressureless Sintering ◽  
Water Reactors

Boron carbide is an attractive neutron absorbing material used both in Fast Breeder Reactors (FBR) and in Pressurised Water Reactors (PWR) owing to its very high absorption cross section for thermal neutrons, chemical stability and refractory character. In the present paper, 10B enriched B4C ceramics are prepared by pressureless sintering at 19602160°C, under argon, using 10B boron carbide powder as raw material, 18 wt% phenolic resin as sintering aid. In the sintering temperature range, with the increasing of sintering temperature, both the relative density and flexural strength increase linearly, the average particle sizes increase from about 3μm at 1960°C to more than 30μm at 2160°C. The sample sintered at 1960°C has a 91.7% of relative density and 192 MPa of flexural strength and a homogeneous texture with 3-4μm particle size, which are enough for pellet application of reactors.

scholarly journals Improvement of mechanical properties of HfB2-based composites by incorporating in situ SiC reinforcement through pressureless sintering

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
S. Ghadami ◽  
E. Taheri-Nassaj ◽  
H. R. Baharvandi ◽  
F. Ghadami
Keyword(s):  
Mechanical Properties ◽  
Thermal Conductivity ◽  
Relative Density ◽  
Pressureless Sintering ◽  
Sintering Process ◽  
Vacuum Atmosphere ◽  
Sic Reinforcement ◽  
Microstructural Studies ◽  
Composite Samples

AbstractHfB2, Si, and activated carbon powders were selected to fabricate 0–30 vol% SiC reinforced HfB2-based composite. Pressureless sintering process was performed at 2050 °C for 4 h under a vacuum atmosphere. Microstructural studies revealed that in situ SiC reinforcement was formed and distributed in the composite according to the following reaction: Si + C = SiC. A maximum relative density of 98% was measured for the 20 vol% SiC containing HfB2 composite. Mechanical investigations showed that the hardness and the fracture toughness of these composites were increased and reached up to 21.2 GPa for HfB2-30 vol% SiC and 4.9 MPa.m1/2 for HfB2-20 vol% SiC, respectively. Results showed that alpha-SiC reinforcements were created jagged, irregular, and elongated in shape which were in situ formed between HfB2 grains and filled the porosities. Formation of alpha-SiC contributed to improving the relative density and mechanical properties of the composite samples. By increasing SiC content, an enhanced trend of thermal conductivity was observed as well as a reduced trend for electrical conductivity.

Effect of Sintering Temperature on Microstructure and Mechanical Properties of Al2O3-TiC-ZrO2 Ceramic Composites

2012 ◽  
Vol 476-478 ◽  
pp. 1031-1035
Author(s):  
Wei Min Liu ◽  
Xing Ai ◽  
Jun Zhao ◽  
Yong Hui Zhou
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Ceramic Composites ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Al2O3-TiC-ZrO2ceramic composites (ATZ) were fabricated by hot-pressed sintering. The phases and microstructure of the composites were studied by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The relative density and mechanical properties (flexural strength, fracture toughness and Vicker’s hardness) of the composites were tested. The results show that the microstructure of the composites was the gray core-white rim. With the increase of sintering temperature, the relative density and mechanical properties of the composites increased first and then decreased. The composite sintered at 1705°C has the highest synthetical properties, and its relative density, flexural strength, fracture toughness and Vickers hardness are 98.3%,970MPa,6.0 MPa•m1/2and 20.5GPa, respectively.

The Study of Thermal Properties and Micro Structures of YSZ

2007 ◽  
Author(s):  
S. M. Guo ◽  
M. B. Silva ◽  
Patrick F. Mensah ◽  
Nalini Uppu
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Gas Turbine ◽  
Bond Coat ◽  
Sintering Temperature ◽  
Heating Process ◽  
Thermal Barrier ◽  
Inlet Temperature ◽  
Low Thermal Conductivity ◽  
Gas Tight

