scholarly journals Effects of Mo segregation on Charpy absorbed energy in Ti-12Mo alloys

2020 ◽  
Vol 321 ◽  
pp. 11050
Author(s):  
Satoshi Emura ◽  
Xin Ji ◽  
Xiaohua Min ◽  
Koichi Tsuchiya
Keyword(s):  
Room Temperature ◽  
Tensile Elongation ◽  
Solution Treatment ◽  
Charpy Impact ◽  
Transgranular Fracture ◽  
Omega Phase ◽  
Absorbed Energy ◽  
Rolled Sample ◽  
Heterogeneous Distribution ◽  
Charpy Absorbed Energy

Beta phase stabilizing elements such as Mo have strong tendency to segregate. We have introduced swirly type segregation of Mo in Ti-12Mo (mass %) alloy through groove bar rolling. After solution treatment and low temperature aging, hard omega phase was precipitated heterogeneously, which improved the room temperature tensile elongation values without sacrificing tensile strength. In this study, the effect of Mo segregation and heterogeneous distribution of omega phase on Charpy absorbed energy was investigated in Ti-12Mo alloy. Samples with two types of segregation were prepared; namely, swirly segregation in bar rolled sample and layered segregation in plate rolled sample. For comparison, we have also prepared Ti-12Mo bar samples with lesser Mo segregation, through high temperature thermomechanical treatment. Charpy impact tests were carried out at room temperature, 373 K and 473 K, respectively, using the samples after aging to introduce isothermal omega-phase. The samples with the segregation exhibited higher Charpy absorbed energy, especially at higher temperature of 473 K, while the sample with the swirly segregation showed higher Charpy absorbed energy than that with the layered segregation. The sample with lesser Mo segregation exhibited brittle intergranular fracture surface after Charpy testing. On the contrary, samples with Mo segregation exhibited ductile transgranular fracture surfaces.

Influence of Heat Treatment on the Microstructures and Mechanical Properties of K465 Superalloy

2016 ◽  
Vol 849 ◽  
pp. 570-579
Author(s):  
Qiang Huang ◽  
Jin Xia Song ◽  
Qing Li ◽  
Wei Peng Ren ◽  
Xin Guang Guan ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Cooling Rate ◽  
Room Temperature ◽  
Rupture Life ◽  
Tensile Elongation ◽  
Solution Treatment ◽  
Stress Rupture ◽  
Stress Rupture Life ◽  
Microstructures And Mechanical Properties

The microstructures and mechanical properties of superalloy K465 under different heat treatment, including as as-cast, solution treatment and aging, were investigated. The results showed that γ' precipitates in as-cast condition exhibited two kinds of morphologies of fine regular cuboidal shape at dendritic arm and coarse irregular form in interdendritic region. MC carbides decomposed into M6C carbides partly after 1210°C/4h solution treatment. The high temperature stress-rupture life can be improved obviously with the increasing cooling rate. When cooling rate was lower than 70°C/min, the room temperature tensile elongation increased with cooling rate increasing. When cooling rate was higher than 90°C/min the room temperature tensile elongation decreased with cooling rate increasing. The proper cooling rate of 70oC/min~90oC/min is advantageous for the achievement of excellent comprehensive properties. When aging treatments continued the regularization of γ' resulted in the improvement of stress-rupture life and the reduction of tensile elongation. The mechanical property gap between the solution treatment and aging can be decreased with increasing cooling rate.

Ductilization of a Ni3(Si,Ti) Intermetallic Alloy by Addition of Interstitial Type Elements

2011 ◽  
Vol 409 ◽  
pp. 321-326
Author(s):  
Hisashi Kosaka ◽  
Yasuyuki Kaneno ◽  
Takayuki Takasugi
Keyword(s):  
Fracture Surface ◽  
Fracture Mode ◽  
Room Temperature ◽  
Tensile Ductility ◽  
Tensile Elongation ◽  
Intermetallic Alloy ◽  
Intermediate Temperature ◽  
Transgranular Fracture ◽  
Ti Alloy ◽  
Brittle Intergranular Fracture

