Fracture Processes in Fully Crystallized Co84Nb10B6 Metallic Glass

1985 ◽  
Vol 58 ◽  
Author(s):  
Janez Megusar ◽  
Tina Vargas ◽  
Nicholas J. Grant

ABSTRACTFracture processes have been studied in a fully crystallized Co84Nb10B6 glass, with the mean grain size ranging from 43 nm to 0.65 μm. Tensile tested specimens with a mean grain size≥ 0.3 μm showed a ductile (dimple) fracture with microvoids initiated at the boride-cobalt matrix interfaces. As the mean grain size (more correctly, the corresponding mean free path of the deforming cobalt phase) was ≤ 0.1 μm, the fracture process may be similarly initiated by the microvoid formation at the boride-cobalt interface. However, one-to-one correspondence between dimples and boride particles may not be preserved. As a result, dimples become more shallow and may include several boride particles instead. Although the fracture surface of the brittle fine grained Co84Nb10B6 alloy gives an appearance of a cleavage fracture on a macroscale, it is distinctly different, by allowing for the microvoid formation on a microscale.


2021 ◽  
Vol 56 (19) ◽  
pp. 11237-11247 ◽  
Author(s):  
Johannes Pötschke ◽  
Manisha Dahal ◽  
Mathias Herrmann ◽  
Anne Vornberger ◽  
Björn Matthey ◽  
...  

AbstractDense (Hf, Ta, Nb, Ti, V)C- and (Ta, Nb, Ti, V, W)C-based high-entropy carbides (HEC) were produced by three different sintering techniques: gas pressure sintering/sinter–HIP at 1900 °C and 100 bar Ar, vacuum sintering at 2250 °C and 0.001 bar as well as SPS/FAST at 2000 °C and 60 MPa pressure. The relative density varied from 97.9 to 100%, with SPS producing 100% dense samples with both compositions. Grain size measurements showed that the substitution of Hf with W leads to an increase in the mean grain size of 5–10 times the size of the (Hf, Ta, Nb, Ti, V,)C samples. Vacuum-sintered samples showed uniform grain size distribution regardless of composition. EDS mapping revealed the formation of a solid solution with no intermetallic phases or element clustering. X-ray diffraction analysis showed the structure of mostly single-phase cubic high-entropy carbides. Hardness measurements revealed that (Hf, Ta, Nb, Ti, V)C samples possess higher hardness values than (Ta, Nb, Ti, V, W)C samples.



Minerals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 653
Author(s):  
Shereef Bankole ◽  
Dorrik Stow ◽  
Zeinab Smillie ◽  
Jim Buckman ◽  
Helen Lever

Distinguishing among deep-water sedimentary facies has been a difficult task. This is possibly due to the process continuum in deep water, in which sediments occur in complex associations. The lack of definite sedimentological features among the different facies between hemipelagites and contourites presented a great challenge. In this study, we present detailed mudrock characteristics of the three main deep-water facies based on sedimentological characteristics, laser diffraction granulometry, high-resolution, large area scanning electron microscopy (SEM), and the synchrotron X-ray diffraction technique. Our results show that the deep-water microstructure is mainly process controlled, and that the controlling factor on their grain size is much more complex than previously envisaged. Retarding current velocity, as well as the lower carrying capacity of the current, has an impact on the mean size and sorting for the contourite and turbidite facies, whereas hemipelagite grain size is impacted by the natural heterogeneity of the system caused by bioturbation. Based on the microfabric analysis, there is a disparate pattern observed among the sedimentary facies; turbidites are generally bedding parallel due to strong currents resulting in shear flow, contourites are random to semi-random as they are impacted by a weak current, while hemipelagites are random to oblique since they are impacted by bioturbation.





Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 334
Author(s):  
Aidong Xia ◽  
Jie Yin ◽  
Xiao Chen ◽  
Zhengren Huang ◽  
Xuejian Liu ◽  
...  

In this work, a (SiC-AlN)/ZrB2 composite with outstanding mechanical properties was prepared by using polymer-derived ceramics (PDCs) and hot-pressing technique. Flexural strength reached up to 460 ± 41 MPa, while AlN and ZrB2 contents were 10 wt%, and 15 wt%, respectively, under a hot-pressing temperature of 2000 °C. XRD pattern-evidenced SiC generated by pyrolysis of polycarbosilane (PCS) was mainly composed by 2H-SiC and 4H-SiC, both belonging to α-SiC. Micron-level ZrB2 secondary phase was observed inside the (SiC-AlN)/ZrB2 composite, while the mean grain size (MGS) of SiC-AlN matrix was approximately 97 nm. This unique nano-micron hybrid microstructure enhanced the mechanical properties. The present investigation provided a feasible tactic for strengthening ceramics from PDCs raw materials.