Thermal barrier coatings (TBCs) are used in gas turbine engines to achieve a better efficiency by allowing increased turbine inlet temperature and decreasing the amount of cooling air used. Plasma spraying is one of the most reliable methods to produce TBCs, which are generally comprised of a top coating of ceramic and a bond-coat of metal. Usually, the top coating is Yttria-Stabilized-Zirconia (YSZ), providing the thermal barrier effect. The bond-coat is typically a layer of M-Cr-Al-Y (where “M” stands for “metal”), employed to improve the attachment between the ceramic top-coat and the substrate. Due to the extreme temperature gradient presented in the plasma jet and the wide particle size distribution, during the coating process, injected ceramic powders may experience a significantly different heating process. Different heating history, coupled with the substrate preheating temperature, may affect the thermal properties of the YSZ layers. In this paper, four sets of mol 8% YSZ disks are fabricated under controlled temperatures of 1100°C, 1200°C, 1400°C and 1600°C. Subsequently the thermal properties and the microstructures of these YSZ disks are studied. The results indicate a strong microstructure change at a temperature slightly below 1400°C. For a high sintering temperature, a dense YSZ layer can be formed, which is good for gas tight operation; At low sintering temperature, say 1200°C, a porous YSZ layer is formed, which has the advantage of low thermal conductivity. For gas turbine TBC applications, a robust low thermal conductivity YSZ layer is desirable, while for Solid Oxide Fuel Cells, a gas-tight YSZ film must be formed. This study offers a general guideline on how to prepare YSZ layers, mainly by controlling the heating process, to form microstructures with desired properties.

scholarly journals Physical, mechanical and thermal properties of Crushed Sand Concrete containing Rubber Waste

2018 ◽  
Vol 149 ◽  
pp. 01076
Author(s):  
Guendouz Mohamed ◽  
Boukhelkhal Djamila
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Flexural Strength ◽  
Municipal Solid Waste ◽  
Solid Waste ◽  
Bulk Density ◽  
Mechanical And Thermal Properties ◽  
The Past ◽  
Rubber Waste ◽  
And Performance

Over the past twenty years, the rubber wastes are an important part of municipal solid waste. This work focuses on the recycling of rubber waste, specifically rubber waste of used shoes discharged into the nature and added in the mass of crushed sand concrete with percentage (10%, 20%, 30% and 40%). The physical (workability, fresh density), mechanical (compressive and flexural strength) and thermal (thermal conductivity) of different crushed sand concrete made are analyzed and compared to the respective controls. The use of rubber waste in crushed sand concrete contributes to reduce the bulk density and performance of sand concrete. Nevertheless, the use of rubber aggregate leads to a significant reduction in thermal conductivity, which improves the thermal insulation of crushed sand concrete.

scholarly journals Experimental investigations into mechanical and thermal properties of rapid manufactured copper parts

2019 ◽  
Vol 234 (1) ◽  
pp. 82-95 ◽  
Author(s):  
Gurminder Singh ◽  
Pulak M Pandey
Keyword(s):  
Thermal Conductivity ◽  
Tensile Strength ◽  
Thermal Properties ◽  
Ultimate Tensile Strength ◽  
Heating Rate ◽  
Sintering Temperature ◽  
Mechanical And Thermal Properties ◽  
Surface Porosity ◽  
Soaking Time ◽  
Ultrasonic Assisted

In the present paper, mechanical and thermal properties of rapidly manufactured copper parts were studied. The combination of three-dimensional printing and ultrasonic assisted pressureless sintering was used to fabricate copper parts. First, the ultimate tensile strength and thermal conductivity were compared between ultrasonic assisted and conventional pressureless sintered samples. The homogenously mixing of particles and local heat generation by ultrasonic vibrations promoted the sintering driving process and resulted in better mechanical and thermal properties. Furthermore, response surface methodology was adopted for the comprehensive study of the ultrasonic sintering parameters (sintering temperature, heating rate, and soaking time with ultrasonic vibrations) on ultimate tensile strength and thermal conductivity of the fabricated sample. Analysis of variance was performed to identify the significant factors and interactions. The image processing method was used to identify the surface porosity at different parameter levels to analyse the experimental results. High ultimate tensile strength was obtained at high sintering temperature, long soaking time, and slow heating rate with low surface porosity. After 60 min of soaking time, no significant effect was observed on the thermal conductivity of the fabricated sample. The significant interactions revealed less effect of soaking time at low sintering temperatures for ultimate tensile strength and less effect of heating rate at low sintering temperatures for thermal conductivity. Multi-objective optimization was carried out to identify parameters for maximum ultimate tensile strength and maximum thermal conductivity.