The effect of a concomitant doping of interstitial type elements boron (B) and carbon (C), and boron (B) and nitrogen (N) on tensile properties of a Ni3(Si,Ti) intermetallic alloy was investigated in the temperature range between room temperature and 973 K. It was found that the concomitant doping of (C/B) and (N/B) remarkably improved the intermediate-temperature tensile elongation of the Ni3(Si,Ti) alloy compared with the simple doping of B or C. It was also shown that the fracture surface of the alloy doped with (C/B) and (N/B) exhibited the ductile transgranular fracture mode while that of the alloy doped with only B showed a brittle intergranular fracture mode at 773 K. These results clearly indicate that the concomitant doping of the interstitial type elements are useful for improving the intermediate-temperature tensile ductility of the Ni3(Si,Ti) alloy.

Thermal Aging Behavior of Grade CF3M Cast Austenitic Stainless Steels

2017 ◽  
Author(s):  
Yasufumi Miura ◽  
Takashi Sawabe ◽  
Kiyoshi Betsuyaku ◽  
Taku Arai
Keyword(s):  
Fracture Toughness ◽  
Stainless Steels ◽  
Thermal Aging ◽  
Impact Test ◽  
Charpy Impact ◽  
Charpy Impact Test ◽  
Ferrite Phase ◽  
Absorbed Energy ◽  
Aging Conditions ◽  
Charpy Absorbed Energy

In this study, CASSs which were thermally aged at 275–400°C for up to 30000 hrs were investigated using atom probe tomography, Charpy impact test, hardness test, and fracture toughness test in order to evaluate the effects of chemical composition and ferrite content on thermal aging embrittlement. Test materials were 4 types of statically casted grade CF3M stainless steels which are used in Japanese BWR plants. As a result of the tests, Charpy absorbed energy at room temperature of all thermal aging conditions were obtained. We also obtained the microstructural evolution in ferrite phase, hardness of ferrite phase, and J–R curves of several aging conditions. The fracture toughness and the Charpy absorbed energy of all materials aged at 275°C for up to 15000 hrs were approximately same as those of unaged materials. On the other hand, reduction of the fracture toughness and the Charpy absorbed energy were observed in the materials aged at 300°C, 320°C, 350°C and 400°C. For the Charpy impact test in this study, the absorbed energy of the material with highest molybdenum was lower than that of the material with highest ferrite content. After the tests, the fracture toughness estimation model for grade CF8M in NUREG/CR-4513 and the method in PVP2005-71528 (H3T model) were discussed in order to confirm the applicability of the prediction methods to CF3M.

Improvement of Room Temperature Ductility of Ni3Al by Unidirectional Solidification

1990 ◽  
Vol 213 ◽  
Author(s):  
Toshiyuki Hirano ◽  
Sea-Sung Chung ◽  
Yoshinao Mishima ◽  
Tomoo Suzuki
Keyword(s):  
Room Temperature ◽  
Single Phase ◽  
Tensile Elongation ◽  
Growth Direction ◽  
Al Alloy ◽  
Transgranular Fracture ◽  
Zone Method ◽  
Room Temperature Ductility ◽  
The Matrix ◽  
Temperature Fracture

ABSTRACTWe present the new promising method to improve the ductility of intermetallic compound, Ni3Al. Stoichiometric and Alrich Ni3A1 were unidirectionally grown at the growth rate of 24 mm/h by a floating zone method (FZ-UDS). The stoichiometric Ni3Al had a columnar-grained and single phase structure, whereas the Al-rich Ni3Al had a Ni3Al matrix with martensite-like precipitates. These alloys exhibited a large tensile elongation along the growth direction at room temperature. Fracture mode is a complete transgranular fracture in the stoichiometric Ni 3Al alloy, and a mixture of transgranular fracture of the matrix and cleavage of the martensite-like precipitates with cracking at the phase boundary in the Al-rich Ni3Al alloys.

scholarly journals Effect of Core Architecture on Charpy Impact and Compression Properties of Tufted Sandwich Structural Composites

Polymers ◽  
2021 ◽  
Vol 13 (10) ◽  
pp. 1665
Author(s):  
Chen Chen ◽  
Peng Wang ◽  
Xavier Legrand
Keyword(s):  
Impact Resistance ◽  
Charpy Impact ◽  
Foam Core ◽  
Structural Composites ◽  
Absorbed Energy ◽  
Compression Properties ◽  
Obvious Benefit ◽  
Negative Effect ◽  
Charpy Absorbed Energy ◽  
Liquid Resin Infusion

