The Effects of Power Level on the Microwave Heating of Selected Chemicals and Minerals

1988 ◽  
Vol 124 ◽  
Author(s):  
S. L. McGill ◽  
J. W. Walkiewicz ◽  
G. A. Smyres

ABSTRACTThe effect of power level on the microwave heating characteristics of a variety of reagent-grade chemicals and minerals has been determined in a Bureau of Mines study. Heating rates of the powdered samples are presented for incident power ranging from 500 to 2,000 W at 2.45 GHz. The apparatus consisted of a WR 975 waveguide-applicator mounted to WR 284 waveguide sections and connected to a 3-kW power source. Tests were conducted in an alumina crucible enclosed in a fused-quartz beaker that was fitted with a Teflon lid to allow for a controlled inert atmosphere and thermocouple insertion. In general, heating rates increased as input power increased. Exceptions to this were some very high-lossy (microwave receptive) and very low-lossy materials that showed negligible changes with increased power. Microwave data collected should provide insight as to possible chemical and mineral processing applications as well as to assist in predictions of processing parameters.

1984 ◽  
Vol 57 (1) ◽  
pp. 134-144 ◽  
Author(s):  
C. S. Wang

Abstract In continuous microwave heating, the temperature rise of rubber extrudates and the level of unabsorbed or reflected microwave power are strongly dependent upon the microwave power level, residence time, and extrudate configuration. It is therefore essential to control these processing parameters, together with the energy absorption characteristics of rubber materials, to improve the efficiency of microwave heating process.


Metals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 888
Author(s):  
Paula Alvaredo-Olmos ◽  
Jon Molina-Aldareguía ◽  
Alvaro Vaz-Romero ◽  
Estela Prieto ◽  
Jesús González-Julián ◽  
...  

This work presents two new compositions of high entropy alloys (HEAs) that were designed with the aim of obtaining a body-centered cubic (BCC) phase with high hardness values and a moderate density. Sintering was performed using Spark Plasma Sintering (SPS) with different heating rates to determine the influence of the processing parameters on the phase formation. The microstructural study revealed that the presence of Ni in the composition promoted phase separation, and the mechanical study confirmed a clear influence on the mechanical properties of both the composition and heating rate. The combination of microscopy with compression and nanoindentation tests at room and high temperature made it possible to advance our understanding of the relationships between the composition, processing, and properties of this emerging group of alloys.


Author(s):  
Frédéric Drillet ◽  
Jérôme Loraine ◽  
Hassan Saleh ◽  
Imene Lahbib ◽  
Brice Grandchamp ◽  
...  

Abstract This paper presents the radio frequency (RF) measurements of an SPST switch realized in gallium nitride (GaN)/RF-SOI technology compared to its GaN/silicon (Si) equivalent. The samples are built with an innovative 3D heterogeneous integration technique. The RF switch transistors are GaN-based and the substrate is RF-SOI. The insertion loss obtained is below 0.4 dB up to 30 GHz while being 1 dB lower than its GaN/Si equivalent. This difference comes from the vertical capacitive coupling reduction of the transistor to the substrate. This reduction is estimated to 59% based on a RC network model fitted to S-parameters measurements. In large signal, the linearity study of the substrate through coplanar waveguide transmission line characterization shows the reduction of the average power level of H2 and H3 of 30 dB up to 38 dBm of input power. The large signal characterization of the SPST shows no compression up to 38 dBm and the H2 and H3 rejection levels at 38 dBm are respectively, 68 and 75 dBc.


2019 ◽  
Vol 38 (2) ◽  
pp. 202-212 ◽  
Author(s):  
Ghulam Ali ◽  
Jan Nisar ◽  
Munawar Iqbal ◽  
Afzal Shah ◽  
Mazhar Abbas ◽  
...  

Due to a huge increase in polymer production, a tremendous increase in municipal solid waste is observed. Every year the existing landfills for disposal of waste polymers decrease and the effective recycling techniques for waste polymers are getting more and more important. In this work pyrolysis of waste polystyrene was performed in the presence of a laboratory synthesized copper oxide. The samples were pyrolyzed at different heating rates that is, 5°Cmin−1, 10°Cmin−1, 15°Cmin−1 and 20°Cmin−1 in a thermogravimetric analyzer in inert atmosphere using nitrogen. Thermogravimetric data were interpreted using various model fitting (Coats–Redfern) and model free methods (Ozawa–Flynn–Wall, Kissinger–Akahira–Sunose and Friedman). Thermodynamic parameters for the reaction were also determined. The activation energy calculated applying Coats–Redfern, Ozawa–Flynn–Wall, Kissinger–Akahira–Sunose and Friedman models were found in the ranges 105–148.48 kJmol−1, 99.41–140.52 kJmol−1, 103.67–149.15 kJmol−1 and 99.93–141.25 kJmol−1, respectively. The lowest activation energy for polystyrene degradation in the presence of copper oxide indicates the suitability of catalyst for the decomposition reaction to take place at lower temperature. Moreover, the obtained kinetics and thermodynamic parameters would be very helpful in determining the reaction mechanism of the solid waste in a real system.


