Precipitates formation and its impact in friction stir welded and post-heat-treated Inconel 718 alloy

2011 ◽  
Vol 1363 ◽  
Author(s):  
Kuk Hyun Song ◽  
Han Sol Kim ◽  
Won Yong Kim
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Inconel 718 ◽  
Rotation Speed ◽  
Base Material ◽  
Post Heat Treatment ◽  
Inconel 718 Alloy ◽  
Friction Stir ◽  
Heat Treated

ABSTRACTIn order to investigate the formation of precipitates such as MC carbides and intermetallic compounds in the friction stir welded and post-heat-treated Inconel 718 alloy, this work was carried out. Furthermore, the microstructural and mechanical properties of welds and post-heat-treated material were evaluated to identify the effect on precipitates formed during post-heat-treatment. Friction stir welding (FSW) was performed at a rotation speed of 200 rpm and welding speed of 150 mm/min; heat treatment was performed after welding at 720 °C for 8 hours in vacuum. As a result, the grain size due to FSW was notably refined from 5–20 μm in the base material to 1–3 μm in the stir zone; this was accompanied by dynamic recrystallization, which resulted in enhancements in the mechanical properties as compared to the base material. In particular, applying heat treatment after FSW led to improvements in the mechanical properties of the welds—the microhardness and tensile strength increased by more than 50% and 40% in fraction, respectively, as compared to FSW alone.

scholarly journals Study of Microstructure and Mechanical Properties of As-built and Heat-treated Additive Manufactured Inconel 718 Alloy

2021 ◽  
Vol 38 (3) ◽  
Author(s):  
Ajay Kumar Maurya ◽  
Amit Kumar
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Inconel 718 ◽  
Failure Modes ◽  
Grain Structure ◽  
Inconel 718 Alloy ◽  
Laves Phases ◽  
Design Data ◽  
Microstructure And Mechanical Properties ◽  
Heat Treated

Additive manufacturing technology is becoming popular in the industry because it allows the manufacturer to fabricate cost-effective, strong, lightweight, and complex-shaped parts directly from 3D design data as compared with the conventional manufacturing method. Inconel 718 alloy is the most demanding material in aviation as well as in the automobile industry, in terms of manufacturing high-performance parts. In this study, Inconel 718 samples were built using the direct metal laser sintering process, and standard heat treatment was performed on the samples to improve their microstructure and mechanical properties. The as-built samples exhibited good grain structure with fine laves phases, but the matrix was free from ?' and ?" phases. During the heat treatment, the strengthening phases ?' and ?" precipitated. The mechanical properties of as-built and heat-treated samples were analysed and compared. Tensile tests revealed that the direct-aged sample had the higher tensile strength compared with the other conditions, whereas the as-built samples had higher ductility. Finally, fractography and microstructure analysis were performed to measure the failure modes of tensile specimens.

scholarly journals Influence of Post Weld Heat Treatment on the Grain Size, and Mechanical Properties of the Alloy-800H Rotary Friction Weld Joints

Materials ◽  
2021 ◽  
Vol 14 (16) ◽  
pp. 4366
Author(s):  
Saqib Anwar ◽  
Ateekh Ur Rehman ◽  
Yusuf Usmani ◽  
Ali M. Al-Samhan
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
Heat Affected Zone ◽  
Tensile Testing ◽  
Weld Zone ◽  
Alloy 800H ◽  
Weld Joints ◽  
Heat Treated ◽  
Friction Weld

This study evaluated the microstructure, grain size, and mechanical properties of the alloy 800H rotary friction welds in as-welded and post-weld heat-treated conditions. The standards for the alloy 800H not only specify the composition and mechanical properties but also the minimum grain sizes. This is because these alloys are mostly used in creep resisting applications. The dynamic recrystallization of the highly strained and plasticized material during friction welding resulted in the fine grain structure (20 ± 2 µm) in the weld zone. However, a small increase in grain size was observed in the heat-affected zone of the weldment with a slight decrease in hardness compared to the base metal. Post-weld solution heat treatment (PWHT) of the friction weld joints increased the grain size (42 ± 4 µm) in the weld zone. Both as-welded and post-weld solution heat-treated friction weld joints failed in the heat-affected zone during the room temperature tensile testing and showed a lower yield strength and ultimate tensile strength than the base metal. A fracture analysis of the failed tensile samples revealed ductile fracture features. However, in high-temperature tensile testing, post-weld solution heat-treated joints exhibited superior elongation and strength compared to the as-welded joints due to the increase in the grain size of the weld metal. It was demonstrated in this study that the minimum grain size requirement of the alloy 800H friction weld joints could be successfully met by PWHT with improved strength and elongation, especially at high temperatures.

