High temperature mechanical properties of steel bars available in Pakistan

2018 ◽  
Vol 9 (3) ◽  
pp. 203-221 ◽  
Author(s):  
Muhammad Masood Rafi ◽  
Abdul Basit Dahar ◽  
Tariq Aziz

Purpose The purpose of this paper is to present the results of experimental testing of steel rebars at elevated temperatures. Three types of bars available in the local market in Pakistan were used. These data are not available in Pakistan. Design/methodology/approach Three types of bars were used, which included cold-twisted ribbed (CTR), hot-rolled deformed (HRD) and thermo-mechanically treated (TMT) bars. The diameter of the bar of each type was 16 mm. The bars were heated in an electrical furnace at temperatures which were varied from 100°C to 900°C in increment of 100°C. Bars of each type were also tested at ambient temperature as control specimens. The change of strength, strain and modulus of elasticity of the bars at high temperatures were determined. Findings The mechanical properties of the bars were nearly unaffected by the temperatures up to 200°C. CTR bars did not show yield plateau and strain hardening both at ambient and high temperatures. The high temperature yield strength and elastic modulus for all the three types of bars were similar at all temperatures. The yield plateau of both the HRD and TMT bars disappeared at temperatures greater than 300°C. The ultimate strength at high temperature of the HRD and TMT bars was also similar. The behaviours of the HRD and TMT bars changed to brittle beyond 400°C as compared to their behaviours at ambient temperature. The CTR bars exhibited ductile characteristics at failure at all the exposure temperatures relative to their behaviour at ambient temperature. Research limitations/implications The parameters of the paper included the rebar type and heating temperature and the effects of temperature on strength and stiffness properties of the steel bars. Practical implications Building fire incidents have increased in Pakistan. As reinforced concrete (RC) buildings exist in the country in significant numbers, the data related to elevated temperature properties of steel is required. These data are not available in Pakistan presently. The presented paper aims at providing this information for the design engineers to enable them to assess and increase fire resistance of RC structural members. Originality/value The presented paper is unique in its nature in that there is no published contribution to date, to the best of authors’ knowledge, which has been carried out to assess the temperature-dependent mechanical properties of steel reinforcing bars available in Pakistan.

Author(s):  
Iurii Bogomol ◽  
Petro Loboda

The processing techniques, microstructures, and mechanical properties of directionally solidified eutectic ceramics are reviewed. It is considered the main methods for preparing of eutectic ceramics and the relationships between thermal gradient, growth rate, and microstructure parameters. Some principles of coupled eutectic growth, main types of eutectic microstructure and the relationship between the eutectic microstructure and the mechanical properties of directionally solidified eutectics at ambient and high temperatures are briefly described. The mechanical behavior and main toughening mechanisms of these materials in a wide temperature range are discussed. It is shown that the strength at high temperatures mainly depends on the plasticity of the phase components. By analyzing the dislocation structure, the occurrence of strain hardening in single crystalline phases during high-temperature deformation is revealed. The creep resistance of eutectic composites is superior to that of the sintered samples due to the absence of glassy phases at the interfaces, and the strain has to be accommodated by plastic deformation within the domains rather than by interfacial sliding. The microstructural and chemical stability of the directionally solidified eutectic ceramics at high temperatures are discussed. The aligned eutectic microstructures show limited phase coarsening up to the eutectic point and excellent chemical resistance. Directionally solidified eutectics, especially oxides, revealed an excellent oxidation resistance at elevated temperatures. It is shown sufficient potential of these materials for high-temperature applications.


2017 ◽  
Vol 8 (4) ◽  
pp. 418-439 ◽  
Author(s):  
Muhammad Masood Rafi ◽  
Tariq Aziz ◽  
Sarosh Hashmat Lodi

Purpose This paper aims to present the results of testing of low-strength concrete specimens exposed to elevated temperatures. These data are limited in the existing literature and do not exist in Pakistan. Design/methodology/approach An experimental testing programme has been employed. Cylindrical specimens of 100 × 200 mm were used in the testing programme. These were heated at temperatures which were varied from 100°C to 900°C in increment of 100°C. Similar specimens were tested at ambient temperature as control specimens. The compressive and tensile properties of heat treated specimens were determined. Findings The colour of concrete started to change at 300°C and hairline cracks appeared at 400°C. Explosive spalling was observed in few specimens in the temperature range of 400°C-650°C which could be attributed to the pore pressure generated by steam. Significant loss of concrete compressive strength occurred on heating temperatures larger than 600°C, and the residual compressive strength was found to be 15 per cent at 900°C. Residual tensile strength of concrete became less than 10 per cent at 900°C. The loss of concrete stiffness reached 85 per cent at 600°C. Residual Poisson’s ratio of concrete increased at high temperatures and became nearly six times larger at 900°C as compared to that at ambient temperature. Research limitations/implications The parameters of the study included heating temperature and effects of temperature on strength and stiffness properties of the concrete specimens. Practical implications Building fire incidents have increased in Pakistan. As a large number of reinforced concrete (RC) buildings exist in the country, the data related to elevated temperature properties of concrete are required. These data are not available in Pakistan presently. The study aims at providing this information for the design engineers to enable them to assess and increase fire resistance of RC structural members. Originality/value The presented study is unique in its nature in that there is no published contribution to date, to the best of authors’ knowledge, which has been carried out to assess the temperature-dependent mechanical properties of concrete in Pakistan.


