scholarly journals Effect of Heating Rate and Annealing Temperature on Secondary Recrystallization of Goss Grains in a Grain Orientated Silicon Steel

2017 ◽  
Vol 57 (6) ◽  
pp. 1112-1120 ◽  
Author(s):  
Fatayalkadri Citrawati ◽  
Md Zakaria Quadir ◽  
Paul Richard Munroe
2007 ◽  
Vol 558-559 ◽  
pp. 747-750 ◽  
Author(s):  
Kyu Seok Han ◽  
Jong Tae Park ◽  
Jae Kwan Kim ◽  
Jerzy A. Szpunar

Recrystallization texture in grain oriented silicon steel at different annealing temperature is investigated. Normalized x-ray intensities of various orientation components observed in Orientation Distribution Function are used for comparison. The computed CSL boundary distributions about Goss component with annealing condition were calculated. The misorientation angle distribution is also measured in order to find the importance of high-energy boundary with misorientation 20~45° range for the secondary recrystallization of Goss grain. From the analysis of CSL boundary distribution and misorienation angle distribution, the distribution of CSL boundaries does not evidently show any preferred difference between Goss and other texture components. Whereas, the misorientation angle analysis shows that the number of 20°~45° misoriented boundaries is higher around the Goss grains than around other texture components.


2019 ◽  
Vol 944 ◽  
pp. 199-204
Author(s):  
Xiang Lu ◽  
Meng Fei Lan ◽  
Feng Fang ◽  
Yuan Xiang Zhang ◽  
Yang Wang ◽  
...  

Grain-oriented silicon steel was produced by strip casting route. The effect of different annealing temperature on primary annealing and secondary annealing was investigated. The result showed that the average grain diameter increased and the grain uniformity was gradually destroyed with the increasing annealing temperature. Regardless of annealing temperature, the primary texture consisted of strong γ-fiber and weak λ-fiber. With the increase of annealing temperature, the γ-fiber intensity increased. In addition, the Goss component was not shown at 780-880 °C but appeared at 980 °C. After secondary annealing, complete abnormal grain growth occurred in all samples and the average grain diameter increased with the primary annealing temperature. The Goss sharpness of secondary grains firstly increased and then decreased with a peak value obtained at 830 °C. This result was explained in terms of the combination of the inhibiting force, primary grain diameter and primary texture.


2016 ◽  
Vol 2016 ◽  
pp. 1-6
Author(s):  
Zhi-chao Li ◽  
Ning Dang ◽  
Zhen-li Mi

OM (optical microscopy) and EBSD (electron backscatter diffraction) techniques were used to study microstructure and texture distribution during primary recrystallization under different intermediate annealing temperatures in CGO silicon steels. The effect of intermediate annealing temperature on texture distribution in 3% Si electrical steel was analyzed. The results indicate that the microstructure in primary recrystallization matrix of CGO silicon steel is comprised of equiaxed ferrite grains. Mean grain size of primary recrystallization increases with the rising of intermediate annealing temperature.γ-fiber texture is the dominant component in primary recrystallization matrix. With higher intermediate annealing temperature,111121texture and111110texture increase and111121texture is stronger than111110texture. Goss texture was observed to be decreased firstly and then increased. The content of high angle grain boundaries in primary recrystallization matrix are affected by intermediate annealing temperature. When intermediate annealing temperature is increased, high angle grain boundaries are increased firstly and then decreased. Misorientation distribution in primary recrystallized matrix is affected by primary recrystallization annealing temperature either. The content of high angle grain boundaries are increased owing to higher primary recrystallization annealing temperature, which can be a benefit to the abnormal growth of Goss grains in secondary recrystallization.


2016 ◽  
Vol 879 ◽  
pp. 350-355
Author(s):  
Fatayalkadri Citrawati ◽  
Md Zakaria Quadir ◽  
Paul Munroe

In this study the effects of heating rate on the sharpness and size of Goss oriented ({110}<001>) grains during secondary recrystallization annealing at 900 °C was observed. The results show that, at the same annealing temperature, rapid heating of the samples to this temperature generates a higher drag force compared to a slower heating rate (5°C/min). The two groups of samples show different growth kinetics for Goss grains, in which at the longest annealing time, the rapid heating sample exhibits larger maximum Goss grain size compared to the slower heated samples.