Mechanical Behavior of Friction Stir Welded AA-6061 Thick Plates in Different Heat Treatment Conditions

2021 ◽  
Vol 875 ◽  
pp. 203-210
Author(s):  
Talha Ahmed ◽  
Wali Muhammad ◽  
Zaheer Mushtaq ◽  
Mustasim Billah Bhatty ◽  
Hamid Zaigham
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aging Treatment ◽  
Travel Speed ◽  
Butt Joint ◽  
Tensile Fracture ◽  
Friction Stir ◽  
Treatment Conditions ◽  
Heat Treated ◽  
Joint Form

In this study, mechanical properties of friction stir welded Aluminum Alloy (AA) 6061 in three different heat treatment conditions i.e. Annealed (O), Artificially aged (T6) and Post Weld Heat Treated (PWHT) were compared. Plates were welded in a butt joint form. Parameters were optimized and joints were fabricated using tool rotational speed and travel speed of 500 rpm and 350 mm/min respectively. Two sets of plates were welded in O condition and out of which one was, later, subjected to post weld artificial aging treatment. Third set was welded in T6 condition. The welds were characterized by macro and microstructure analysis, microhardness measurement and mechanical testing. SEM fractography of the tensile fracture surfaces was also performed. Comparatively better mechanical properties were achieved in the plate with PWHT condition.

scholarly journals Research on the Friction Stir Welding of Sc-Modified AA2519 Extrusion

Metals ◽  
2019 ◽  
Vol 9 (10) ◽  
pp. 1024 ◽  
Author(s):  
Robert Kosturek ◽  
Lucjan Śnieżek ◽  
Janusz Torzewski ◽  
Marcin Wachowski
Keyword(s):  
Mechanical Properties ◽  
Friction Stir Welding ◽  
Base Material ◽  
Stir Zone ◽  
Welding Parameters ◽  
Friction Stir ◽  
Treated Condition ◽  
Heat Treated ◽  
Heat Treated Condition ◽  
Fsw Parameters

The aim of this research was to investigate the effect of friction stir welding (FSW) parameters on microstructure and mechanical properties of Sc-modified AA2519 extrusion joints. The workpiece was welded by FSW in non-heat-treated condition with seven different sets of welding parameters. For each obtained joint macrostructure and microstructure observations were performed. Mechanical properties of joints were investigated using tensile test together with localization of fracture location. Joint efficiencies were established by comparing measured joints tensile strength to the value for base material. The obtained results show that investigated FSW joints of Sc-modified AA2519 in the non-heat-treated condition have joint efficiency within the range 87–95%. In the joints obtained with the lowest ratio of the tool rotation speed to the tool traverse speed, the occurrence of imperfections (voids) localized in the stir zone was reported. Three selected samples were subjected to further investigations consisting microhardness distribution and scanning electron microscopy fractography analysis. As the result of dynamic recrystallization, the microhardness of the base material value of 86 HV0.1 increased to about 110–125 HV0.1 in the stir zone depending on the used welding parameters. Due to lack of the strengthening phase and low strain hardening of used alloy the lack of a significantly softened zone was reported by both microhardness analysis and investigation of the fractured samples.

scholarly journals Effects of Post Heat Treatment on the Mechanical Properties of Cold-Rolled Ti/Cu Clad Sheet

Metals ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1672
Author(s):  
Chang-Suk Youn ◽  
Dong-Geun Lee
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Rolling Process ◽  
Post Treatment ◽  
Post Heat Treatment ◽  
Clad Sheet ◽  
Heat Treated ◽  
Bonding Properties ◽  
High Elongation ◽  
Cold Rolled

Titanium and titanium alloys have excellent corrosion and heat resistance, but weak electric and thermal conductivity. The weak conductivity of titanium can be overcome by cladding with copper, which has high conductivity. Although titanium is expensive, it is selected as a material suitable for applications requiring corrosion resistance such as in heat exchangers. This study was to investigate the effect of post heat treatment on the mechanical properties of the Ti/Cu cold-rolled clad plate by using the interfacial diffusion bonding. A titanium clad by cold rolling should be heat-treated after the rolling process to improve the bonding properties through the diffusion of metals and removal of residual stress due to work hardening, despite the easy formation of intermetallic compounds of Ti and Cu. As a result post-treatment, the elongation was improved by more than two times from 21% to max. 53% by the Ti-Cu interface diffusion phenomenon and the average tensile strength of the 450 °C heat-treated specimens was 353 MPa. By securing high elongation while maintaining excellent tensile and yield strength through post-treatment, the formability of Ti-Cu clad plate can be greatly improved.