2013 ◽  
Vol 634-638 ◽  
pp. 1807-1810
Author(s):  
Guang Xu ◽  
Jing Yang ◽  
Tao Xiong ◽  
Peng Deng ◽  
Long Fei Cao

Sub-nano structured steel was obtained by cold rolling and annealing martensite microstructure for a plain carbon steel. The mean grain size is several hundreds nanometer. The steel has very high strength and also good total elongation.



2005 ◽  
Vol 37 (1) ◽  
pp. 55-60 ◽  
Author(s):  
V.V. Ivanov ◽  
S.Y. Ivin ◽  
V.R. Khrustov ◽  
Y.A. Kotov ◽  
A.M. Murzakaev ◽  
...  

Gasproof thin-wall tubes of fine-grained ceramics based on zirconia and gadolinia have been produced by magnetic pulsed compaction and thermal sintering. Data on their structures and electric characteristics are presented. The tubes with a diameter of ~ 15 mm, wall thickness of ~ 0.7 mm, and length up to 80 mm are characterized by an uniform porous-free structure with a mean grain size in the range of 100 - 300 nm. The obtained ceramics possess high electrolytic properties.



1970 ◽  
Vol 14 ◽  
pp. 35-42 ◽  
Author(s):  
Danda Pani Adhikari

A 17.63 m long bore-hole core extracted from the deepest part of Lake Yamanaka, one of the Fuji-five Lakes at the northeasternfoot of Mount Fuji, central Japan, composed of sediment with intercalations of scoria fallout deposits. The sediment of the upper11.4 m was investigated for grain-size distribution by using a laser diffraction particle size analyser. The mean grain-size profileshowed various degrees of fluctuations, both short-and long-terms, and the size-frequency distribution revealed unimodal-trimodalmixing of sediments. Changes in lake size and water depth appear to be the main factors affecting the variability in the grain-sizedistribution and properties. The lake level appears low during 7000–5000 cal BP and 2800–1150 cal BP and relatively high during5000–2800 cal BP and 1150 cal BP– present.DOI: http://dx.doi.org/10.3126/bdg.v14i0.5437Bulletin of the Department of Geology Vol.14 2011, pp.35-42 



2010 ◽  
Vol 667-669 ◽  
pp. 457-461
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Tao Peng ◽  
Xin Tao Liu ◽  
...  

Cyclic channel die compression (CCDC) of AZ31-1.7 wt.% Si alloy was performed up to 5 passes at 623 K in order to investigate the microstructure and mechanical properties of compressed alloys. The results show that multi-pass CCDC is very effective to refine the matrix grain and Mg2Si phases. After the alloy is processed for 5 passes, the mean grain size decreases from 300 μm of as-cast to 8 μm. Both dendritic and Chinese script type Mg2Si phases break into small polygonal pieces and distribute uniformly in the matrix. The tensile strength increases prominently from 118 MPa to 216 MPa, whereas the hardness of alloy deformed 5 passes only increase by 8.4% compared with as-cast state.



2017 ◽  
Vol 35 (5) ◽  
pp. 2079-2105 ◽  
Author(s):  
Leila Hazout ◽  
Zein El-Abidine Zitouni ◽  
Mostefa Belkhatir ◽  
Tom Schanz


2010 ◽  
Vol 150-151 ◽  
pp. 1358-1363
Author(s):  
Bin Fang ◽  
Chuan Zhen Huang ◽  
Chong Hai Xu ◽  
Sheng Sun

The fabrication is a key process for the preparation of ceramic tool materials, which governs the mechanical properties of ceramic tool materials under the condition of the same compositions. A computer simulation coupled with fabrication temperature for the hot-pressing process of single-phase ceramic tool materials has been developed using a two-dimensional hexagon lattice model mapped from the realistic microstructure without considering the presence of pores. The fabrication of single-phase Al2O3 is simulated. The mean grain size of simulated microstructure by Monte Carlo Potts model integrated with fabrication temperature increases with an increase in fabrication temperature, which is consistent with the experiment results.



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