Improvement in Mechanical Performance of Biomaterial Ti Alloy by Controlling Volume Fraction of Martensite Phase

2021 ◽  
Vol 1016 ◽  
pp. 18-23
Author(s):  
Toshikazu Akahori ◽  
Shota Ino ◽  
Tomokazu Hattori

Recently, biomaterial α + β type Ti alloys with relatively low Young’s modulus and high specific strength have been widely used all over the world. Martensite (M) phase in α + β type Ti alloy has been reported to improve the toughness and ductility, therefore, there is high possibility of improvement in the mechanical properties easily by controlling the volume fraction of M phase. In this study, the change in mechanical properties of α + β type Ti-6Al-7Nb (Ti67) with various volume fractions of M phase were systematically investigated through the various heat treatments and thermo-mechanical treatments. Microstructures of Ti67 subjected to ST at 1173 K to 1273 K below the temperature of β transus were composed of martensite and primary α phases. The volume fraction of M phase increased with an increase in ST temperature. Tensile strength increased simply with an increase in the volume fraction of M phase, while the elongation, reduction of area and Young’s modulus showed a reverse trend. Fatigue limit of Ti67 subjected to ST at 1243K showed the highest value of 880 MPa.

Author(s):  
Matheus de Mendonça Chitan ◽  
Katia Cristiane Gandolpho Candioto

Abstract Abrasive tools consist of abrasive grains, binder and pores. Binders are the matrix of the material and may be of the metallic, vitrified or resin type. The wide use of polymeric materials (resinoid) is due to their low cost and excellent mechanical properties. The grain has the function of roughing the material, the binder, on the other hand, has the characteristics of ensuring grain adhesion and the pores in the structure are responsible for cooling the abrasive tool. In this work, we report the preparation and evaluation of the mechanical characteristics of resin bond composite abrasives with different structures based on the porous concentration. The composite abrasives were made with phenolic resin and alumina grains. Four different structures were studied from 10 to 30% of porous volume fraction with 50% of grain volume fraction. The concentration of porous and bond in the structure composition were employed to compare the mechanical performance of the prepared composite abrasive. To evaluate the mechanical properties of composites, Impact strength, Young’s Modulus by impulse excitation and flexural strength were realized. It was observed that as the porosity is higher, the impact resistance (absorbed energy) is lower, which confirms the lower resistance produced by the surface area contact (grain/binder) and a greater accumulation of tension in the binder material, the higher porosity value, higher the flexural strength value until 20% of porosity. Samples with higher volumes level of porosity presented lower Young’s Modulus but the presence of pores produced by volatiles by-products (mainly water) should act as stress concentrators, thus favoring lower mechanical properties at the resin-grain interface.


2021 ◽  
Vol 21 (2) ◽  
pp. 7-11
Author(s):  
Ahmed Mansoor Abbood ◽  
Haider K. Mehbes ◽  
Abdulkareem. F. Hasan

In this study, glass-filled epoxy functionally graded material (FGM) was prepared by adopting the hand lay-up method. The vertical gravity casting was used to produce a continuous variation in elastic properties. A 30 % volume fraction of glass ingredients that have mean diameter 90 μm was spread in epoxy resin (ρ = 1050 kg/m3). The mechanical properties of FGM were evaluated according to ASTM D638. Experimental results showed that a gradually relationship between Young’s modulus and volume fraction of glass particles, where the value of Young’s modulus at high concentration of glass particles was greater than that at low concentration, while the value of Poisson’s ratio at high concentration of glass particles was lower than that at low concentration. The manufacture of this FG beam is particularly important and useful in order to benefit from it in the field of various fracture tests under dynamic or cyclic loads.


2011 ◽  
Vol 146 ◽  
pp. 12-26 ◽  
Author(s):  
A. Gherissi ◽  
R.Ben Cheikh ◽  
E. Dévaux ◽  
Fethi Abbassi

In this study, we present the manufacturing process of two new composites materials in the form of long fibers of polylactic-acid (PLA) or polypropylene (PP), reinforced by cellulose whiskers micro-fibers loads. In order to evaluate the mechanical properties of these advanced materials, a several uniaxial tensile tests were carried out. The PP and the PLA have initially been spinning without the addition of cellulose whiskers micro-fibers. In order to study the effects of cellulose whiskers micro-fibers reinforcements in the Mechanical behavior of the PLA and PP filaments, we determinate the proprieties of these advanced material from the tensile results. For the PP composite filaments material case, the whiskers reinforcement increases Young's modulus and failure resistance, but it reduces the limit strength failure. For the PLA composites the addition of 1% wt of cellulose whiskers from the total volume fraction of the material, increase the Young’s modulus more than 50% and a decrease of the failure resistance and the limit strength of composite. The obtained composites fibers are very rigid and brittle. What follows, that the addition of cellulose whiskers micro fibers in PP matrix, provides mechanical properties more convenient compared to the PLA matrix.