Effect of post-heat treatment cooling on microstructure and mechanical properties of selective laser melting manufactured austenitic 316L stainless steel

2020 ◽  
Vol 26 (10) ◽  
pp. 1739-1749
Author(s):  
Saad Waqar ◽  
Jiangwei Liu ◽  
Qidong Sun ◽  
Kai Guo ◽  
Jie Sun
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Grain Size ◽  
316L Stainless Steel ◽  
Laser Melting ◽  
Content Type ◽  
Post Annealing ◽  
Cooling Conditions ◽  
Microstructure And Mechanical Properties ◽  
Heat Treated

Purpose This paper aims to investigate the influence of different post-annealing cooling conditions, i.e. furnace cooling (heat treatment (HT) 1 – slow cooling) and air cooling (HT 2 – fast cooling), on the microstructure and mechanical properties of selective laser melting (SLM) built austenitic 316L stainless steel (SS). Design/methodology/approach Three sets of 316L SS samples were fabricated using a machine standard scanning strategy. Each set consists of three tensile samples and a cubic sample for microstructural investigations. Two sets were subsequently subjected to annealing HT with different cooling conditions, i.e. HT 1 and HT 2, whereas one set was used in the as-built (AB) condition. The standard metallographic techniques of X-ray diffraction, scanning electron microscopy and electron back-scattered diffraction were used to investigate the microstructural variations induced by different cooling conditions. The resultant changes in mechanical properties were also investigated. Findings The phase change of SLM fabricated 316L was observed to be independent of the investigated cooling conditions and all samples consist of austenite phase only. Both HT 1 and HT 2 lead to dissolved characteristic melt pools of SLM. Noticeable increase in grain size of HT 1 and HT 2 samples was also observed. Compared with AB samples, the grain size of HT 1 and HT 2 was increased by 12.5% and 50%, respectively. A decreased hardness and strength, along with an increased ductility was also observed for HT 2 samples compared with HT 1 and AB samples. Originality/value From previous studies, it has been noticed that most investigations on HT of SLM fabricated 316L were mainly focused on the HT temperature or holding time. However, the post-HT cooling rate is also an equally important factor in deciding the microstructure and mechanical properties of heat-treated components. Therefore, this paper investigates the influence of different post-annealing cooling conditions on microstructure and mechanical properties of SLM fabricated 316L components. This study provides a foundation for considering the post-HT cooling rate as an influential parameter that controls the properties of heat-treated SLM components.

scholarly journals Microstructural Evolution and Mechanical Properties of Friction Stir Welded Butt Joints of 5A06 Alloy Ultra-Thin Sheets

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3906 ◽  
Author(s):  
Yang Han ◽  
Xiaoqing Jiang ◽  
Tao Yuan ◽  
Shujun Chen ◽  
Dongxiao Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Grain Size ◽  
Grain Boundaries ◽  
Microstructural Evolution ◽  
Welding Speed ◽  
Base Material ◽  
Thin Plates ◽  
Al Alloy ◽  
Minimum Thickness ◽  
Friction Stir

Ultra-thin plates have great potential for applications in aircraft skin, the packaging industry, and packaging of electronic products. Herein, 1 mm-thick 5A06 Al alloy was welded with friction stir welding. The microstructural evolution of the welds was investigated in detail with optical microscopy, scanning electron microscopy, and electron backscatter diffraction. The results showed that the friction stir welds of 1 mm-thick 5A06 Al alloy were well formed without obvious defect and with a minimum thickness reduction of 0.025 mm. Further, the grain size and the proportion of low-angle grain boundaries decreased with decreasing welding speed, because of the increasing degree of dynamic recrystallization. Among all of the welded joints, the welding speed of 100 mm/min yielded the smallest grain size and the highest proportion of high-angle grain boundaries, and thus the best mechanical properties. Specifically, the tensile strength of the joint was greater than that of the base material, while the elongation reached 80.83% of the base material.

Effect of Aging Heat Treatment on the Mechanical Properties in Inconel 718 Alloy

2013 ◽  
Vol 30 (3) ◽  
pp. 271-277 ◽  
Author(s):  
Hee Jae Kang ◽  
Jung Min Kim ◽  
Sung Hwan Jee ◽  
Jie Hyun Sung ◽  
Young Hee Kim ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Inconel 718 ◽  
Inconel 718 Alloy ◽  
Aging Heat Treatment
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