Author(s):  
Ethan M. Moon ◽  
Vadim V. Yakovlev

PurposeThis paper aims to introduce and illustrate a computational technique capable of determining the geometry and complex permittivity of a supplementary dielectric insert making distributions of microwave-induced dissipated power within the processed material as uniform as possible.Design/methodology/approachThe proposed technique is based on a 3D electromagnetic model of the cavity containing both the processed material and the insert. Optimization problem is formulated for design variables (geometrical and material parameters of the insert) identified from computational tests and an objective function (the relative standard deviation [RSD]) introduced as a metric of the field uniformity. Numerical inversion is performed with the method of sequential quadratic programming.FindingsFunctionality of the procedure is illustrated by synthesis of a dielectric insert in an applicator for microwave fixation. Optimization is completed for four design variables (two geometrical parameters, dielectric constant and the loss factor of the insert) with 1,000 points in the database. The best three optimal solutions provide RSD approximately 20 per cent, whereas for the patterns corresponding to all 1,000 non-optimized (randomly chosen) sets of design variables this metric is in the interval from 27 to 136 per cent with the average of 78 per cent.Research limitations/implicationsAs microwave thermal processing is intrinsically inhomogeneous and the heating time is not a part of the underlying model, the procedure is able to lead only to a certain degree of closeness to uniformity and is intended for applications with high heating rates. The initial phase of computational identification of design variables and their bounds is therefore very important and may pre-condition the “quality” of the optimal solution. The technique may work more efficiently in combination with advanced optimization techniques dealing with “smart” (rather than random) generation of the data; for the use with more general microwave heating processes characterized by lower heating rates, the technique has to use the metric of non-uniformity involving temperature and heating time.Practical implicationsWhile the procedure can be used for computer-aided design (CAD) of microwave applicators, a related practical limitation may emerge from the fact that the material with particular complex permittivity (determined in the course of optimization) may not exist. In such cases, the procedure can be rerun for the constant values of material parameters of the available medium mostly close to the optimal ones to tune geometrical parameters of the insert. Special manufacturing techniques capable of producing a material with required complex permittivity also may be a practical option here.Originality/valueNon-uniformity of microwave heating remains a key challenge in the design of many practical applicators. This paper suggests a concept of a practical CAD and outlines corresponding computational procedure that could be used for designing a range of applied systems with high heating rates.


2019 ◽  
Vol 11 (7) ◽  
pp. 658-665
Author(s):  
Daniel Kienemund ◽  
Nicole Bohn ◽  
Thomas Fink ◽  
Mike Abrecht ◽  
Walter Bigler ◽  
...  

AbstractLow loss, ferroelectric, fully-printed varactors for high-power matching applications are presented. Piezoelectric-induced acoustic resonances reduce the power handling capabilities of these varactors by lowering the Q-factor at the operational frequency of 13.56 MHz. Here, a quality factor of maximum 142 is achieved with an interference-based acoustic suppression approach utilizing double metal–insulator–metal structures. The varactors show a tunability of maximum 34% at 300 W of input power. At a power level of 1 kW, the acoustic suppression technique greatly reduces the dissipated power by 62% from 37 W of a previous design to 14.2 W. At this power level, the varactors remain tunable with maximum 18.2% and 200 V of biasing voltage.


2020 ◽  
Vol 2020 ◽  
pp. 1-10
Author(s):  
Mohammad M. Fakharian

This paper introduces a wideband rectenna that can scavenge ambient wireless power to a range of frequency band from 0.91 GHz to 2.55 GHz efficiently. The proposed rectenna is based on a wideband 2 × 2 fractal monopole antenna array with omnidirectional radiation patterns and high gains of 5 to 8.3 dBi at the desired bands. An improved two-branch impedance matching technique is presented which is designed to enhance the rectifier circuit performance with a relatively low input power ranging from −25 dBm to 10 dBm. Also, a full-wave wideband rectifier that can suitably improve the RF-to-DC power conversion efficiency is designed for the rectenna. A peak efficiency of 76%, 71%, 61%, and 62% is obtained at 950, 1850, 2100, and 2450 MHz, respectively. Measurement results show that a conversion efficiency of 68% has been achieved over an optimal 4.7 kΩ resistor when the simultaneous four-band input power level is −10 dBm. Moreover, an output DC voltage of around 243 mV with voltage varying within 160–250 mV can be achieved by gathering the low ambient wireless power inside laboratory. This study proves that the proposed rectenna can be applied to a range of many low-power electronic applications.


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