2019 ◽  
Vol 25 (10) ◽  
pp. 1661-1683 ◽  
Author(s):  
Rafael Quelho de Macedo ◽  
Rafael Thiago Luiz Ferreira ◽  
Kuzhichalil Jayachandran

Purpose This paper aims to present experimental and numerical analyses of fused filament fabrication (FFF) printed parts and show how mechanical characteristics of printed ABS-MG94 (acrylonitrile butadiene styrene) are influenced by the void volume fraction, cooling rate and residual thermal stresses. Design/methodology/approach Printed specimens were experimentally tested to evaluate the mechanical properties for different printing speeds, and micrographs were taken. A thermo-mechanical finite element model, able to simulate the FFF process, was developed to calculate the temperature fields in time, cooling rate and residual thermal stresses. Finally, the experimental mechanical properties and the microstructure distribution could be explained by the temperature fields in time, cooling rate and residual thermal stresses. Findings Micrographs revealed the increase of void volume fraction with the printing speed. The variations on voids were associated to the temperature fields in time: when the temperatures remained high for longer periods, less voids were generated. The Young's Modulus of the deposited filament varied according to the cooling rate: it decreased when the cooling rate increased. The influence of the residual thermal stresses and void volume fraction on the printed parts failure was also investigated: in the worst scenarios evaluated, the void volume fraction reduced the strength in 9 per cent, while the residual thermal stresses reduced it in 3.8 per cent. Originality/value This work explains how the temperature fields can affect the void volume fraction, Young's Modulus and failure of printed parts. Experimental and numerical results are shown. The presented research can be used to choose printing parameters to achieve desired mechanical properties of FFF printed parts.


2010 ◽  
Vol 654-656 ◽  
pp. 2220-2224 ◽  
Author(s):  
Takuya Ishimoto ◽  
Takayoshi Nakano

To evaluate the material parameters of regenerated bone, it is important to clarify the mechanical performance of the regenerated portion. In general, the shape and size of regenerated bone tissue is heterogeneous. It is often difficult to elucidate material properties by means of conventional mechanical tests such as compressive and/or tensile tests and bending tests. The nanoindentation technique has been utilized to evaluate the material properties of small or microstructured materials because they do not necessarily require a large well-designed specimen. Thus, this technique may be useful for the evaluation of the material properties of regenerated bone tissue. In this study, this technique was applied for the assessment of the Young’s modulus and hardness of regenerated and intact long bones of a rabbit. The regenerated bone exhibited a significantly lower Young’s modulus and hardness than the intact bone. The regenerated long bone also exhibited impaired mechanical properties, which may have been caused by the difference in the nano-organization of its collagen fibers and mineral crystals (the main components of bone tissue), from that of the intact bone.


2012 ◽  
Vol 472-475 ◽  
pp. 1813-1817 ◽  
Author(s):  
Yu Lin Yang ◽  
Zhe Yong Fan ◽  
Ning Wei ◽  
Yong Ping Zheng

In this paper the mechanical properties of a series of hydrogen functionalized graphyne are investigated through acting tensile loads on the monolayer networks. Molecular dynamics simulations are performed to calculate the fracture strains and corresponding maximum forces for pristine graphyne along both armchair and zigzag directions. Furthermore, hydrogen functionalized graphynes with different functionalization sites are analyzed to investigate the effect of functionlization on the mechanical performance. Finally, Young's modulus of all the investigated architectures are computed. The obtained results show that monolayer graphyne is mechanically stable with high strength and stiffness, and the mechanical performance can be tuned through structure engineering and functionalization.


2006 ◽  
Vol 317-318 ◽  
pp. 305-308 ◽  
Author(s):  
Rak Joo Sung ◽  
Takafumi Kusunose ◽  
Tadachika Nakayama ◽  
Yoon Ho Kim ◽  
Tohru Sekino ◽  
...  

A novel transparent polycrystalline silicon nitride was fabricated by hot-press sintering with MgO and AlN as additives. The mixed powder with 3 wt.% MgO and 9 wt.% AlN was sintered at 1900oC for 1 hour under 30 MPa pressure in a nitrogen gas atmosphere. Transparent polycrystalline silicon nitride was successfully fabricated. The mechanical properties such as density, hardness, young’s modulus, fracture strength and fracture toughness were evaluated. The effect of α/β phase on the mechanical properties of transparent polycrystalline silicon nitride was investigated. The properties were changed depending on the amount of α/β phase. The hardness and Young's modulus increased with increasing the volume fraction of α-phase fraction as a reflection of the higher hardness of α-phase Si3N4. The fracture toughness and fracture strength decreased with decreasing the volume fraction of β-phase Si3N4.