Thermal Expansion of SrZr4-xTix(PO4)6 Ceramics

2018 ◽  
Vol 281 ◽  
pp. 169-174
Author(s):  
Yang Wang ◽  
Yuan Yuan Song ◽  
Yuan Yuan Zhou ◽  
Lu Ping Yang ◽  
Fu Tian Liu
Keyword(s):  
Thermal Expansion ◽  
Relative Density ◽  
Thermophysical Properties ◽  
Sintering Temperature ◽  
Temperature Range ◽  
Thermal Expansion Coefficients ◽  
High Relative Density ◽  
Low Thermal Expansion ◽  
Expansion Coefficients

Low thermal expansion ceramics have been widely applied in multiple fields. In this paper, a series of low thermal expansion ceramics SrZr4-xTix(PO4)6 was prepared and characterized. The SrZr4-xTix(PO4)6 ceramics could be well sintered in the temperature range of 1400~1500 °C. The effect of the addition of Ti substituting Zr and the sintering temperature was studied. The Ceramic with x =0.1 sintered at 1450 °C, the SrZr4-xTix(PO4)6 had a high relative density. The thermal expansion coefficients were about 3.301×10-6 °C-1. It was demonstrated that the microstructure of the SrZr4-xTix(PO4)6 could be altered by adding varying amount of Ti to tailor the thermophysical properties of the material.

Effect of Y2O3 on the Sintering, Mechanical and Dielectric Properties of Mullite/h-BN Composites

2016 ◽  
Vol 848 ◽  
pp. 28-31
Author(s):  
Han Jin ◽  
Yong Feng Li ◽  
Zhong Qi Shi ◽  
Hong Yan Xia ◽  
Guan Jun Qiao
Keyword(s):  
Fracture Toughness ◽  
Dielectric Constant ◽  
Phase Composition ◽  
High Temperature ◽  
Dielectric Properties ◽  
Liquid Phase ◽  
Flexural Strength ◽  
Sintering Temperature ◽  
Pressureless Sintering ◽  
Different Temperatures

Mullite/10 wt. %h-BN composites with 5 wt. % Y2O3 additive were fabricated by pressureless sintering at different temperatures. The densification, phase composition, microstructure, mechanical and dielectric properties of the mullite/h-BN composites were investigated. With the addition of Y2O3, the sintering temperature of the mullite/h-BN composites declined, while the density, mechanical and dielectric properties all increased. The addition of Y2O3 promoted the formation of liquid phase at high temperature, which accelerated the densification. Besides, Y2O3 particles which were located at the grain boundaries inhibited the grain growth of mullite matrix. For the mullite/h-BN composites with Y2O3 additive, the appropriate sintering temperature was about 1600°C. The relative density, flexural strength, fracture toughness and dielectric constant of the Y2O3 doped mullite/h-BN composite sintered at 1600 °C reached 82%, 135 MPa, 2.3 MPa·m1/2 and 4.9, respectively.

Effect of Iron Additive on the Sintering Behavior of Hot-Pressed ZrC-W Composites

2008 ◽  
Vol 368-372 ◽  
pp. 1764-1766 ◽  
Author(s):  
Yu Jin Wang ◽  
Lei Chen ◽  
Tai Quan Zhang ◽  
Yu Zhou
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Sintering Behavior ◽  
Hot Press ◽  
Sintering Additive ◽  
Microstructure And Mechanical Properties ◽  
Hot Press Sintering

The ZrC-W composites with iron as sintering additive were fabricated by hot-press sintering. The densification, microstructure and mechanical properties of the composites were investigated. The incorporation of Fe beneficially promotes the densification of ZrC-W composites. The relative density of the composite sintered at 1900°C can attain 95.3%. W2C phase is also found in the ZrC-W composite sintered at 1700°C. The content of W2C decreases with the increase of sintering temperature. However, W2C phase is not identified in the composite sintered at 1900°C. The flexural strength and fracture toughness of the composites are strongly dependent on sintering temperature. The flexural strength and fracture toughness of ZrC-W composite sintered at optimized temperature of 1800°C are 438 MPa and 3.99 MPa·m1/2, respectively.

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