Fabrication and Mechanical Properties of Glass Fiber/Epoxy Nanocomposites

2006 ◽  
Vol 505-507 ◽  
pp. 37-42 ◽  
Author(s):  
Jia Lin Tsai ◽  
Jui Ching Kuo ◽  
Shin Ming Hsu

This research is aimed to fabricate glass fiber/epoxy nanocomposites containing organoclay as well as to understand the organoclay effect on the in-plane shear strength of the nanocomposites. To demonstrate the organoclay effect, three different loadings of organoclay, were dispersed in the epoxy resin using mechanical mixer followed by sonication. The corresponding glass/epoxy nanocomposites were prepared by impregnating the organoclay epoxy mixture into the dry glass fiber through a vacuum hand lay-up process. Off-axis block glass/epoxy nanocomposites were tested in compression to produce in-plane shear failure. It is noted only the specimens showing in-plane shear failure mode were concerned in this study. Through coordinate transformation law, the uniaxial failure stresses were then converted to a plot of shear stress versus transverse normal stress from which the in-plane shear strength was obtained. Experimental results showed that the fiber/epoxy nanocomposite exhibit higher in-plane shear strength than the conventional composites. This increased property could be ascribed to the enhanced fiber/matrix adhesion promoted by the organoclay.

2007 ◽  
Vol 334-335 ◽  
pp. 773-776 ◽  
Author(s):  
Jia Lin Tsai ◽  
Ming Dao Wu

This research focuses on the fabrication of glass fiber/epoxy organoclay nanocomposites as well as on the investigation of organoclay effect on transverse tensile strength and in-plane shear strength of the nanocomposites. To demonstrate the organoclay effect, three different loadings of organoclay were dispersed respectively in the epoxy resin using a mechanical mixer followed by sonication. The corresponding glass/epoxy nanocomposites were produced by impregnating dry glass fiber with organoclay epoxy compound via a vacuum hand lay-up procedure. For evaluating transverse tensile strengths, the unidirectional coupon specimens were prepared and tested in the transverse direction. Results indicate that with the increment of organoclay loadings, the glass/epoxy nanocomposites demonstrate higher transverse tensile strength. On the other hand, the in-plane shear strengths were measured from [± 45]s laminates. It is revealed that when the organoclay loadings increase, the in-plane shear strength of glass/epoxy nanocomposites also increases appropriately. Scanning Electron Microscopy (SEM) observations on the failure surfaces indicate that the increasing characteristics in transverse and in-plane failure stresses may be ascribed to the enhanced fiber/matrix bonding modified by the organoclay.


2018 ◽  
Vol 2018 ◽  
pp. 1-12
Author(s):  
Fei Wang ◽  
Ping Cao ◽  
Yu Chen ◽  
Qing-peng Gao ◽  
Zhu Wang

In order to investigate the influence of the joint on the failure mode, peak shear strength, and shear stress-strain curve of rock mass, the compression shear test loading on the parallel jointed specimens was carried out, and the acoustic emission system was used to monitor the loading process. The joint spacing and joint overlap were varied to alter the relative positions of parallel joints in geometry. Under compression-shear loading, the failure mode of the joint specimen can be classified into four types: coplanar shear failure, shear failure along the joint plane, shear failure along the shear stress plane, and similar integrity shear failure. The joint dip angle has a decisive effect on the failure mode of the specimen. The joint overlap affects the crack development of the specimen but does not change the failure mode of the specimen. The joint spacing can change the failure mode of the specimen. The shear strength of the specimen firstly increases and then decreases with the increase of the dip angle and reaches the maximum at 45°. The shear strength decreases with the increase of the joint overlap and increases with the increase of the joint spacing. The shear stress-displacement curves of different joint inclination samples have differences which mainly reflect in the postrupture stage. From monitoring results of the AE system, the variation regular of the AE count corresponds to the failure mode, and the peak value of the AE count decreases with the increase of joint overlap and increases with the increase of joint spacing.