2015 ◽  
Vol 1760 ◽  
Author(s):  
Joung Wook Kim ◽  
Kyosuke Yoshimi ◽  
Hirokazu Katsui ◽  
Takashi Goto

ABSTRACTThe effect of Ti addition on the density and microstructure development of MoSiBTiC alloy was investigated. Two kinds of MoSiBTiC alloys with the composition of Mo-5Si-10B-10Ti-10C (10Ti alloy) and Mo-5Si-10B-15Ti-10C (15Ti alloy) (at. %) were prepared by conventional arc-melting. The primary phase of as-cast 10Ti and 15Ti alloys was (Ti,Mo)C, and there were two eutectic phases of Moss + (Ti,Mo)C and Moss + T2 + (Ti,Mo)C in the alloys. In addition, 10Ti alloy had a Moss + T2 + (Mo,Ti)2C eutectic. There was no Moss + T2 + (Mo,Ti)2C eutectic in the 15Ti alloy, and thus it is apparent that the (Mo,Ti)2C formation was suppressed by 5 at. % Ti addition. The volume fraction of (Ti,Mo)C increased and thus the density reduced from 8.78 to 8.43 g/cm3 with the Ti addition. In all constituent phases, Ti concentration increased while Mo concentration decreased. In spite of the changes, hardness, Young’s modulus and shear modulus were hardly changed. Therefore, Ti addition seems to be effective to further lower the density without deteriorating mechanical properties of the MoSiBTiC alloy.


Metals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 1175
Author(s):  
Pavel A. Somov ◽  
Eugene S. Statnik ◽  
Yuliya V. Malakhova ◽  
Kirill V. Nyaza ◽  
Alexey I. Salimon ◽  
...  

Recent years witnessed progressive broadening of the practical use of 3D-printed aluminium alloy parts, in particular for specific aerospace applications where weight saving is of great importance. Selective laser melting (SLM) is an intrinsically multi-parametric fabrication technology that offers multiple means of controlling mechanical properties (elastic moduli, yield strength, and ductility) through the control over grains size, shape, and orientation. Targeted control over mechanical properties is achieved through the tuning of 3D-printing parameters and may even obviate the need of heat treatment or mechanical post-processing. Systematic studies of grain structure for different printing orientations with the help of EBSD techniques in combination with mechanical testing at different dimensional levels are the necessary first steps to implement this agenda. Samples of 3D-printable Al-Mg-Si RS-333 alloy were fabricated in three orientations with respect to the principal build direction and the fast laser beam scanning direction. Sample structure and proper-ties were investigated using a number of techniques, including EBSD, in situ SEM tensile testing, roughness measurements, and nanoindentation. The as-printed samples were found to display strong variation in Young’s modulus values from nanoindentation (from 43 to 66 GPa) and tensile tests (from 54 to 75 GPa), yield stress and ultimate tensile strength (100–195 and 130–220 MPa) in different printing orientations, and almost constant hardness of about 0.8 GPa. A further preliminary study was conducted to assess the effect of surface finishing on the mechanical performance. Surface polishing was seen to reduce Young’s modulus and yield strength but improves ductility, whereas the influence of sandblasting was found to be more controversial. The experimental results are discussed in connection with the grain morphology and orientation.


2005 ◽  
Vol 502 ◽  
pp. 201-204 ◽  
Author(s):  
Tsunemichi Imai ◽  
Shang Li Dong ◽  
Ichinori Shigematsu ◽  
Naobumi Saito ◽  
Kazutaka Suzuki ◽  
...  

The XN-05C/2017, XN-05C/MESO-10 and BGC152/MESO-10 aluminum composites reinforced by low young’s modulus amorphous carbon fiber and particle, respectively, were fabricated by a PM route followed by hot extrusion and rolling in this study. The mechanical properties of the prepared composites were investigated subsequently. The XN-05C/2017 and XN-05C/MESO-10 were found to exhibit low elastic modulus of 50~60GPa within the fiber volume fraction of 0.10~0.15, while the BGC152/MESO-10 shows a data of 50GPa with a particle volume fraction of 0.10. The tensile strength of XN-05C/MESO-10 was evaluated to be 400~600MPa in the case of Vf=0.10~0.15, and become to decease with increasing fiber volume fraction. Damping application would be a potential consideration for the amorphous carbon fiber reinforced aluminum composites.


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