Author(s):  
Mohammad S. Alam ◽  
K. M. Rafidh Hassan ◽  
Jeffrey C. Suhling ◽  
Pradeep Lall

Lead free solders are renowned as interconnects in electronic packaging due to their relatively high melting point, attractive mechanical properties, thermal cycling reliability, and environment friendly chemical properties. The mechanical behavior of lead free solders is highly dependent on the operating temperature. Previous investigations on mechanical characterization of lead free solders have mainly emphasized stress-strain and creep testing at temperatures up to 125 °C. However, electronic devices, sometimes, experience harsh environment applications including well drilling, geothermal energy, automotive power electronics, and aerospace engines where solders are exposed to very high temperatures from 125–200 °C. Mechanical properties of lead free solders at elevated temperatures are limited. In this work, we have investigated the mechanical behavior SAC305 (96.5Sn-3.0Ag-0.5Cu) and SAC_Q (SAC+Bi) lead free solders at extreme high temperatures up to 200 °C. Stress-strain tests were performed on reflowed uniaxial specimens at four elevated temperatures (T = 125, 150, 175, and 200 °C). In addition, changes of the mechanical behavior of these alloys due to isothermal aging at T = 125 °C have been studied. Extreme care has been taken during specimen preparation so that the fabricated solder uniaxial test specimens accurately reflect the solder material microstructures present in actual lead free solder joints. High temperature tensile properties of the solders including initial modulus, yield stress, and ultimate tensile strength have been compared. As expected, our results show substantial degradations of the mechanical properties of lead-free solders at higher temperatures. With prior aging, these degradations become even more significant. Comparison of the results has shown that the addition of Bi to traditional SAC alloys improves their high temperature properties and significantly reduces their aging induced degradations.


2019 ◽  
Vol 10 (4) ◽  
pp. 468-481 ◽  
Author(s):  
Mariyana Aida Ab Kadir ◽  
Mohammad Iqbal Khiyon ◽  
Abdul Rahman Mohd. Sam ◽  
Ahmad Beng Hong Kueh ◽  
Nor Hasanah Abdul Shukor Lim ◽  
...  

Purpose The purpose of this paper is to examine the mechanical properties, material composition of spent garnet as a sand replacement in high-strength concrete at room and elevated temperatures. Bonding of the concrete containing spent garnet and reinforcing rebar is investigated. Moreover, the optimum thickness of concrete cover subjected to elevated temperatures is investigated. Design/methodology/approach First, the plain spent garnet was physically, chemically and thermally studied. Then, a series of concrete specimens with 0, 20, 40, 60, 80 and 100 per cent of spent garnet were prepared to determine the optimum percentage of spent garnet. Finally, the physical and mechanical behaviours of concrete specimens and effects of cover thickness on steel rebar when subjected to elevated temperature of 200°C, 400°C, 600°C and 800°C for 1 h were studied. It was observed that spent garnet was thermally stable compared to river sand. Findings Mechanical properties were found to be optimal for concrete with 40% spent garnet replacement. Physically, spent garnet concrete changed colour to brown at 400°C, and to whitish grey at 600°C. The residual compressive strength of spent garnet concrete was also found slightly higher than that for control specimens. At various high temperatures, the reduction in ultimate tensile stress for steel bar inside concrete cover of 30 mm was the lowest compared to that of 20 mm. Research limitations/implications Spalling effect it not considered in this study. Practical implications The optimum concrete cover is important issues in reinforced concrete design. This can be used as a guideline by structural designers when using a different type of concrete material in the construction. Social implications Utilization of the waste spent garnet reduces usage of natural aggregates in concrete production and enhances its performance at elevated temperatures. Natural aggregates are normally taken from sand and rock. The new innovation in concrete perhaps can produce light concrete, reduce the cost of concrete production and at the same time also mitigates environmental problems affect from waste material such as minimizing disposal area. Originality/value Utilization of spent garnet in ordinary Portland cement (OPC) concrete at high temperature is a new innovation. It shows that the concrete cover of the concrete element reduced as compared to the OPC concrete. Reduce in weight concrete however the strength of concrete is similar to conventional concrete. This study at elevated temperature has never been performed by any previous researcher.


