Effect of variation in SiC loading, current density and bath temperature on coating thickness and tensile strength of Ni-SiC nanocomposite coatings

2013 ◽  
Vol 10 (6) ◽  
pp. 515-522
Author(s):  
K. Sharma ◽  
A. Seethagirisha

The mechanical properties like hardness, tensile strength, wear resistance of electro-co-deposited Ni-SiC coatings are dependent on factors like bath temperature, current density, duration of deposition, amount of SiC particles etc. Ni-SiC nano composite coatings were prepared on a mild steel substrate by electro-co-deposition process. In this study, the effect of electrochemical bath parameters such as bath temperature, current density and SiC loading were varied and effect of this variation on the coating thickness and tensile strength of Ni-SiC composite coating was studied. The experimental results showed that, a uniform deposit thickness was obtained for 3 A/dm2 current density, temperature of 55°C and loading of 4 g/l. A peak value of coating thickness was observed at a current density of 4 A/dm2 from the experiment. The experimental results also showed that, the tensile strength of the composite coating containing SiC the is significantly higher than pure Ni coating and the tensile strength increases with an increase in the percentage of SiC particles in Ni-SiC coatings. The tensile strength of the composite coating increased by nearly about 52% with increasing SiC loading and then decreased.

2014 ◽  
Vol 543-547 ◽  
pp. 3707-3710
Author(s):  
Yong Wang ◽  
Lei Zhang

In order to investigate and predict effects of preparation parameters on wear mass loss of Ni-SiC composite coatings, Ni coatings and Ni-SiC composite coatings were prepared on steel substrates by electrodeposition process. The results showed that the contents of SiC particles increased with density of pulse current and on-duty ratio of pulse current increasing. The predictive curves of wear mass losses predicted by ANN had the similar shapes with the measured curve, and the maximum error was 9.7%. When the current density was between 30 A/dm2 and 50 A/dm2, the wear losses of Ni coatings and Ni-SiC coatings decreased with the increase of current density. SiC particles in a composite coating electrodeposited by ultrasonic parameters were much greater in number and were dispersed homogeneously in the deposit, and the Ni-SiC composite coating exhibited a dense structure.


2011 ◽  
Vol 687 ◽  
pp. 641-646 ◽  
Author(s):  
Xue Song Li ◽  
Yue Yang ◽  
You Yang ◽  
Hua Wu

Eelectrodeposited black Cr-C nano-composite coating was prepared on the steel substrate and the effects of current density on the properties of the composite coating were studied in the present paper. The surface morphology and phase composition of the composite coatings were analyzed by means of scanning electronic microscopy (SEM) and X-ray diffractometer (XRD). Microhardness was determined by micrometer and the wear resistance of the coatings was evaluated by CETR using a universal materials tester (UMT). The results showed that formed under the condition of current density of 100A/dm2, temperature of 15°C, and the optimum particle content in electrolyte was 10g/l. The maximum microhardness of black Cr-C nano-composite coating was 10.8 Gpa, simutaneously, the wearing resistance of the coating improved significantly compared to the steel substrate.


2007 ◽  
Vol 345-346 ◽  
pp. 1533-1536 ◽  
Author(s):  
Teck Su Oh ◽  
Jae Ho Lee ◽  
Ji Young Byun ◽  
Tae Sung Oh

In Ni-SiC composite coating, the SiC content is dependent on the surface properties of SiC particles. As sulfuric acid has a strong dehydration force, addition of sulfuric acid in the Ni sulfamate bath changed the surface properties of SiC particles, affecting the codeposition behavior of SiC particles. Also the additives such as SDS affect the electrodeposition behavior of the Ni-SiC composite coating. In this study, effects of the HSO4 ‾ and the current density on the electrodeposition behavior of the Ni-SiC composite coating have been investigated. The Ni-SiC composite coatings were electrodeposited at current densities of 50~200mA/cm2. The surface and cross-sectional morphologies of the Ni-SiC composite coatings were observed using SEM, and their mechanical properties were characterized with micro-Vikers hardness.


2012 ◽  
Vol 457-458 ◽  
pp. 146-149
Author(s):  
Yan Hai Cheng ◽  
Shi Ju Zhang ◽  
Yu Xing Peng ◽  
Fang Fang Xing ◽  
Jie Li ◽  
...  

In this study, Ni-P-SiC composite coatings were prepared by adding different amount of SiC particles into electroless Ni-P plating solution. The effects of SiC particles concentration in solution on depositing rate and composition of the coatings were investigated. The different SiC contents in coatings could be obtained by adjusting the amount of SiC particle concentration in electroless plating solution. Scanning electron microscopy (SEM) results indicate that SiC particles are dispersed in the composite coating and Ni-P alloy is mainly as a bond metal envelope with SiC particles. At the same time, the microhardness became increased and the wear resistance improved with the increasing of SiC content.


2020 ◽  
Vol 34 (27) ◽  
pp. 2050243
Author(s):  
Hui Fan ◽  
Jie Jiang ◽  
Yangpei Zhao ◽  
Shankui Wang ◽  
Zhijing Li

Ni–Al2O3 composite coatings were prepared with a modified Watt’s bath by using jet electrodeposition method. As the key process parameter, current density and the addition of Al2O3 nanoparticles in electrolyte were studied about the effect on the surface morphology and co-deposition of Al2O3 nanoparticles of composite coating. The mechanical and tribological properties of the composite coating were also tested. The results show that properly increasing the current density and Al2O3 addition can increase the co-deposition of nanoparticles in the coating and promote the formation of a dense and refined coating structure. Using the optimized process parameters of current density (300 A/dm2) and Al2O3 addition (30 g/L), the co-deposition of Al2O3 in the composite coating can reach a maximum of 13.1 at.%. The hardness of the coating reaches the peak at 623 HV. The wear rate of the composite coating is also greatly reduced with optimized parameters.


