scholarly journals Constitutive modeling of viscoplasticity including phase transformations for graded thermo‐mechanical processing

PAMM ◽  
2021 ◽  
Vol 21 (1) ◽  
Author(s):  
Hendrik Westermann ◽  
Alexander Reitz ◽  
Rolf Mahnken ◽  
Olexandr Grydin ◽  
Mirko Schaper
Keyword(s):  
Phase Transformations ◽  
Constitutive Modeling ◽  
Mechanical Processing

scholarly journals Characterization of Phase Transformations During Graded Thermo-Mechanical Processing of Press-Hardening Sheet Steel 22MnB5

2020 ◽  
Vol 51 (11) ◽  
pp. 5628-5638
Author(s):  
A. Reitz ◽  
O. Grydin ◽  
M. Schaper
Keyword(s):  
Phase Transformations ◽  
Sheet Steel ◽  
Steel Specimen ◽  
High Strength ◽  
High Energy ◽  
Mechanical Processing ◽  
Press Hardening ◽  
Flat Steel ◽  
High Energy Absorption ◽  
Press Hardening Steel

Abstract Safety-relevant components in automobiles require materials that combine high strength with sufficient residual ductility and high-energy absorption. A graded thermo-mechanical treatment of the press-hardening steel 22MnB5 with graded microstructure can provide a material with such properties. Different austenitization temperatures, cooling and forming conditions within a sheet part lead to the development of microstructures with mixed phase compositions. To determine the resulting phase contents in such graded processed parts, a large number of dilatometric tests are usually required. With a non-contact characterization method, it is possible to detect local phase transformations on an inhomogeneously treated flat steel specimen. For press-hardening steel after heat treatment and thermo-mechanical processing, correlations between austenitization temperature, hot deformation strain, microstructure, and hardness are established.

scholarly journals Parameter Identification for Thermo-Mechanical Constitutive Modeling to Describe Process-Induced Residual Stresses and Phase Transformations in Low-Carbon Steels

2021 ◽  
Vol 11 (2) ◽  
pp. 550
Author(s):  
Muhammed Zubair Shahul Hameed ◽  
Christoph Hubertus Wölfle ◽  
Tobias Robl ◽  
Thomas Obermayer ◽  
Stefan Rappl ◽  
...  
Keyword(s):  
Residual Stresses ◽  
Phase Transformations ◽  
Constitutive Modeling ◽  
Elevated Temperatures ◽  
Surface Region ◽  
Carbon Steels ◽  
Experimental Investigations ◽  
Stress Distributions ◽  
Low Carbon ◽  
Continuous Cooling Transformation Diagram

Reinforcing steel bars (rebars) are widely manufactured using the Tempcore™ process. Several studies have been conducted analyzing the effect of the heat treatment route on the strength and corrosion resistance of rebars, but knowledge of its effects on the residual stresses of the finished product are largely lacking. This paper presents experimental investigations to identify the material parameters necessary to simulate the Tempcore™ process using thermo-elasto-plastic constitutive modeling in order to study the generation of residual stresses during the manufacturing process. Mechanical parameters such as yield strength at elevated temperatures and elastic constants were determined experimentally. A continuous cooling transformation diagram needed to model the phase transformations was also identified and is presented here. Residual stress distributions in the surface region of the rebar were characterized using X-ray diffraction. Further characterizations of microstructure, chemical composition, and hardness were carried out. The constitutive modeling approach for the numerical simulation is briefly described for which the experimentally determined parameters are required as input.

Influence of Thermo-Mechanical Processing on the Microstructure of Beryllia Dispersed Nickel Alloys

1973 ◽  
Vol 31 ◽  
pp. 184-185
Author(s):  
M.S. Grewal ◽  
S.A. Sastri ◽  
N.J. Grant
Keyword(s):  
High Temperature ◽  
Nickel Alloys ◽  
Thermomechanical Processing ◽  
Cold Work ◽  
High Temperature Strength ◽  
Strengthening Effect ◽  
Mechanical Processing ◽  
Uniform Dispersion ◽  
Oxide Particles ◽  
Nickel Base

Currently there is a great interest in developing nickel base alloys with fine and uniform dispersion of stable oxide particles, for high temperature applications. It is well known that the high temperature strength and stability of an oxide dispersed alloy can be greatly improved by appropriate thermomechanical processing, but the mechanism of this strengthening effect is not well understood. This investigation was undertaken to study the dislocation substructures formed in beryllia dispersed nickel alloys as a function of cold work both with and without intermediate anneals. Two alloys, one Ni-lv/oBeo and other Ni-4.5Mo-30Co-2v/oBeo were investigated. The influence of the substructures produced by Thermo-Mechanical Processing (TMP) on the high temperature creep properties of these alloys was also evaluated.

