Effect on Fracture Pressure by Adding Iron-Based and Calcium-Based Nanoparticles to a Nonaqueous Drilling Fluid for Permeable Formations

2016 ◽  
Vol 138 (3) ◽  
Author(s):  
Oscar Contreras ◽  
Mortadha Alsaba ◽  
Geir Hareland ◽  
Maen Husein ◽  
Runar Nygaard

This paper presents a comprehensive experimental evaluation to investigate the effects of adding iron-based and calcium-based nanoparticles (NPs) to nonaqueous drilling fluids (NAFs) as a fluid loss additive and for wellbore strengthening applications in permeable formations. API standard high-pressure-high-temperature (HPHT) filter press in conjunction with ceramic disks is used to quantify fluid loss reduction. Hydraulic fracturing experiments are carried out to measure fracturing and re-opening pressures. A significant enhancement in both filtration and strengthening was achieved by means of in situ prepared NPs. Our results demonstrate that filtration reduction is essential for successful wellbore strengthening; however, excessive reduction could affect the strengthening negatively.

Geofluids ◽  
2019 ◽  
Vol 2019 ◽  
pp. 1-18 ◽  
Author(s):  
Biao Ma ◽  
Xiaolin Pu ◽  
Zhengguo Zhao ◽  
Hao Wang ◽  
Wenxin Dong

The lost circulation in a formation is one of the most complicated problems that have existed in drilling engineering for a long time. The key to solving the loss of drilling fluid circulation is to improve the pressure-bearing capacity of the formation. The tendency is to improve the formation pressure-bearing capacity with drilling fluid technology for strengthening the wellbore, either to the low fracture pressure of the formation or to that of the naturally fractured formation. Therefore, a laboratory study focused on core fracturing simulations for the strengthening of wellbores was conducted with self-developed fracture experiment equipment. Experiments were performed to determine the effect of the gradation of plugging materials, kinds of plugging materials, and drilling fluid systems. The results showed that fracture pressure in the presence of drilling fluid was significantly higher than that in the presence of water. The kinds and gradation of drilling fluids had obvious effects on the core fracturing process. In addition, different drilling fluid systems had different effects on the core fracture process. In the same case, the core fracture pressure in the presence of oil-based drilling fluid was less than that in the presence of water-based drilling fluid.


Author(s):  
Zisis Vryzas ◽  
Vassilios C. Kelessidis ◽  
Lori Nalbandian ◽  
Vassilios Zaspalis

Smart drilling fluids, which can change their properties according to the flow environment, must be carefully designed so that they can handle the difficult challenges of HP/HT drilling successfully. Due to their unique physico-chemical properties, nanoparticles (NP) are considered as very good candidates for the formulation of these smart drilling fluids. This study presents filtration and rheological results of newly developed high-performance water-based drilling fluid systems containing different nanoparticles, commercial (C) titanium oxide (TiO2) and commercial (C) copper oxide (CuO) NP and compares them with results from using custom-made (CM) iron oxide (Fe3O4) NP and commercial (C) iron oxide (Fe3O4) NP, previously reported. Novel nano-based drilling fluids were made of de-ionized water, 7 wt% commercial Na-bentonite (base fluid), and NP were added at 0.5 wt%. The rheological properties of the produced suspensions were measured at temperatures up to 60°C and at atmospheric pressure with a Couette-type viscometer. Filtration characteristics were determined at elevated pressures and temperatures in a HP/HT filter press (500 psi/176°C) using ceramic discs as filter media, of permeability, k = 775 mD. The results of this study showed that the samples containing 0.5 wt% C TiO2 caused a reduction in the fluid loss by 23%, while C CuO NP resulted in 16% reduction, when compared to that of the base fluid, at these HPHT conditions. This should be compared to the 47% and 34% reduction in fluid loss of 0.5% CM Fe3O4 NP and of 0.5% of C Fe3O4 NP, reported previously. Analysis of rheological data revealed shear-thinning behavior for all the tested novel drilling fluids. The samples containing TiO2 and CuO NP exhibited a yield stress less than that of the base fluid, compared to the increased yield stress observed for the C and CM Fe3O4 NP. This behavior can be attributed to the fact that TiO2 and CuO NP may also act as deflocculants and prevent the gelation of bentonite suspensions. This study shows that commercial nanoparticles of TiO2 and CuO do not perform as well as the Fe3O4 NP on filtration but provide drilling fluids with lower yield stresses, thus they could be considered as alternatives to Fe3O4 in situations where the rheological properties are critical.