This study presents a novel sandwich structure that replaces the polypropylene (PP) foam core with a carbon fiber non-woven material in the tufting process and the liquid resin infusion (LRI) process. An experimental investigation was conducted into the flatwise compression properties and Charpy impact resistance of sandwich composites. The obtained results validate an enhancement to the mechanical properties due to the non-woven core and tufting yarns. Compared to samples with a pure foam core and samples without tufting threads, the compressive strength increased by 45% and 86%, respectively. The sample with a non-woven layer and tufting yarns had the highest Charpy absorbed energy (23.85 Kj/m2), which is approximately 66% higher than the samples without a non-woven layer and 90% higher than the samples without tufting yarns. Due to the buckling of the resin cylinders in the Z-direction that occurred in all of the different sandwich samples during the compression test, the classical buckling theory was adopted to analyze the differences between the results. The specific properties of the weight gains are discussed in this paper. The results show that the core layers have a negative effect on impact resistance. Nevertheless, the addition of tufting yarns presents an obvious benefit to all of the specific properties.

scholarly journals Analysis of Statistical Scatter in Charpy Impact Toughness

2014 ◽  
Vol 783-786 ◽  
pp. 2394-2399 ◽  
Author(s):  
Yasuhito Takashima ◽  
Mitsuru Ohata ◽  
Fumiyoshi Minami
Keyword(s):  
Brittle Fracture ◽  
Impact Toughness ◽  
Weibull Distribution ◽  
Shape Parameter ◽  
Charpy Impact ◽  
Numerical Results ◽  
Statistical Distribution ◽  
Absorbed Energy ◽  
Charpy Impact Toughness ◽  
Charpy Absorbed Energy

Charpy impact toughness values show large statistical scatter, particularly in the ductile-to-brittle transition temperature (DBTT) range. Although the statistical distribution of Charpy absorbed energy has not been clarified, critical values of the stress intensity factor, J-integral and crack-tip opening displacement (CTOD) at brittle fracture generally show the Weibull distribution with two or three parameters. This study proposes a brittle fracture model, based on the weakest link theory, for evaluating the scatter in Charpy absorbed energy KV. The numerical results show that the amplitude of the opening stress fields ahead of the V-notch at varying amounts of KV are uniquely characterized as the square of the applied load. With these numerical results, the Weibull shape parameter of the statistical distribution of KV is almost equal to 2. The proposed statistical model is verified through experimental results. It is found that the statistical distribution of KV is characterized by a two-parameter Weibull distribution with the shape parameter of 2 under the condition of pure brittle fracture.

Mechanical Properties and Aging Behavior of Ultrafine Grained Al-Ag Alloy Fabricated by Accumulative Roll-Bonding

2014 ◽  
Vol 794-796 ◽  
pp. 851-856
Author(s):  
Tadashiege Nagae ◽  
Nobuhiro Tsuji ◽  
Daisuke Terada
Keyword(s):  
Mechanical Properties ◽  
Grain Refinement ◽  
Accumulative Roll Bonding ◽  
Precipitation Hardening ◽  
Tensile Elongation ◽  
Solution Treatment ◽  
High Strength ◽  
Subsequent Aging ◽  
Roll Bonding ◽  
Ultrafine Grained

Accumulative roll-bonding (ARB) process is one of the severe plastic deformation processes for fabricating ultrafine grained materials that exhibit high strength. In aluminum alloys, aging heat treatment has been an important process for hardening materials. In order to achieve good mechanical properties through the combination of grain refinement hardening and precipitation hardening, an Al-4.2wt%Ag binary alloy was used in the present study. After a solution treatment at 550°C for 1.5hr, the alloy was severely deformed by the ARB process at room temperature (RT) up to 6 cycles (equivalent strain of 4.8). The specimens ARB-processed by various cycles (various strains) were subsequently aged at 100, 150, 200, 250°C, and RT. The hardness of the solution treated (ST) specimen increased by aging. On the other hand, hardness of the ARB processed specimen decreased after aging at high temperatures such as 250°C. This was probably due to coarsening of precipitates or/and matrix grains. The specimen aged at lower temperature showed higher hardness. The maximum harnesses achieved by aging for the ST specimen, the specimens ARB processed by 2 cycles, 4 cycles and 6 cycles were 55HV, 71HV, 69HV and 65HV, respectively. By tensile tests it was shown that the strength increased by the ARB process though the elongation decreased significantly. However, it was found that the tensile elongation of the ARB processed specimens was improved by aging without sacrificing the strength. The results suggest that the Al-Ag alloy having large elongation as well as high strength can be realized by the combination of the ARB process for grain refinement and the subsequent aging for precipitation hardening.

