Ion-Implantation Studies of Graphite

1982 ◽  
Vol 20 ◽  
Author(s):  
B.S. Elman ◽  
M. Hom ◽  
E.W. Maby ◽  
M.S. Dresselhaus
Keyword(s):  
Raman Spectroscopy ◽  
Elevated Temperature ◽  
Ion Implantation ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Pyrolytic Graphite ◽  
Structural Disorder ◽  
Postimplantation Annealing ◽  
Lattice Damage ◽  
Secondary Ion

ABSTRACTIon implantation of highly oriented pyrolytic graphite (HOPG) is studied using various characterization techniques, including Raman spectroscopy and Secondary Ion Mass Spectroscopy (SIMS). Particular attention is given to the annealing of the implantation-induced lattice damage using both hot substrate implantation (200 < T1< 1000°C) and postimplantation annealing. The Raman spectra provide detailed information on the implantation-induced structural disorder by analysis of the disorder-induced and Raman-allowed features in the first- and second-order spectra. SIMS measurements show that the implanted profile is essentially the same for hot substrate and room temperature implantation for the case of HOPG. It is shown that implantation at elevated temperatures prevents amorphization more effectively than implantation at room temperature and subsequent annealing at the same elevated temperature. The annealing results show that fundamentally different defects are created during room temperature and hot substrate implantation.

Magnetoreflection in Ion-Implanted Graphite

1983 ◽  
Vol 27 ◽  
Author(s):  
L.E Mcneil ◽  
B.S. Elman ◽  
M.S Dresselhaus ◽  
G. Dresselhaus ◽  
T. Venkatesan
Keyword(s):  
Raman Spectroscopy ◽  
Band Structure ◽  
Ion Implantation ◽  
Room Temperature ◽  
Electronic Band Structure ◽  
Band Model ◽  
Electronic Band ◽  
Lattice Damage ◽  
Induced Changes ◽  
Foreign Species

ABSTRACTThe use of a hot stage (T ∼ 600°C) for ion implantation into graphite permits the introduction of foreign species into the host material while eliminating most of the lattice damage associated with ion implantation at room temperature. This permits the use of the magnetoreflection technique for examination of changes in the electronic band structure induced by implantation Samples of graphite implanted with 31P and 11B at various energies and fluences are examined, and the in-plane and c-axis disorder are characterized using Raman spectroscopy and Rutherford Backscattering Spectrometer (RBS) techniques. Implantation-induced changes in the electronic band structure are interpreted in terms of the Slonczewski-Weiss- McClure band model. Small changes are found relative to the band parameters that describe pristine graphite.

Effects of Elevated Temperatures on the Compressive Strength of HFCC

2011 ◽  
Vol 261-263 ◽  
pp. 416-420 ◽  
Author(s):  
Fu Ping Jia ◽  
Heng Lin Lv ◽  
Yi Bing Sun ◽  
Bu Yu Cao ◽  
Shi Ning Ding
Keyword(s):  
Compressive Strength ◽  
Elevated Temperature ◽  
Fly Ash ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Relative Strength ◽  
Ordinary Concrete ◽  
Residual Compressive Strength ◽  
Fly Ash Concrete ◽  
The Relationship

This paper presents the results of elevated temperatures on the compressive of high fly ash content concrete (HFCC). The specimens were prepared with three different replacements of cement by fly ash 30%, 40% and 50% by mass and the residual compressive strength was tested after exposure to elevated temperature 250, 450, 550 and 650°C and room temperature respectively. The results showed that the compressive strength apparently decreased with the elevated temperature increased. The presence of fly ash was effective for improvement of the relative strength, which was the ratio of residual compressive strength after exposure to elevated temperature and ordinary concrete. The relative compressive strength of fly ash concrete was higher than those of ordinary concrete. Based on the experiments results, the alternating simulation formula to determine the relationship among relative strength, elevated temperature and fly ash replacement is developed by using regression of results, which provides the theoretical basis for the evaluation and repair of HFCC after elevated temperature.

Raman Spectra of Ion Implanted Graphite

1981 ◽  
Vol 7 ◽  
Author(s):  
B.S. Elman ◽  
H. Mazurek ◽  
M.S. Dresselhaus ◽  
G. Dresselhaus
Keyword(s):  
Raman Spectroscopy ◽  
Ion Implantation ◽  
Raman Spectra ◽  
Annealing Temperature ◽  
Annealing Process ◽  
Lattice Order ◽  
Annealing Temperatures ◽  
High Fluences ◽  
Lattice Damage ◽  
The Way

ABSTRACTRaman spectroscopy is used in a variety of ways to monitor different aspects of the lattice damage caused by ion implantation into graphite. Particular attention is given to the use of Raman spectroscopy to monitor the restoration of lattice order by the annealing process, which depends critically on the annealing temperature and on the extent of the original lattice damage. At low fluences the highly disordered region is localized in the implanted region and relatively low annealing temperatures are required, compared with the implantation at high fluences where the highly disordered region extends all the way to the surface. At high fluences, annealing temperatures comparable to those required for the graphitization of carbons are necessary to fully restore lattice order.