2021 ◽  
Vol 11 (1) ◽  
pp. 137-145
Author(s):  
Hani Ali Al Khalaf ◽  
Zeeshan Ahmad ◽  
Gabriella Kovácsné Federer

This study aims to evaluate the effect of wheat flour as a natural and environmentally friendly material on the properties of water-based mud. Recently, many experiments have been conducted with various additives to improve the properties of drilling fluids. The effect of using wheat flour as a new additive to drilling fluid was studied to improve rheological and filtration properties. In the laboratory several samples of water-based mud were prepared, different concentrations of wheat flour from 1 wt% to 7 wt% were added to the mud and tested by using a Fann 35 viscometer, 140 Fann Mud balance, and an API LT-LP filter press. The results showed that adding 7 wt% of wheat flour was the optimal concentration. It was found that the apparent viscosity and yield point increased by 50% and 35%, respectively, when 7 wt% of wheat flour was added to the water-based drilling fluid. Likewise, the fluid loss rate was reduced by 25% when using the same concentration of wheat flour.


Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-12
Author(s):  
Kai Zhao ◽  
Junliang Yuan ◽  
Ming Liu ◽  
Chuanliang Yan ◽  
Liangbin Dou ◽  
...  

Drilling fluid loss in depleted reservoir has been an import issue faced by further tapping the potential of old oil fields. Accurate evaluation of the fracture pressure is the foundation to avoid mud loss. Traditional views suggest that tensile failure is the only fracture mode and the fracture pressure should be determined by a tensile failure criterion, which are not suitable for wells drilled in the depleted reservoir. In this paper, the analysis focuses on the fracture mode and fracture pressure in depleted reservoir, and case studies show that three fracture modes may first occur, and the fracture mode will be changed with reservoir depletion which highly depends on reservoir depletion degree, well azimuth and deviation angle, and the in situ stress state; different failure criteria at different stages of reservoir depletion should be selected to accurately evaluate the fracture pressure. For the vertical well, fracture pressure is no longer a single linear reduction with reservoir depletion; instead, a three-step and two-step reduction may appear, and for the directional well, the fracture pressure is not always decreased; the other patterns such as increase and first increase then decrease may also appear for the wells drilled in reverse and strike fault stress regimes.


1969 ◽  
Vol 9 (04) ◽  
pp. 403-411 ◽  
Author(s):  
B.K. Sinha ◽  
Harvey T. Kennedy

Abstract Recommendations are made for obtaining consistent and reproducible test data on drilling fluids having identical composition. Previously, such a procedure has been difficult to accomplish even when the fluids were mixed in similar equipment. A survey of work in this area indicates that previous methods have been unsatisfactory because previous methods have been unsatisfactory because (1) the muds are extremely sensitive to the duration and violence of agitation during a normal mixing routine, and (2) gelling of the muds occurs before the properties can reach constant values. This gelling is caused by water evaporation resulting from the increase in temperature associated with the agitation. The work shows that these problems largely can be overcome by (1) agitating the constituents of the drilling fluid more vigorously, (2) maintaining a fairly constant temperature, and(3) Protecting the fluid from evaporation. When these steps are followed, the fluid properties approach asymptotic values that do not change by prolonged or accelerated agitation or by aging for a month. The time required to reach asymptotic values or a stabilized state is from 2 to 6 hours and is a function of the mud composition. Introduction Preparation of drilling fluids in the laboratory to determine their suitability to meet specific drilling requirements or to serve as a base fluid to evaluate the effectiveness of thinners, dispersants or other additives normally begins with combining measured quantities of the constituents and stirring them for a short time in a low-speed mixer. This is done to obtain a uniform mixture and to hydrate clays. Then the fluid is further agitated in a higher-speed device (Hamilton Beach mixer or Waring blender) to disperse more thoroughly and clay particles The biggest obstacle in the laboratory investigation of drilling fluids has been the lack of a method of producing a mixture by which reproducible results of the measured properties could be obtained. Numerous investigators have encountered this difficulty. Prior to 1929, density was the only property of mud that customarily was measured. The use of Wyoming bentonite on a large scale after 1929 was mainly responsible for the development of more elaborate testing procedures and for the application of the principles of colloid chemistry to the drilling fluids. Ambrose and Loomis in 1931 were among the first to recognize the plastic flow characteristics of drilling fluids, although Bingham in 1916 had observed The same phenomenon with dilute clay suspensions. Marsh introduced the Marsh funnel for field testing in 1931. By this time, non-Newtonian characteristics of drilling fluids were established. The Stormer and MacMichael viscometers were used to study the rheological properties of the fluids. In the 1930's and early 1940's, the work conducted by several investigators contributed toward a better understanding of drilling fluids. In the mid 1930's, fluid-loss and the associated mud-cake-forming properties of drilling fluids were recognized as important to the behavior of these fluids. The other properties of drilling fluids, including gel strength, pH, and sand content soon were recognized. In 1937, API published its first recommended procedure for test methods. Since that time, these procedures have been revised periodically. The latest edition, RP-13B, was published in 1961 However, in spite of the recognized need for a method of mixing that provides drilling fluids with stabilized properties, no such method previously has been described. SPEJ P. 403