scholarly journals Experimental and Numerical Investigation of the ECAP Processed Copper: Microstructural Evolution, Crystallographic Texture and Hardness Homogeneity

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 607
Author(s):  
A. I. Alateyah ◽  
Mohamed M. Z. Ahmed ◽  
Yasser Zedan ◽  
H. Abd El-Hafez ◽  
Majed O. Alawad ◽  
...  
Keyword(s):  
Grain Size ◽  
Equal Channel Angular Pressing ◽  
Cross Section ◽  
Room Temperature ◽  
Pure Copper ◽  
High Density ◽  
Ecap Processing ◽  
Heterogeneous Distribution ◽  
Angular Pressing ◽  
Average Grain Size

The current study presents a detailed investigation for the equal channel angular pressing of pure copper through two regimes. The first was equal channel angular pressing (ECAP) processing at room temperature and the second was ECAP processing at 200 °C for up to 4-passes of route Bc. The grain structure and texture was investigated using electron back scattering diffraction (EBSD) across the whole sample cross-section and also the hardness and the tensile properties. The microstructure obtained after 1-pass at room temperature revealed finer equiaxed grains of about 3.89 µm down to submicrons with a high density of twin compared to the starting material. Additionally, a notable increase in the low angle grain boundaries (LAGBs) density was observed. This microstructure was found to be homogenous through the sample cross section. Further straining up to 2-passes showed a significant reduction of the average grain size to 2.97 µm with observable heterogeneous distribution of grains size. On the other hand, increasing the strain up to 4-passes enhanced the homogeneity of grain size distribution. The texture after 4-passes resembled the simple shear texture with about 7 times random. Conducting the ECAP processing at 200 °C resulted in a severely deformed microstructure with the highest fraction of submicron grains and high density of substructures was also observed. ECAP processing through 4-passes at room temperature experienced a significant increase in both hardness and tensile strength up to 180% and 124%, respectively.

Strength of Commercial Aluminum Alloys after Equal Channel Angular Pressing and Post-ECAP Processing

2006 ◽  
Vol 114 ◽  
pp. 91-96 ◽  
Author(s):  
Maxim Yu. Murashkin ◽  
M.V. Markushev ◽  
Julia Ivanisenko ◽  
Ruslan Valiev
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Tensile Strength ◽  
Aluminum Alloys ◽  
Ultimate Tensile Strength ◽  
Equal Channel Angular Pressing ◽  
Room Temperature ◽  
Solution Treatment ◽  
Ecap Processing ◽  
Angular Pressing

The effects of equal channel angular pressing (ECAP), further heat treatment and rolling on the structure and room temperature mechanical properties of the commercial aluminum alloys 6061 (Al-0.9Mg-0.7Si) and 1560 (Al-6.5Mg-0.6Mn) were investigated. It has been shown that the strength of the alloys after ECAP is higher than that achieved after conventional processing. Prior ECAP solution treatment and post-ECAP ageing can additionally increase the strength of the 6061 alloy. Under optimal ageing conditions a yield strength (YS) of 434 MPa and am ultimate tensile strength (UTS) of 470 MPa were obtained for the alloy. Additional cold rolling leads to a YS and UTS of 475 and 500 MPa with 8% elongation. It was found that the post-ECAP isothermal rolling of the 1560 alloy resulted in the formation of a nano-fibred structure and a tensile strength (YS = 540 MPa and UTS = 635 MPa) that has never previously been observed in commercial non-heat treatable alloys.

Sign in / Sign up

Export Citation Format

Share Document