Experimental Study on the Mechanical Property and Forming Limit of Magnesium Sheet at Elevated Temperatures

2009 ◽  
Author(s):  
Y. Huang ◽  
J. Huang ◽  
J. Cao
Keyword(s):  
Elevated Temperature ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Strain Curve ◽  
Tensile Tests ◽  
Alloy Sheet ◽  
Dome Height ◽  
Forming Limit ◽  
Uniaxial Tensile ◽  
Magnesium Sheet

Magnesium alloy sheet has received increasing attention in automotive and aerospace industries. It is widely recognized that magnesium sheet has a poor formability at room temperature. While at elevated temperature, its formability can be dramatically improved. Most of work in the field has been working with the magnesium sheet after annealed around 350°C. In this paper, the as-received commercial magnesium sheet (AZ31B-H24) with thickness of 2mm has been experimentally studied without any special heat treatment. Uniaxial tensile tests at room temperature and elevated temperature were first conducted to have a better understanding of the material properties of magnesium sheet (AZ31B-H24). Then, limit dome height (LDH) tests were conducted to capture forming limits of magnesium sheet (AZ31B-H24) at elevated temperatures. An optical method has been introduced to obtain the stress-strain curve at elevated temperatures. Experimental results of the LDH tests were presented.

scholarly journals Application of a √ area -Approach for Fatigue Assessment of Cast Aluminum Alloys at Elevated Temperature

Metals ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 1033 ◽  
Author(s):  
Roman Aigner ◽  
Christian Garb ◽  
Martin Leitner ◽  
Michael Stoschka ◽  
Florian Grün
Keyword(s):  
Elevated Temperature ◽  
Fatigue Strength ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Damage Mechanism ◽  
Cyclic Fatigue ◽  
Fatigue Tests ◽  
Cast Aluminum ◽  
Fatigue Assessment ◽  
Cast Aluminum Alloys

This paper contributes to the effect of elevated temperature on the fatigue strength of common aluminum cast alloys EN AC-46200 and EN AC-45500. The examination covers both static as well as cyclic fatigue investigations to study the damage mechanism of the as-cast and post-heat-treated alloys. The investigated fracture surfaces suggest a change in crack origin at elevated temperature of 150 ∘ C. At room temperature, most fatigue tests reveal shrinkage-based micro pores as their crack initiation, whereas large slipping areas occur at elevated temperature. Finally, a modified a r e a -based fatigue strength model for elevated temperatures is proposed. The original a r e a model was developed by Murakami and uses the square root of the projected area of fatigue fracture-initiating defects to correlate with the fatigue strength at room temperature. The adopted concept reveals a proper fit for the fatigue assessment of cast Al-Si materials at elevated temperatures; in detail, the slope of the original model according to Murakami should be decreased at higher temperatures as the spatial extent of casting imperfections becomes less dominant at elevated temperatures. This goes along with the increased long crack threshold at higher operating temperature conditions.

Impurity Profiles in InP from Ion Implantation at Elevated Temperatures

1991 ◽  
Vol 240 ◽  
Author(s):  
P. Kringhoj ◽  
B. G. Svensson
Keyword(s):  
Mass Spectrometry ◽  
Ion Implantation ◽  
Elevated Temperatures ◽  
Secondary Ion Mass Spectrometry ◽  
Implantation Damage ◽  
Ion Mass Spectrometry ◽  
Chemical Profiles ◽  
Impurity Profiles ◽  
Secondary Ion

ABSTRACTThe chemical profiles of Zn, Ge, and Se implanted into InP at elevated temperatures have been measured with secondary ion mass spectrometry and correlated to the implantation damage as deduced from RBS/channeling measurements. An asymmetric broadening of the chemical profiles towards the bulk was found for implantation temperatures above 150°C. This effect is concluded to be due to impurity channeling during implantation.