2020 ◽  
Vol 117 (6) ◽  
pp. 607
Author(s):  
Lifeng Fan ◽  
Xingyuan Zhao ◽  
Rong Zhu ◽  
Jianzhong He ◽  
Yuan Xiang Zhang

A grain-oriented silicon steel sheet was manufactured by slab reheated at “medium temperature” and two-stage cold rolling method. The function of heating rate on secondary recrystallization in grain-oriented silicon steel was investigated. The results show that: compared with 30 °C/h heating rate, the initial temperature of the secondary recrystallization can increase by 10 °C at the heating rate of 20 °C/h. Furthermore, the temperature region of secondary recrystallization also extended either with the increased heating rate. Even though the inhibitors maintain AlN, complex precipitation of AlN and sulphide in both heating rate, the average diameter and Zener factor of inhibitors are distinct. Inhibitors in the route of 20 °C/h heating rate express stronger inhibition than that of 30 °C/h, and the average diameter and Zener factor are 17.519 nm and 3.925 × 10−4 nm−1, respectively. In addition, more Goss texture component and less γ-fiber texture ({111}//ND) component form at the heating rate of 30 °C/h than 20 °C/h at 1000 °C, but the final Goss texture component of 20 °C/h is greater than 30 °C/h. The average grain size of the final annealing sheets increased with the heating rate decreasing from 30 °C/h to 20 °C/h, and iron loss reduced by 0.05 W/Kg, the magnetic induction intensity increased by 0.025 T.


1999 ◽  
Vol 32 (1-4) ◽  
pp. 119-136
Author(s):  
Jong Soo Woo ◽  
Chan-Hee Han ◽  
Byung-Deug Hong ◽  
Jirou Harase

Primary recrystallized Fe–3%Si specimens containing AI and nitrided were annealed intermittently with the heating rate of 15℃/h in 100% N2 atmosphere. The magnetic induction B8 was measured after each annealing. The onset of secondary recrystallization was detected by the rapid rise of B8. The maximum B8 obtained was about 1.94 T when the onset temperature of the secondary recrystallization was around 1075℃ regardless of the initial grain size or nitrogen content.The same primary specimens were coated with MgO and annealed with the same heating rate in 5% H2–N2. The maximum B8 obtained was nearly same as with the above annealing condition, however, the initial grain size and nitrogen content was quite contrary in this annealing. The difference in the optimum grain size and nitrogen content for obtaining the highest B8 between both annealings was explained on the assumption that ∑9 boundaries become most mobile at 1075℃ regardless of the annealing methods. Based on this finding, the possibility of producing grain oriented silicon steel without hot band annealing and nitriding treatment was shown.


Materials ◽  
2021 ◽  
Vol 14 (4) ◽  
pp. 1024
Author(s):  
Jingjing Peng ◽  
Changshan Hao ◽  
Hongyan Liu ◽  
Yue Yan

Highly transparent indium-free multilayers of TiO2/Cu/TiO2 were obtained by means of annealing. The effects of Cu thickness and annealing temperature on the electrical and optical properties were investigated. The critical thickness of Cu mid-layer with optimal electrical and optical properties was 10 nm, with the figure of merit reaching as high as 5 × 10−3 Ω−1. Partial crystallization of the TiO2 layer enhanced the electrical and optical properties upon annealing. Electrothermal experiments showed that temperatures of more than 100 °C can be reached at a heating rate of 2 °C/s without any damage to the multilayers. The experimental results indicate that reliable transparent TiO2/Cu/TiO2 multilayers can be used for electrothermal application.


Metals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1655
Author(s):  
Xin Tian ◽  
Shuang Kuang ◽  
Jie Li ◽  
Jing Guo ◽  
Yunli Feng

An Nb-containing grain-oriented silicon steel was produced through double-stage cold rolling in order to investigate the effect of the heating rate during intermediate annealing on primary recrystallization and decarburization behavior. The microstructure and texture were observed and analyzed by an optical microscope and an electron backscatter diffraction system. A transmission electron microscope was used to observe the precipitation behavior of inhibitors. The decarburization effect during intermediate annealing was also calculated and discussed. The results show that primary recrystallization takes place after intermediate annealing. As the heating rate increases, the average grain size decreases gradually. The textures of {411}<148> and {111}<112> were found to be the strongest along the thickness direction in all of the annealed specimens and are mainly surrounded by HEGB and HAGB (> 45°). A large number of inhibitors with the size of 14~20 nm precipitate are distributed evenly in the matrix. The above results indicate that the higher heating rate during intermediate annealing contributes to both an excellent microstructure and magnetic properties. From the calculation, as the heating rate increases, decarbonization tends to proceed in the insulation stage, and the total amount of carbonization declines.


2013 ◽  
Vol 753 ◽  
pp. 337-340 ◽  
Author(s):  
Yoshiyuki Ushigami ◽  
Yoshihiro Arita ◽  
Kohsaku Ushioda

It has been observed that grain size of Goss secondary grain has a strong correlation with deviation angle from the exact Goss orientation and sharper Goss grain has larger grain diameter. This orientation selectivity of secondary recrystallization has been investigated with the statistical model of grain growth in which inhibitor and texture are taken into account. The model assumes that sharper Goss grain has a higher frequency of CSL boundaries to the matrix grains and thus has lower statistical grain boundary energy and suffers lower pinning force from the inhibitor. The analysis showed that this model successfully explains orientation selectivity and depicts the effect of inhibitor and texture.


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