2018 ◽  
Vol 2018 ◽  
pp. 1-10
Author(s):  
Daniel Bohling ◽  
Andrzej Cwirzen ◽  
Karin Habermehl-Cwirzen

Full utilization of mechanical properties of glass fiber fabric-reinforced cement composites is very limited due to a low bond strength between fibers and the binder matrix. An experimental setup was developed and evaluated to correlate the mortar penetration depth with several key parameters. The studied parameters included fresh mortar properties, compressive and flexural strengths of mortar, the fabric/mortar bond strength, fabric pullout strength, and a single-lap shear strength. Results showed that an average penetration of mortar did not exceed 100 µm even at a higher water-to-binder ratio. The maximum particle size of the used fillers should be below an average spacing of single glass fibers, which in this case was less than 20 µm to avoid the sieving effect, preventing effective penetration. The pullout strength was strongly affected by the penetration depth, while the single-lap shear strength was also additionally affected by the mechanical properties of the mortar.


2016 ◽  
Vol 83 (6) ◽  
Author(s):  
Youming Chen ◽  
Raj Das ◽  
Mark Battley

Study on the response of honeycombs subjected to in-plane shear helps establish the constitutive relations for honeycombs and shed light on the mechanics of cellular materials. The present study explores the nonlinear elastic response of honeycombs under in-plane shear by analyzing the large deflection of cell walls in a unit cell. Governing equations are established which relate the macroscopic response of honeycombs to the deflection of cell walls. Solving these equations, the behavior of regular honeycombs under in-plane shear along horizontal (X) and vertical (Y) directions was investigated. It is found that the response of regular honeycombs under in-plane shear depends on the nondimensional shear stress which is a parameter combining the thickness-to-length ratio of cell walls, the Young's modulus of base materials, and macroscopic shear stress. Lateral shrinking is a distinctive characteristic for honeycombs under in-plane shear, which should be taken into account when establishing constitutive relations and performing simple shear experiments. Expressions for predicting the shear strength of honeycombs are formulated in this paper. It is noted that the normalized shear strength of regular honeycombs depends on two ratios: the thickness-to-length ratio of cell walls and the ratio of Young's modulus to yield strength of base materials, and the former has a dominant effect. By comparing honeycombs with cell walls of uniform thickness against honeycombs with vertical cell walls of double thickness, it is found that doubling the thickness of vertical cell walls of honeycombs increases their shear strength along horizontal (X) direction nearly twice, but does not improve the shear strength that much along the vertical (Y) direction.


2017 ◽  
Vol 37 (3) ◽  
pp. 247-259
Author(s):  
John Olusanya ◽  
Krishnan Kanny ◽  
Shalini Singh

Abstract The correlation between cure properties and structure of nanoclay filled composite laminate has not been studied extensively. Most of the cure studies were preferably done using small samples through a calorimetric method. In this study, the effect of varying weight ratio of nanoclay (1–5 wt%) on bulk cure properties of epoxy glass fiber reinforced composite (GFRC) laminates was studied. Bulk cure of unfilled and clay filled GFRC laminates was determined using the dynamic mechanical analysis-reheat method (DMA-RM). DMA-RM cure properties gave a better coordinate method, with better cure efficiency achieved in clay filled GFRC laminates when compared to unfilled GFRC laminates. The correlation between nanoclay and DMA-RM degree of cure was coordinated with compressive and in-plane shear strength properties. The degree of cure value of 78% by DMA-RM at 1 wt% clay filled GFRC corresponds with the compressive modulus and in-plane shear strength highest values, which are 20% and 14% increase, respectively, also at 1 wt% clay filled GFRC. The structures of the unfilled and clay filled epoxy were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Clay filled epoxy up to 3 wt% showed no distinct diffraction peak, which suggested that nanoclay is randomly dispersed in the matrix.


Polymers ◽  
2019 ◽  
Vol 11 (7) ◽  
pp. 1116 ◽  
Author(s):  
Maoyuan Li ◽  
Peng Chen ◽  
Bing Zheng ◽  
Tianzhengxiong Deng ◽  
Yun Zhang ◽  
...  

Due to its superior mechanical properties, graphene (Gr) has the potential to achieve high performance polymer-based nanocomposites. Previous studies have proved that defects in the Gr sheets could greatly reduce the mechanical properties of Gr, while the Stone-Wales (SW) defect was found to enhance the interfacial mechanical strength between Gr and epoxy. However, the combined effects of defects on the overall mechanical properties of Gr/epoxy nanocomposites have not been well understood. In this paper, the effect of the SW defect on the mechanical properties of Gr/epoxy nanocomposites was systematically investigated by using molecular dynamic simulations. The simulation results showed that the SW defect would degrade the mechanical properties of nanocomposites, including the Young’s modulus and in-plane shear modulus. Surprisingly, the transverse shear modulus could be remarkably enhanced with the existence of SW. The reinforcing mechanisms were mainly due to two aspects: (1) the SW defect could increase the surface roughness of the Gr, preventing the slippage between Gr and epoxy during the transverse shea; and (2) the nanocomposite with defective Gr enables a higher interaction energy than that with perfect graphene. Additionally, the effects of temperature, the dispersion and volume fraction of Gr were also investigated.