Sliding Behavior of Alumina/Nickel and Alumina/Nickel Aluminide Couples at Room and Elevated Temperature

1988 ◽  
Vol 110 (4) ◽  
pp. 646-652 ◽  
Author(s):  
Peter J. Blau ◽  
Charles E. DeVore
Keyword(s):  
Elevated Temperature ◽  
Friction Coefficient ◽  
Nickel Aluminide ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Sliding Friction ◽  
Surface Damage ◽  
Polycrystalline Alumina ◽  
Ordered Intermetallic ◽  
Pin On Disk

Nickel aluminide alloys are ordered intermetallic compounds which show promise for elevated temperature applications, some of which involve sliding contact. The present investigation was conducted to develop an initial understanding of the unlubricated sliding behavior of a nickel aluminide alloy at room and elevated temperatures. In particular, the variations in the friction coefficient and the wear track morphology during the break-in stage and subsequent transitions were studied. Pin-on-disk experiments were conducted at room temperature and at 650° C (923° K) in air using fixed 9.5 mm diameter polycrystalline alumina balls as the pin material. To provide a comparison in behavior, nickel (Ni-200) disks were tested under the same conditions. The sliding friction coefficient of alumina on nickel aluminide was considerably higher than that for alumina on nickel at room temperature, but it was only slightly higher at 650° C. The wear was similar for both materials at room temperature, but the nickel aluminide exhibited relatively mild wear at 650° C, displaying less severe surface damage than the nickel. Work on identifying key friction and wear mechanisms and on evaluating the temperature limitations for future applications will continue.

Oxide Scale Formation on Iron-Chromium Alloys in Elevated Temperature Air Environments

CORROSION ◽  
1981 ◽  
Vol 37 (12) ◽  
pp. 700-711 ◽  
Author(s):  
P. Fabis ◽  
R. Heidersbach ◽  
C. Brown ◽  
T. Rockett
Keyword(s):  
Raman Spectroscopy ◽  
Room Temperature ◽  
Elevated Temperatures ◽  
Experimental Program ◽  
Oxide Scales ◽  
Chromium Alloys ◽  
Spectroscopy Instrumentation ◽  
Commercial Iron ◽  
Iron Chromium

Abstract Oxide scales formed on metals at elevated temperatures may be different, both chemically and structurally, from the scales on the metal once it has cooled to room temperature. This paper discusses Raman spectroscopy instrumentation for the in-situ identification of scales formed on metal surfaces exposed to gaseous environments. The results of an experimental program to characterize scales formed on two commercial iron-chromium alloys, AISI 446 and 502, in air and oxygen environments are also presented.

Tribological Behavior of DLC Films by RF-PECVD at the Elevated Temperature

2007 ◽  
Vol 353-358 ◽  
pp. 1781-1784
Author(s):  
Yong Kyung Cho ◽  
Yun Ha Shin ◽  
Sung Hoon Jeong ◽  
Young Ze Lee
Keyword(s):  
Raman Spectroscopy ◽  
Elevated Temperature ◽  
Vapor Deposition ◽  
Room Temperature ◽  
Tribological Behavior ◽  
Chemical Vapor ◽  
Diamond Like Carbon ◽  
Radio Frequency Plasma ◽  
Frequency Plasma ◽  
Higher Temperature

The tribological behaviors of Diamond-like carbon (DLC) films, prepared by the radio frequency plasma enhanced chemical vapor deposition (RF-PECVD) method, were studied in the room temperature and the elevated temperature. The ball-on-disk tests with DLC films on steel specimens were conducted at a sliding speed of 60 rpm, a load of 10 N, and surrounding temperatures of 25°C and 75°C. The results show that the coefficients of friction and the amounts of wear of DLC films were decreased at higher temperature. After tests the wear tracks of hydrogenated DLC film were analyzed by Raman spectroscopy.

GaN P-N Structures Fabricated by Mg ION Implantation

1998 ◽  
Vol 537 ◽  
Author(s):  
E.V. Kalinina ◽  
V.A. Solov'ev ◽  
A.S. Zubrilov ◽  
V.A. Dmitriev ◽  
A.P. Kovarsky
Keyword(s):  
Ion Implantation ◽  
Room Temperature ◽  
Implantation Dose ◽  
Electrical Characteristics ◽  
Scattered Electron ◽  
Current Voltage ◽  
Capacitance Voltage ◽  
Electron Beam Induced Current ◽  
P Type ◽  
Secondary Ion

AbstractIn this paper we report on the first GaN p-n diodes fabricated by Mg ion implantation doping of n-type GaN epitaxial layers. Ion implantation was performed at room temperature. Implantation dose ranged from 1013 to 2 × 1016 cm2. After implantation samples were annealed for 10-15 s at a wide temperature interval from 600°C to 1200°C in flowing N2 to form p-type layers. Secondary ion mass spectroscopy, scanning electron microscopy with electron beam induced current and back scattered electron modes as well as current-voltage and capacitance-voltage measurements were used to study structural and electrical characteristics of the Mg implanted p-n structures.

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