Electrophoretic deposition of TiO2 nanopillars from stable colloidal solution.
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ABSTRACTTitanium dioxide nanoparticles were synthesized by solvothermal treatment in the presence of oleic acid and oleylamine. As Ti(IV) reactant, crystals of [Ti8O12 (H2O)24]Cl8, HCl, 7H2O were preferred because their hydrolysis and condensation can be controlled in ethanol/water solution. The organic surfactants allowed the control of the shape and they can be removed by an acid treatment of the particles. The TiO2 nanoparticles can then be re-dispersed in an ethanol-based charging solution. A fixed applied voltage promotes the electrophoretic deposition of the nanoparticles (<15 nm in size) into pores of anodized aluminium oxide (AAO) template.
2015 ◽
Vol 654
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pp. 230-239
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2017 ◽
2014 ◽
Vol 22
(2)
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pp. 73-87
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2018 ◽
Vol 20
(9)
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pp. 787-795
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