2020 ◽  
Vol 27 (1) ◽  
pp. 129-138
Author(s):  
Van Su Le ◽  
Michal M. Szczypinski ◽  
Pavlína Hájková ◽  
Vladimir Kovacic ◽  
Totka Bakalova ◽  
...  

AbstractIn this work, geopolymer foam composites containing waste basalt fibre (10, 30, and 50%wt) were exposed to elevated temperatures of 200, 400, 600, 800 and 1000∘C. With an increase in high temperature, the geopolymer foams material exhibits a decrease in compressive strength and bending strength. When heated above 600∘C, geopolymer foams materials exhibit a significant reduction in mechanical properties. It shows clearly with the naked eye that surface cracks in case of samples containing 10% of basalt filler. However, when increasing fillers with basalt fibres up to 30% and 50%, the cracking of the sample surface is no longer visible to the naked eye. Especially when the temperature increases, the mechanical properties also increase without decreasing in the sample of 50% by weighing to the binder. The results show that reinforcing the geopolymer foams with basalt ground fibre improves the mechanical properties at high temperatures.


2012 ◽  
Vol 532-533 ◽  
pp. 234-237
Author(s):  
Wei Lai Chen ◽  
Ding Hong Yi ◽  
Jian Fu Zhang

The purpose of this paper is to study the effect of high temperature in injection molding process on mechanical properties of the warp-knitted and nonwoven composite fabrics (WNC)used in car interior. Tensile, tearing and peeling properties of WNC fabrics were tested after heat treatment under120, 140,160,180°C respectively. It was found that, after 140°C heat treatment, the breaking and tearing value of these WNC fabrics are lower than others. The results of this study show that this phenomenon is due to the material properties of fabrics. These high temperatures have no much effect on peeling properties of these WNC fabrics. It is concluded that in order to preserve the mechanical properties of these WNC fabrics, the temperature near 140°C should be avoided possibly during injection molding process.


2014 ◽  
Vol 1014 ◽  
pp. 49-52
Author(s):  
Xiao Ping Su

With the wide application of high strength concrete in the building construction,the risk making concrete subject to high temperatures during a fire is increasing. Comparison tests on the mechanical properties of high strength concrete (HSC) and normal strength concrete (NSC) after the action of high temperature were made in this article, which were compared from the following aspects: the peak stress, the peak strain, elasticity modulus, and stress-strain curve after high temperature. Results show that the laws of the mechanical properties of HSC and NSC changing with the temperature are the same. With the increase of heating temperature, the peak stress and elasticity modulus decreases, while the peak strain grows rapidly. HSC shows greater brittleness and worse fire-resistant performance than NSC, and destroys suddenly. The research and evaluation on the fire-resistant performance of HSC should be strengthened during the structural design and construction on the HSC buildings.


2020 ◽  
Vol 86 (17) ◽  
Author(s):  
Miha Bahun ◽  
Marko Šnajder ◽  
Dušan Turk ◽  
Nataša Poklar Ulrih

ABSTRACT Pernisine is a subtilisin-like protease that was originally identified in the hyperthermophilic archaeon Aeropyrum pernix, which lives in extreme marine environments. Pernisine shows exceptional stability and activity due to the high-temperature conditions experienced by A. pernix. Pernisine is of interest for industrial purposes, as it is one of the few proteases that has demonstrated prion-degrading activity. Like other extracellular subtilisins, pernisine is synthesized in its inactive pro-form (pro-pernisine), which needs to undergo maturation to become proteolytically active. The maturation processes of mesophilic subtilisins have been investigated in detail; however, less is known about the maturation of their thermophilic homologs, such as pernisine. Here, we show that the structure of pro-pernisine is disordered in the absence of Ca2+ ions. In contrast to the mesophilic subtilisins, pro-pernisine requires Ca2+ ions to adopt the conformation suitable for its subsequent maturation. In addition to several Ca2+-binding sites that have been conserved from the thermostable Tk-subtilisin, pernisine has an additional insertion sequence with a Ca2+-binding motif. We demonstrate the importance of this insertion for efficient folding and stabilization of pernisine during its maturation. Moreover, analysis of the pernisine propeptide explains the high-temperature requirement for pro-pernisine maturation. Of note, the propeptide inhibits the pernisine catalytic domain more potently at high temperatures. After dissociation, the propeptide is destabilized at high temperatures only, which leads to its degradation and finally to pernisine activation. Our data provide new insights into and understanding of the thermostable subtilisin autoactivation mechanism. IMPORTANCE Enzymes from thermophilic organisms are of particular importance for use in industrial applications, due to their exceptional stability and activity. Pernisine, from the hyperthermophilic archaeon Aeropyrum pernix, is a proteolytic enzyme that can degrade infective prion proteins and thus has a potential use for disinfection of prion-contaminated surfaces. Like other subtilisin-like proteases, pernisine needs to mature through an autocatalytic process to become an active protease. In the present study, we address the maturation of pernisine and show that the process is regulated specifically at high temperatures by the propeptide. Furthermore, we demonstrate the importance of a unique Ca2+-binding insertion for stabilization of mature pernisine. Our results provide a novel understanding of thermostable subtilisin autoactivation, which might advance the development of these enzymes for commercial use.


Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1330
Author(s):  
Muhammad Farzik Ijaz ◽  
Mahmoud S. Soliman ◽  
Ahmed S. Alasmari ◽  
Adel T. Abbas ◽  
Faraz Hussain Hashmi

Unfolding the structure–property linkages between the mechanical performance and microstructural characteristics could be an attractive pathway to develop new single- and polycrystalline Al-based alloys to achieve ambitious high strength and fuel economy goals. A lot of polycrystalline as-cast Al-Cu-Mg-Ag alloy systems fabricated by conventional casting techniques have been reported to date. However, no one has reported a comparison of mechanical and microstructural properties that simultaneously incorporates the effects of both alloy chemistry and mechanical testing environments for the as-cast Al-Cu-Mg-Ag alloy systems. This preliminary prospective paper presents the examined experimental results of two alloys (denoted Alloy 1 and Alloy 2), with constant Cu content of ~3 wt.%, Cu/Mg ratios of 12.60 and 6.30, and a constant Ag of 0.65 wt.%, and correlates the synergistic comparison of mechanical properties at room and elevated temperatures. According to experimental results, the effect of the precipitation state and the mechanical properties showed strong dependence on the composition and testing environments for peak-aged, heat-treated specimens. In the room-temperature mechanical testing scenario, the higher Cu/Mg ratio alloy with Mg content of 0.23 wt.% (Alloy 1) possessed higher ultimate tensile strength when compared to the low Cu/Mg ratio with Mg content of 0.47 wt.% (Alloy 2). From phase constitution analysis, it is inferred that the increase in strength for Alloy 1 under room-temperature tensile testing is mainly ascribable to the small grain size and fine and uniform distribution of θ precipitates, which provided a barrier to slip by deaccelerating the dislocation movement in the room-temperature environment. Meanwhile, Alloy 2 showed significantly less degradation of mechanical strength under high-temperature tensile testing. Indeed, in most cases, low Cu/Mg ratios had a strong influence on the copious precipitation of thermally stable omega phase, which is known to be a major strengthening phase at elevated temperatures in the Al-Cu-Mg-Ag alloying system. Consequently, it is rationally suggested that in the high-temperature testing scenario, the improvement in mechanical and/or thermal stability in the case of the Alloy 2 specimen was mainly due to its compositional design.


2019 ◽  
Vol 2019 ◽  
pp. 1-10 ◽  
Author(s):  
Qifang Xie ◽  
Lipeng Zhang ◽  
Shenghua Yin ◽  
Baozhuang Zhang ◽  
Yaopeng Wu

Fires are always known for seriously deteriorating concrete in structures, especially for those with certain carbonation due to long-time service. In this paper, 75 prism specimens were prepared and divided into four groups (three carbonated groups and one uncarbonated group). Specimens were tested under different temperatures (20, 300, 400, 500, 600, and 700°C), exposure times (3, 4, and 6 hours), and cooling methods (water and natural cooling). Surface characteristics, weight loss rate, and residual mechanical properties (strength, initial elastic modulus, peak, and ultimate compressive strains) of carbonated concrete specimens after elevated temperatures were investigated and compared with that of the uncarbonated ones. Results show that the weight loss rates of the carbonated concrete specimens are slightly lower than that of the uncarbonated ones and that the cracks are increased with raising of temperatures. Surface colors of carbonated concrete are significantly changed, but they are not sensitive to cooling methods. Surface cracks can be evidently observed on carbonated specimens when temperature reaches 400°C. Residual compressive strength and initial elastic modulus of carbonated concrete after natural cooling are generally larger than those cooled by water. The peak and ultimate compressive strains of both carbonated and uncarbonated concrete specimens increase after heating, but the values of the latter are greater than that of the former. Finally, the constitutive equation to predict the compressive behaviors of carbonated concrete after high temperatures was established and validated by tests.


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