Comparison of Grain Structures and Textures in AA5754 Aluminum Alloy Sheets Processed by Room Temperature Rolling and Rolling with Liquid Nitrogen

2007 ◽  
Vol 558-559 ◽  
pp. 217-222 ◽  
Author(s):  
Hai Ou Jin ◽  
Pei Dong Wu ◽  
David J. Lloyd
Keyword(s):  
Liquid Nitrogen ◽  
Room Temperature ◽  
Electron Backscatter Diffraction ◽  
Optical Microscope ◽  
Grain Structure ◽  
Micro Hardness ◽  
Grain Structures ◽  
Room Temperature Rolling ◽  
The One ◽  
Backscatter Diffraction

Two AA5754 sheets have been processed by cold rolling with 83% thickness reduction, one at room temperature and another with liquid nitrogen as coolant. The sheets were subsequently annealed at 220-275°C for 1 hour. The development of grain structure and texture was studied by optical microscope, scanning electron microscopy (SEM), X-ray diffraction and electron backscatter diffraction (EBSD) in SEM, and the mechanical property by micro-hardness testing. It has been demonstrated that the as-rolled sheets have the same micro-hardness, but the grain structures and textures are very different. Compared to the sheet processed with liquid nitrogen, the one rolled at room temperature has stronger shear texture and finer grain structure.

scholarly journals Microstructure Evolution and Mechanical Property Characterization of 6063 Aluminum Alloy Tubes Processed with Friction Stir Back Extrusion

JOM ◽  
2019 ◽  
Vol 71 (12) ◽  
pp. 4436-4444
Author(s):  
Suhong Zhang ◽  
Alan Frederick ◽  
Yiyu Wang ◽  
Mike Eller ◽  
Paul McGinn ◽  
...  
Keyword(s):  
Aluminum Alloy ◽  
Microstructure Evolution ◽  
Electron Backscatter Diffraction ◽  
Deformation Gradient ◽  
Optical Microscope ◽  
Grain Structure ◽  
Frictional Heat ◽  
Friction Stir ◽  
Metal Extrusion ◽  
Backscatter Diffraction

Abstract Friction stir back extrusion (FSBE) is a technique for lightweight metal extrusion. The frictional heat and severe plastic deformation of the process generate an equiaxed refined grain structure because of dynamic recrystallization. Previous studies proved that the fabrication of tube and wire structures is feasible. In this work, hollow cylindrical billets of 6063-T6 aluminum alloy were used as starting material. A relatively low extrusion ratio allows for a temperature and deformation gradient through the tube wall thickness to elucidate the effect of heat and temperature on the microstructure evolution during FSBE. The force and temperature were recorded during the processes. The microstructures of the extruded tubes were characterized using an optical microscope, energy-dispersive x-ray spectroscopy, electron backscatter diffraction, and hardness testing. The process reduced the grain size from 58.2 μm to 20.6 μm at the inner wall. The microhardness of the alloy was reduced from 100 to 60–75 HV because of the process thermal cycle.

scholarly journals Cryogenic Deformation Behavior and Microstructural Characteristics of 2195 Alloy

Metals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1406
Author(s):  
Jin Zhang ◽  
Wenfu Tan ◽  
Cheng Wang ◽  
Chunnan Zhu ◽  
Youping Yi
Keyword(s):  
Electron Microscope ◽  
Electron Backscatter Diffraction ◽  
Underlying Mechanism ◽  
Optical Microscope ◽  
W State ◽  
Grain Structure ◽  
Cryogenic Deformation ◽  
Transmission Electron ◽  
Strength And Plasticity ◽  
Backscatter Diffraction

Cryogenic deformation can improve the strength and plasticity of Al–Li alloy, although the underlying mechanism is still not yet well understood. The effects of cryogenic temperature on the tensile properties and microstructure of an Al–Cu–Li alloy were investigated by means of tensile property test, roughness measurement, scanning electron microscope (SEM), optical microscope (OM), electron backscatter diffraction (EBSD), and transmission electron microscope (TEM). The results indicated that the strength and elongation of the as-annealed (O-state) and solution-treated (W-state) alloys increased with the decrease in deformation temperature, where the increasing trend of elongation of the W-state alloy was more significant than that of the O-state alloy. In addition, a temperature range was observed at approximately 178 K that caused the strength of the W-state alloy to slightly decrease. The decrease in temperature inhibited the dynamic recovery of the Al–Cu–Li alloy, which increased the dislocation density and the degree of work hardening, thus improving the strength of the alloy. At cryogenic temperatures, the internal grain structure was more involved in the deformation and the overall deformation was more uniform, which caused the alloy to have higher plasticity. This study provides a theoretical basis for the cryogenic forming of Al–Li alloy.