2018 ◽  
Author(s):  
Ζήσης Βρύζας

Η γεώτρηση αποτελεί την πλέον δαπανηρή εργασία σε μια καμπάνια εξεύρεσης και παραγωγής υδρογονανθράκων. Πέραν αυτού συνιστά και την μοναδική διεργασία που δίνει τη δυνατότητα ακριβούς προσδιορισμού των αποθεμάτων στο υπέδαφος. Ο πολφός (γεωτρητικά ρευστά) είναι το ‘αίμα’ της γεώτρησης: παρέχει πίεση, μεταφορά τριμμάτων/θραυσμάτων από τον πυθμένα του φρέατος, ψύξη και λίπανση κοπτικού και στήλης, καθώς επίσης διατηρεί τα θραύσματα εν αιωρήσει όταν υπάρχει διακοπή της κυκλοφορίας. Ως ρευστό γεώτρησης (drilling fluid) χρησιμοποιείται συνήθως ένα αιώρημα πηλού και άλλων υλικών σε νερό. Τα ρευστά διάτρησης με βάση το νερό αποτελούνται από α) νερό, το οποίο αποτελεί την συνεχή φάση και παρέχει το αρχικό ιξώδες (φρέσκο ή θαλασσινό), β) ενεργά στερεά για την ενίσχυση του ιξώδους και του σημείου διαρροής (μπεντονίτης, που συνιστάται στην περίπτωση του φρέσκου νερού και ατταπουλγίτης, αμίαντος ή σιπιόλιθος, που συνιστώνται στην περίπτωση του θαλασσινού νερού), και γ) αδρανή στερεά για την επίτευξη της απαιτούμενης πυκνότητας (βαρύτης, θειούχος μόλυβδος, σιδηρομεταλλεύματα ή χαλαζιακά υλικά).Τα γεωτρητικά ρευστά αποτελούν το 10-20% του συνολικού κόστους κατά την διάρκεια μιας γεώτρησης. Ποσοστό πολύ υψηλό όταν μιλάμε για επενδύσεις εκκατομυρίων δολλαρίων. Λόγω των ολοένα πιο βαθιών αλλά και περίπλοκων γεωλογικών σχηματισμών υπάρχει τεράστια ανάγκη από την πετρελαική βιομηχανία για καινούργια και περισσότερο αποδοτικά γεωτρητικά ρευστά τα οποία θα μπορούν να ανταπεξέλθουν στα ολοένα και πιο απαιτητικά περβάλλοντα θερμοκρασίας και πίεσης. Τα σημαντικότερα ζητήματα τα οποία καλούνται να ανταποκριθούν τα ρευστά είναι οι ολοένα αυξανόμενες συνθήκες πίεσης και θερμοκρασίας στο υπέδαφος που είναι απόροια της αναζήτησης υδρογονανθράκων σε πλέον δύσβατες περιοχές με μεγαλύτερα βάθη που αυξάνουν τους κινδύνους και το κόστος για μια γεώτρηση. Η απώλεια ρευστού κυκλοφορίας (fluid loss) είναι ένα από τα σημαντικότερα και πλέον δαπανηρά προβλήματα κατά την διαδικασία μιας γεώτρησης. Ως απώλεια ρευστού κυκλοφορίας ορίζεται η συνολική ή μερική απώλεια των ρευστών της γεώτρησης σε εξαιρετικά διαπερατές ζώνες (porous sands), σε σπηλαιώδεις σχηματισμούς (cavernous zones), σε φυσικές ρηγματώσεις (natural fractures) και σε ρηγματώσεις προκαλούμενες κατά τη διάτρηση (induced fractures). Τα τελευταία χρόνια έχουν γίνει αρκετές προσπάθειες για την βελτίωση των γεωτρητικών ρευστών με την χρήση νανοσωματιδίων, τα οποία έχουν τη δυνατότητα να βελτιώσουν τις ιδιότητες των γεωτρητικών ρευστών όταν προστίθενται ακόμα και σε χαμηλές συγκεντρώσεις (<1 wt%). Οι μοναδικές τους ιδιότητες σχετίζονται με το μικρό τους μέγεθος και επομένως τον εξαιρετικά μεγάλο λόγο επιφάνειας προς όγκο.