2014 ◽  
Vol 633-634 ◽  
pp. 787-790
Author(s):  
Lin Wang ◽  
Jin Lin Lu ◽  
Cheng Wei Li ◽  
Shu Mei Kang

In order to improve the corrosion resistance of Ni-nanoZrO2 composite coatings. By orthogonal test method,the process for composite electroplating of Ni-ZrO2 was optimized involved current density、bath temperature、the ZrO2 particle concentration. Corrosion resistance and the hardness were tested, microstructure was observed with a scanning electron microscope. The optimized technological conditions are:current density i4A/dm2,bath temperature 45°C, nanoZrO2 addition 7g/L. In this optimum process condition, corrosion current density is 6.186×10-6 A/cm2, corrosion resistance is good, and its hardness is much better than pure nickel plating, also a flat morphology and compact microstructure Ni-ZrO2 nanocomposite coating is get.


2015 ◽  
Vol 228 ◽  
pp. 132-137 ◽  
Author(s):  
B. Łosiewicz ◽  
Grzegorz Dercz ◽  
Magdalena Popczyk

The Ni-Mo+MoO2composite coatings were obtained onto the steel substrate using anin situco-deposition of a Ni-Mo alloy and MoO2powder particles maintained in suspension in the potassium pyrophosphate bath. To characterize the physical and chemical properties of the obtained coatings, SEM, EDS, and XRD methods, were applied. It was found that the co-deposited MoO2particles strongly influenced the properties of the Ni-Mo alloy coating. In comparison with the comparable Ni-Mo deposit containing 45 at.% of Mo, the presence of MoO2embedded into the composite coating diminished the content of Mo alloyed with Ni to 23 at.%. The electrodeposited Ni-Mo+MoO2composite coating obtained under proposed electrochemical conditions contained 25 at.% of MoO2. The effect of the embedded MoO2as composite component on changes of the surface morphology and structure of the Ni-Mo binary alloy, was also discussed.


2012 ◽  
Vol 503-504 ◽  
pp. 503-506
Author(s):  
Li Bin Niu ◽  
Chun Yuan ◽  
Du Meng Cao

In the paper, titanium tri-aluminide (Al3Ti) particles reinforced aluminium (Al)-based composite coatings were fabricated by infiltration plus in-situ techniques at 891.3 °C. The obtained composite coatings are characterized by XRD, SEM and friction and wear testers. The experimental results show that the reaction between Ti wires and Al molten increases with extending time, Ti wires can totally transform into Al3Ti particles for 20 min, which present blocky and strip-like states, respectively. The wear rates of the composite coatings decrease with increasing time.


2011 ◽  
Vol 314-316 ◽  
pp. 253-258
Author(s):  
Xin Kun Suo ◽  
Xue Ping Guo ◽  
Wen Ya LI ◽  
Marie Pierre Planche ◽  
Chao Zhang ◽  
...  

In this paper, dense AZ91D/SiC composite coatings were fabricated by cold spraying. The microstructure and microhardness of the as-sprayed coatings were investigated. The results show that the content of SiC particles in the composite coating was 23.6 ± 7.5 vol.%. The microhardness of the composite coating was improved to 140 HV0.3 due to the enhancement of SiC particles, compared to 98 HV0.3 for the pure AZ91D coating. The wear behavior of the composite coating in an ambient condition was studied through a ball-on-disc dry sliding test system. The composite coating showed higher friction coefficient and lower wear rate than the pure AZ91D coating. The wear mechanism of the composite coating was discussed.


Coatings ◽  
2018 ◽  
Vol 8 (9) ◽  
pp. 297 ◽  
Author(s):  
Yuncai Zhao ◽  
Wen He ◽  
Huihui Du ◽  
Peng Luo

The plasma sprayed Fe-based Ni/WC composite coating on the surface of 45 steel was post-treated by laser remelting with the addition of nano-SiC. The effect of laser power on the interface microstructure of a laser remelting nano-SiC modified Fe-based Ni/WC composite coatings were researched. The metallographic structure, microscopic morphology, phase composition, and microhardness of the remelted layer were visually analyzed by metallographic microscope, scanning electron microscope (SEM), X-ray diffractometer (XRD), and microhardness tester, respectively. The results showed that the nano-SiC modified remelted coating was smooth and compact, and with no fine cracks. The remelted layer was mainly composed of [Fe,Ni], Cr, Fe0.04Ni0.36 phase. The metal elements Fe, Ni, Cr, and Si, and non-metallic element C, appeared to diffuse, and there was metallurgical bonding between the coating and the matrix. With the increase of laser power, the smaller the average grain size, the wider the half-peak height (FWHM), and the more obvious the grain refinement. When the laser power was 500 W, the interface metallurgical showed the best effect. Furthermore, the nano-sized SiC particles served as the core of the heterogeneous nucleation to refine the grains on the one hand, and promoted the formation of a hard intermediate phase in the coating on the other hand. Therefore, the laser remelting and the addition of nano-SiC particles greatly improved the microhardness of the coating. The larger the laser power, the smaller the microstructure characteristics and the fewer the number of holes. With increasing laser power, the hardness increased in general terms and the maximum hardness increased by 51%.


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