Cross Section Analysis of Cu Filled TSVs Based on High Throughput Plasma-FIB Milling

2012 ◽  
Author(s):  
Frank Altmann ◽  
Jens Beyersdorfer ◽  
Jan Schischka ◽  
Michael Krause ◽  
German Franz ◽  
...  
Keyword(s):  
High Resolution ◽  
Cross Section ◽  
High Throughput ◽  
Cross Sections ◽  
Electron Backscatter Diffraction ◽  
Grain Structure ◽  
Electron Backscatter ◽  
Section Surface ◽  
Backscatter Diffraction ◽  
Section Analysis

Abstract In this paper the new Vion™ Plasma-FIB system, developed by FEI, is evaluated for cross sectioning of Cu filled Through Silicon Via (TSV) interconnects. The aim of the study presented in this paper is to evaluate and optimise different Plasma-FIB (P-FIB) milling strategies in terms of performance and cross section surface quality. The sufficient preservation of microstructures within cross sections is crucial for subsequent Electron Backscatter Diffraction (EBSD) grain structure analyses and a high resolution interface characterisation by TEM.

Physical Based Microstructure Modelling Coupled with Nucleation Theory during and after Hot Forming of AA5083

2010 ◽  
Vol 89-91 ◽  
pp. 509-514
Author(s):  
Pavel Sherstnev ◽  
Christof Sommitsch ◽  
Stefan Mitsche ◽  
Carsten Melzer
Keyword(s):  
Aluminium Alloy ◽  
Hot Rolling ◽  
Volume Fraction ◽  
Electron Backscatter Diffraction ◽  
Grain Structure ◽  
Nucleation Theory ◽  
Structure Evolution ◽  
Nucleation Sites ◽  
Nucleation Mechanisms ◽  
Backscatter Diffraction

A physical model based on three types of dislocations and three nucleation sites for recrystallized grain is applied to hot rolling simulation. This model was implemented into a commercial Finite Element (FE) analysis package FORGE 2008 to calculate both the structure evolution during and the recrystallized volume fraction after hot working of aluminium alloy 5083. It is shown that the main nucleation mechanisms in the aluminium alloy are the particle stimulated nucleation (PSN) and nucleation at grain boundaries. Hence the precipitation kinetics during homogenisation was investigated by use of the thermodynamic calculation software MatCalc. To validate the simulation results hot rolling experiments were performed by means of a laboratory mill. The grain structure evolution was analysed by electron backscatter diffraction (EBSD).

scholarly journals Texture Evolution in AA6082-T6 BFSW Welds: Optical Microscopy and EBSD Characterisation

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3215 ◽  
Author(s):  
Abbas Tamadon ◽  
Dirk J. Pons ◽  
Don Clucas ◽  
Kamil Sued
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Optical Microscopy ◽  
Electron Backscatter Diffraction ◽  
Texture Evolution ◽  
Grain Structure ◽  
Friction Stir ◽  
Fine Grain ◽  
Grain Structures ◽  
Dynamic Recrystallisation

One of the difficulties with bobbin friction stir welding (BFSW) has been the visualisation of microstructure, particularly grain boundaries, and this is especially problematic for materials with fine grain structure, such as AA6082-T6 aluminium as here. Welds of this material were examined using optical microscopy (OM) and electron backscatter diffraction (EBSD). Results show that the grain structures that form depend on a complex set of factors. The motion of the pin and shoulder features transports material around the weld, which induces shear. The shear deformation around the pin is non-uniform with a thermal and strain gradient across the weld, and hence the dynamic recrystallisation (DRX) processes are also variable, giving a range of observed polycrystalline and grain boundary structures. Partial DRX was observed at both hourglass boundaries, and full DRX at mid-stirring zone. The grain boundary mapping showed the formation of low-angle grain boundaries (LAGBs) at regions of high shear as a consequence of thermomechanical nature of the process.

scholarly journals Microstructure and Texture Evolutions During Deep Drawing of Mg–Al–Mn Sheets at Elevated Temperatures

Materials ◽  
2020 ◽  
Vol 13 (16) ◽  
pp. 3608 ◽  
Author(s):  
Jae-Hyung Cho ◽  
Sang-Ho Han ◽  
Geon Young Lee
Keyword(s):  
Dynamic Recrystallization ◽  
Deep Drawing ◽  
Elevated Temperatures ◽  
Tensile Deformation ◽  
Electron Backscatter Diffraction ◽  
Texture Evolution ◽  
Grain Structure ◽  
Transmission Electron ◽  
Backscatter Diffraction ◽  
Twin Roll