Σε αυτή την εργασία, εξετάστηκαν διάφορα εμπορικά νανοσωματίδια (Fe2O3, Fe3O4, SiO2) καθώς επίσης συντέθηκαν, με την μέθοδο της συγκαταβύθισης, νανοσωματιδία μαγνητίτη (custom-made Fe3O4), με και χωρίς επικάλυψη κιτρικού οξέος, τα οποία ερευνήθηκαν ως προς την ικανότητα τους να βελτιώσουν τις ρεολογικές ιδιότητες και την απώλεια ρευστών σε αιωρήματα μπετονίτη. Προκειμένου να χαρακτηρισθούν φυσικοχημικά τα αιωρήματα υπέστησαν ξήρανση με κοκκοποίηση σε θερμοκρασία υγρού Ν2 και κρυοξήρανση. Η μορφολογία, η κρυσταλλική δομή και οι επιφανειακές ομάδες των ξηρών κόνεων εξετάσθηκαν με ηλεκτρονική μικροσκοπία HR-TΕM, περίθλαση ακτίνων Χ (XRD), φυσική ρόφηση Ν2 και φασματοσκοπία FTIR. Οι αλληλεπιδράσεις των σωματιδίων μπετονίτη με τα νανοσωματίδια και οι διάφορες δομές που δημιουργούνται και πως τελικά αυτές επηρεάζουν τις ρεολογικές ιδιότητες των αιωρημάτων εξετάστηκαν με το HR-TEM στους 25°C και 60°C. Με βάση τις εικόνες από το HR-TEM, ένα μοντέλο αλληλεπιδράσεων μεταξύ των διαφορετικών τύπων νανοσωματιδίων και σωματιδίων μπετονίτη δημιουργήθηκε για πρώτη φορά για τέτοια αιωρήματα. Οι ρεολογικές ιδιότητες των παραγόμενων δειγμάτων εξετάστηκαν και σε συνθήκες ατμοσφαιρικής πίεσης (μέχρι 70°C) με την χρήση περιστροφικού ιξωδόμετρου (Grace M3600-Couette type geometry) αλλά και σε συνθήκες υψηλής πίεσης και θερμοκρασίας (69 bar-121°C) (Chandler 7600 HPHT viscometer). Το μοντέλο Herschel-Bulkley χρησιμοποιήθηκε για να περιγράψει τη μεταβολή του ιξώδους με τη μεταβολή των ρεολογικών παραμέτρων δείχνοντας εξαιρετική εφαρμογή για τις διαφορετικές πειραματικές μετρήσεις με συντελεστές συσχέτισης (R2) >0.99 σε όλες τις περιπτώσεις. Οι ρεολογικές μετρήσεις έδειξαν ότι η προσθήκη των νανοσωματιδίων βελτιώνει σημαντικά τις ρεολογικές ιδιότητες των αιωρημάτων μπετονίτη στις διάφορες συνθήκες πίεσης και θερμοκρασίας. Οι απώλειες ρευστών (fluid loss) εξετάστηκαν με φιλτροπρέσες υψηλής πίεσης και θερμοκρασίας (20.7 bar και 121°C) οι οποίες υπολογίζουν τον ρυθμό διήθησης του πολφού μέσω του χρησιμοποιούμενου φίλτρου (κεραμικός δίσκος). Η μεγαλύτερη μείωση στην απώλεια ρευστών επιτεύχθηκε για το δείγμα που περιείχε 0.5 wt% custom-made Fe3O4 με μείωση -40% σε σχέση με το αρχικό δείγμα μπετονίτη που δείχνει την τεράστια ικανότητα των νανοσωματιδίων να βελτιώσουν σημαντικά τις απώλειες ρευστών ακόμα και σε τόσο μικρές συγκεντρώσεις. Τέλος, εξετάστηκε η ικανότητα των παραγόμενων ρευστών να αλλάζουν τις ρεολογικές τους ιδιότητες υπό την επίδραση διάφορων μαγνητικών πεδίων (μέχρι 0.7 Tesla). Τα αποτελέσματα έδειξαν ότι τα καινούργια γεωτρητικά ρευστά έχουν την ικανότητα να αυξάνουν την τάση διολίσθησης (yield stress) έως και 300% σε σχέση με αυτή που μετρήθηκε χωρίς την εφαρμογή μαγνητικού πεδίου. Αυτό είναι κάτι πολύ σημαντικό που επιτρέπει την χρήση έξυπνων ρευστών (smart drilling fluids) τα οποία μπορούν να εξοικονομήσουν και χρόνο αλλά και κόστη κατά την διάρκεια μιας γεώτρησης.Τα νανοσωματίδια δείχνουν πολλές ελπιδοφόρες δυνατότητες σε εφαρμογές γεωτρήσεων αφού έχουν τη δυνατότητα να βελτιώσουν ή και να λύσουν το πρόβλημα της απώλειας ρευστών, όταν προστίθενται ακόμα και σε χαμηλές συγκεντρώσεις (>0.5 wt%), ενώ ταυτόχρονα βελτιστοποιούν τις ρεολογικές ιδιότητες των γεωτρητικών ρευστών. Η χρήση τους για την ανάπτυξη βελτιωμένων γεωτρητικών ρευστών υπόσχεται να αλλάξει την βιομηχανία των γεωτρήσεων και να την βοηθήσει να εξορυχθούν πολύπλοκοι γεωλογικοί σχηματισμοί πιο αποδοτικά αλλά και οικονομικά.