Phase Transformations in Ti-7w/oMo-3w/oMe Alloy

1974 ◽  
Vol 32 ◽  
pp. 514-515
Author(s):  
S. Fujishiro
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Transmission Electron Microscopy ◽  
Tensile Strength ◽  
Mechanical Processing ◽  
Ray Method ◽  
X Ray ◽  
Transmission Electron ◽  
Water Quench ◽  
Alpha Beta

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.

The use of high-resolution FESEM to study solid-state phase transformations and reactions

1994 ◽  
Vol 52 ◽  
pp. 1028-1029
Author(s):  
P. G. Kotula ◽  
D. D. Erickson ◽  
C. B. Carter
Keyword(s):  
Solid State ◽  
High Resolution ◽  
Phase Transformations ◽  
High Efficiency ◽  
Sol Gel ◽  
Quantitative Information ◽  
Solid State Reactions ◽  
Critical Dimensions ◽  
Backscattered Electrons ◽  
Backscattered Electron

High-resolution field-emission-gun scanning electron microscopy (FESEM) has recently emerged as an extremely powerful method for characterizing the micro- or nanostructure of materials. The development of high efficiency backscattered-electron detectors has increased the resolution attainable with backscattered-electrons to almost that attainable with secondary-electrons. This increased resolution allows backscattered-electron imaging to be utilized to study materials once possible only by TEM. In addition to providing quantitative information, such as critical dimensions, SEM is more statistically representative. That is, the amount of material that can be sampled with SEM for a given measurement is many orders of magnitude greater than that with TEM.In the present work, a Hitachi S-900 FESEM (operating at 5kV) equipped with a high-resolution backscattered electron detector, has been used to study the α-Fe2O3 enhanced or seeded solid-state phase transformations of sol-gel alumina and solid-state reactions in the NiO/α-Al2O3 system. In both cases, a thin-film cross-section approach has been developed to facilitate the investigation. Specifically, the FESEM allows transformed- or reaction-layer thicknesses along interfaces that are millimeters in length to be measured with a resolution of better than 10nm.

The use of transmission and analytical electron microscopy in studying reactions and phase transformations in thin film

1993 ◽  
Vol 51 ◽  
pp. 842-843
Author(s):  
K. Barmak
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Phase Transformations ◽  
Analytical Electron Microscopy ◽  
Ex Situ ◽  
Multilayer Thin Films ◽  
Absolute Concentration ◽  
Analytical Electron ◽  
Deposition Step

Generally, processing of thin films involves several annealing steps in addition to the deposition step. During the annealing steps, diffusion, transformations and reactions take place. In this paper, examples of the use of TEM and AEM for ex situ and in situ studies of reactions and phase transformations in thin films will be presented.The ex situ studies were carried out on Nb/Al multilayer thin films annealed to different stages of reaction. Figure 1 shows a multilayer with dNb = 383 and dAl = 117 nm annealed at 750°C for 4 hours. As can be seen in the micrograph, there are four phases, Nb/Nb3-xAl/Nb2-xAl/NbAl3, present in the film at this stage of the reaction. The composition of each of the four regions marked 1-4 was obtained by EDX analysis. The absolute concentration in each region could not be determined due to the lack of thickness and geometry parameters that were required to make the necessary absorption and fluorescence corrections.

A Transmission Electron Microscopical Investigation of Phase Transformations in TiNi

1980 ◽  
Vol 38 ◽  
pp. 340-341
Author(s):  
P. Moine ◽  
G. M. Michal ◽  
R. Sinclair
Keyword(s):  
Electron Microscopy ◽  
Phase Transformations ◽  
Applied Stress ◽  
Structural Changes ◽  
Microscopical Investigation ◽  
Temperature Range ◽  
Transmission Electron ◽  
Electron Microscopical ◽  
Diffraction Effects ◽  
Microscopy Images

Premartensitic effects in near equiatomic TiNi have been pointed out by several authors(1-5). These include anomalous contrast in electron microscopy images (mottling, striations, etc. ),diffraction effects(diffuse streaks, extra reflections, etc.), a resistivity peak above Ms (temperature at which a perceptible amount of martensite is formed without applied stress). However the structural changes occuring in this temperature range are not well understood. The purpose of this study is to clarify these phenomena.

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