Texture and microstructure evolution of ingot and twin-roll casted Mg–Al–Mn magnesium sheets were examined during deep drawing at elevated temperatures. The twin-roll casted sheets possessed smaller grain sizes and weaker basal intensity levels than the ingot-casted sheets. The strength and elongation at room temperature for the twin-roll casted sheets were greater than those of the ingot-casted sheets. At elevated temperatures, the ingot-casted sheets showed better elongation than the twin-roll casted sheets. Different size and density of precipitates were examined using transmission electron microscopy (TEM) for both ingot-casted and twin-roll-casted sheets. The deep drawing process was also carried out at various working temperatures and deformation rates, 225 °C to 350 °C and 30 mm/min to 50 mm/min, respectively. The middle wall part of cups were mainly tensile deformation, and the lower bent regions of drawn cups were most thinned region. Overall, the ingot-casted sheets revealed better deep drawability than the twin-roll casted sheets. Microstructure and texture evolution of the top, middle and lower parts of drawn cups were investigated using electron backscatter diffraction. Increased deformation rate is important to activate tensile twins both near the bent and flange areas. Ingot casted sheets revealed more tensile twins than twin-roll casted sheets. Increased working temperature is important to activate non-basal slips and produce the DRXed grain structure in the flange. Dynamic recrystallization were frequently found in the top flanges of the cups. Both tensile twins and non-basal slips contributed to occurrence of the dynamic recrystallization in the flange.

Shear Pressing for Grain Refinement of Al-Mg-Li Sheet

2007 ◽  
Vol 546-549 ◽  
pp. 885-888
Author(s):  
Yu Xuan Du ◽  
Xin Ming Zhang ◽  
Ling Ying Ye ◽  
Zhi Hui Luo
Keyword(s):  
Shear Deformation ◽  
Grain Refinement ◽  
Electron Backscatter Diffraction ◽  
Grain Structure ◽  
Grain Refining ◽  
Metallic Materials ◽  
Inclined Plane ◽  
Fine Grained ◽  
Electron Backscatter ◽  
Backscatter Diffraction

A novel shear-deformation technique, named ‘shear pressing’ (SP), was developed for fabrication of plate-shaped fine grained metallic materials. The principle of SP is that a material is subjected to shear deformation by utilizing pressing with inclined plane dies. A micrometer order grain structure was obtained in an Al-Mg-Li alloy at strain of ε = -2.3 by utilizing this technique. The grain refinement sequences during pressing were examined by electron backscatter diffraction. The enhancement of grain refinement to the Al-Mg-Li alloy was compared with plane strain compression (PSC) at similar strains. The effect of the shear strain on the accelerated grain refining during compressing has been discussed.

scholarly journals On the Formation of Micro-Shrinkage Porosities in Ductile Iron Cast Components

Metals ◽  
2018 ◽  
Vol 8 (7) ◽  
pp. 551 ◽  
Author(s):  
Ehsan Ghassemali ◽  
Anders Jarfors ◽  
Attila Diószegi
Keyword(s):  
Ductile Iron ◽  
Electron Backscatter Diffraction ◽  
Pressure Change ◽  
Grain Structure ◽  
Absolute Pressure ◽  
Dendrite Fragmentation ◽  
Austenite Grain ◽  
Backscatter Diffraction ◽  
Parent Austenite ◽  
Ebsd Method

A combination of direct austempering after solidification (DAAS) treatment and electron backscatter diffraction (EBSD) method was used to study the formation of micro-shrinkage porosities in ductile iron. Analyzing the aus-ferritic microstructure revealed that most of micro-shrinkage porosities are formed at the retained austenite grain boundaries. There was no obvious correlation between the ferrite grains or graphite nodules and micro-shrinkage porosities. Due to the absolute pressure change at the (purely) shrinkage porosities, the dendrite fragmentation rate during the DAAS process would be altered locally, which caused a relatively finer parent-austenite grain structure near such porosities.

Formation of Nanoporous Gold Studied by Transmission Electron Backscatter Diffraction

2015 ◽  
Vol 21 (6) ◽  
pp. 1387-1397 ◽  
Author(s):  
Leo T.H. de Jeer ◽  
Diego Ribas Gomes ◽  
Jorrit E. Nijholt ◽  
Rik van Bremen ◽  
Václav Ocelík ◽  
...  
Keyword(s):  
Crystallographic Texture ◽  
Manufacturing Process ◽  
Electron Backscatter Diffraction ◽  
Nanoporous Materials ◽  
Nanoporous Gold ◽  
Grain Structure ◽  
Misorientation Distribution ◽  
Transmission Electron ◽  
Electron Backscatter ◽  
Backscatter Diffraction

AbstractTransmission electron backscatter diffraction (t-EBSD) was used to investigate the effect of dealloying on the microstructure of 140-nm thin gold foils. Statistical and local comparisons of the microstructure between the nonetched and nanoporous gold foils were made. Analyses of crystallographic texture, misorientation distribution, and grain structure clearly prove that during the dealloying manufacturing process of nanoporous materials the crystallographic texture is enhanced significantly with a clear decrease of internal strain, whereas maintaining the grain structure.

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