Molecules ◽  
2021 ◽  
Vol 26 (16) ◽  
pp. 4877
Author(s):  
Mobeen Murtaza ◽  
Sulaiman A. Alarifi ◽  
Muhammad Shahzad Kamal ◽  
Sagheer A. Onaizi ◽  
Mohammed Al-Ajmi ◽  
...  

Drilling issues such as shale hydration, high-temperature tolerance, torque and drag are often resolved by applying an appropriate drilling fluid formulation. Oil-based drilling fluid (OBDF) formulations are usually composed of emulsifiers, lime, brine, viscosifier, fluid loss controller and weighting agent. These additives sometimes outperform in extended exposure to high pressure high temperature (HPHT) conditions encountered in deep wells, resulting in weighting material segregation, high fluid loss, poor rheology and poor emulsion stability. In this study, two additives, oil wetter and rheology modifier were incorporated into the OBDF and their performance was investigated by conducting rheology, fluid loss, zeta potential and emulsion stability tests before and after hot rolling at 16 h and 32 h. Extending the hot rolling period beyond what is commonly used in this type of experiment is necessary to ensure the fluid’s stability. It was found that HPHT hot rolling affected the properties of drilling fluids by decreasing the rheology parameters and emulsion stability with the increase in the hot rolling time to 32 h. Also, the fluid loss additive’s performance degraded as rolling temperature and time increased. Adding oil wetter and rheology modifier additives resulted in a slight loss of rheological profile after 32 h and maintained flat rheology profile. The emulsion stability was slightly decreased and stayed close to the recommended value (400 V). The fluid loss was controlled by optimizing the concentration of fluid loss additive and oil wetter. The presence of oil wetter improved the carrying capacity of drilling fluids and prevented the barite sag problem. The zeta potential test confirmed that the oil wetter converted the surface of barite from water to oil and improved its dispersion in the oil.