2020 ◽  
pp. 152808372096073
Author(s):  
Marwa A Abd El-baky ◽  
Mohamed A Attia

In this study, the effect of different weight percentages (wt. %) of halloysite nanotubes (HNTs) on the mechanical performance of glass laminate aluminum (Al) reinforced epoxy (GLARE) was investigated. GLARE (3/2) laminates with quasi-isotropic lay-up, [Al/[(0°/90°)/(45°/−45°)]s/Al/[(0°/90°)/(45°/−45°)]s/Al] filled with 0, 0.25, 0.5, 1, 2 and 3 wt. % of HNTs were fabricated using hand lay-up followed by compression molding. To explore the effect of HNTs on the mechanical properties, tensile, flexural, in-plane shear, interlaminar shear, bearing and impact tests were conducted. Results demonstrated that the inclusion of 1 wt. % of HNTs into GLARE leads to maximum improvements of 35.67, 8.50, 28.85, 50.47, 50.27, 30.43, 23.73, 72.08, 30.74, and 51.52% in tensile strength, tensile strain, Young's modulus, modulus of toughness, flexural strength, flexural strain, in-plane shear strength, interlaminar shear strength, bearing strength, and impact strength, respectively, compared to pristine GLARE. An enhancement of 38.89% in the flexural modulus was attained by adding 0.5 wt. % of HNTs to GLARE compared to pristine GLARE. The tensile strength, tensile strain, modulus of toughness, flexural strength, flexural modulus, flexural strain, in-plane shear strength, and interlaminar shear strength of GLARE filled with 3 wt. % of HNTs are 0.91, 0.88, 0.91, 0.91, 0.71, 0.83, 0.85, and 0.91 times those of the original GLARE. But Young’s modulus, bearing strength, and impact strength are 1.10, 1.15 and 1.20 times those of the original GLARE. To investigate the fracture mechanism, field emission scanning electron microscope (FE-SEM) and energy-dispersive X-ray spectroscopy (EDX) were used. The microscopic images revealed that adding HNTs lead to the improvement in the interaction between the epoxy matrix and glass fiber, thereby improving the mechanical properties.


2020 ◽  
Vol 12 (3) ◽  
pp. 1255 ◽  
Author(s):  
Liang Chen ◽  
Xianbiao Mao ◽  
Peng Wu

Comprehensive understanding of the effects of temperature and inclination angle on mechanical properties and fracture modes of rock is essential for the design of rock engineering under complex loads, such as the construction of nuclear waste repository, geothermal energy development and stability assessment of deep pillar. In this paper, a novel inclined uniaxial compression (inclined UCS) test system was introduced to carry out two series of inclined uniaxial compression tests on granite specimens under various inclination angles (0–20°) and treated temperatures (25–800 °C) at 5° inclination. Experimental results revealed that the peak compression stress and elastic modulus gradually decreased, while peak shear stress increased nonlinearly with the increasing inclination angle; the peak compression and shear stress as well as elastic modulus slightly increased from 25 to 200 °C, then gradually decreased onwards with the increasing temperature. The effect of temperature on peak axial strain was the same as that on peak shear displacement. Acoustic emission (AE) results suggested that the relationship between crack initiation stress, inclination angle and treated temperature followed a similar trend as that of the peak compression stress and elastic modulus. Particularly, the crack initiation (CI) stress threshold and shear stress corresponding to CI threshold under 800 °C were only 7.4% of that under 200 °C and revealed a severe heat damage phenomenon, which was consistent with the results of the scanning electron microscopy (SEM) with the appearance of a large number of thermal pores observed only under 800 °C. The failure modes tended to shear failure with the increasing inclination angle, indicating that the shear stress component can accelerate sliding instability of rocks. On the other hand, the failure patterns with different temperatures changed from combined splitting-shear failure (25–400 °C) to single shear failure (600 and 800 °C). The study results can provide an extremely important reference for underground thermal engineering construction under complex loading environment.


Sign in / Sign up

Export Citation Format

Share Document