Author(s):  
Erfan Veisi ◽  
Mastaneh Hajipour ◽  
Ebrahim Biniaz Delijani

Cooling the drill bit is one of the major functions of drilling fluids, especially in high temperature deep drilling operations. Designing stable drilling fluids with proper thermal properties is a great challenge. Identifying appropriate additives for the drilling fluid can mitigate drill-bit erosion or deformation caused by induced thermal stress. The unique advantages of nanoparticles may enhance thermal characteristics of drilling fluids. The impacts of nanoparticles on the specific heat capacity, thermal conductivity, rheological, and filtration control characteristics of water‐based drilling fluids were experimentally investigated and compared in this study. Al2O3, CuO, and Cu nanoparticles were used to prepare the water-based drilling nanofluid samples with various concentrations, using the two-step method. Transmission Electron Microscopy (TEM) and X-Ray Diffraction (XRD) were utilized to study the nanoparticle samples. The nanofluids stability and particle size distribution were, furthermore, examined using Dynamic Light Scattering (DLS). The experimental results indicated that thermal and rheological characteristics are enhanced in the presence of nanoparticles. The best enhancement in drilling fluid heat capacity and thermal conductivity was obtained as 15.6% and 12%, respectively by adding 0.9 wt% Cu nanoparticles. Furthermore, significant improvement was observed in the rheological characteristics such as the apparent and plastic viscosities, yield point, and gel strength of the drilling nanofluids compared to the base drilling fluid. Addition of nanoparticles resulted in reduced fluid loss and formation damage. The permeability of filter cakes decreased with increasing the nanoparticles concentration, but no significant effect in filter cake thickness was observed. The results reveal that the application of nanoparticles may reduce drill-bit replacement costs by improving the thermal and drilling fluid rheological characteristics and decrease the formation damage due to mud filtrate invasion.


2020 ◽  
Vol 10 (8) ◽  
pp. 3449-3466
Author(s):  
Atul Kumar Patidar ◽  
Anjali Sharma ◽  
Dev Joshi

Abstract The hydrocarbon extraction and exploitation using state-of-the-art modern drilling technologies urge the use of biodegradable, environment-friendly drilling fluid and drilling fluid additives to protect the environment and humanity. As more environmental laws are enacted and new safety rules implemented to oust the usage of toxic chemicals as fluid additives, it becomes inevitable that we re-evaluate our choice of drilling fluid additives. Drilling fluids and its additives play a crucial role in drilling operations as well as project costing; hence, it is needed that we develop cost-effective environment-friendly drilling fluid additives that meet the requirements for smooth functioning in geologically complex scenarios as well as have a minimal ecological impact. The current research work demonstrates key outcomes of investigations carried out on the formulation of a sustainable drilling fluid system, where groundnut husk is used as a fluid loss additive and a rheological modifier having no toxicity and high biodegradability. Cellulose was generated from groundnut husk at two varying particle sizes using mesh analysis, which was then compared with the commercially available PAC at different concentrations to validate its properties as a comparable fluid loss retarder additive as well as a rheological modifier. In the present work, various controlling characteristics of proposed groundnut husk additive are discussed, where comparison at different concentrations with a commercially available additive, PAC, is also validated. The API filtration losses demonstrated by the (63–74) µm and the (250–297) µm proposed additive showed a decrease of 91.88% and 82.31%, respectively, from the base mud at 4% concentration. The proposed husk additives acted as a filtrate retarder additive without much deviation from base rheology and with considerably higher pH than the base mud. This investigation indicates that the proposed fluid loss additive and rheological modifier can minimize the environmental hazards and have proved to be a cost-effective eco-friendly alternative in this challenging phase of the hydrocarbon exploration industry.


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