scholarly journals Research on the Microstructures and Mechanical Properties of Bainite/Martensite Rail Treated by the Controlled-Cooling Process

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3061 ◽  
Author(s):  
Jiajia Qiu ◽  
Min Zhang ◽  
Zhunli Tan ◽  
Guhui Gao ◽  
Bingzhe Bai

A bainite/martensite multiphase rail is treated by the controlled-cooling process with different finish-cooling temperatures. The simulated temperature–time curves of the position of 5 mm and 15 mm below the rail tread (P5 and P15) express different trends. P5 has greater impact toughness and lower tensile strength than P15. Microstructural characterization was carried out by conducting scanning electron microscopy, X-ray diffraction, electron backscatter diffraction, and transmission electron microscopy. The greater tensile strength is due to the dispersed ε-carbides hindering the movement of dislocations. The greater impact toughness is attributed to the filmy retained austenite and the smaller effective grain with high-angle boundary. Finite element modeling (FEM) and microstructural characterization reasonably explain the changes of mechanical properties. The present work provides experimental and theoretical guidance for the development of rail with excellent mechanical properties.

2010 ◽  
Vol 163-167 ◽  
pp. 337-341 ◽  
Author(s):  
Liang Yun Lan ◽  
Chun Lin Qiu ◽  
De Wen Zhao

The nucleation and crystallographic characteristics of acicular ferrite in the as-rolled and tempered steel were investigated by using an optical microscopy (OM), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) equipped with electron backscatter diffraction (EBSD). The results showed that acicular ferrite forms at nucleation sites such as dislocations within austenite grains under the heavy reduction in the austensite non-recrystallization region and accelerated cooling conditions, and the inclusions such as Al2O3•MnS may have promotion effect for the formation of acicular ferrite. Acicular ferrite has high misorientation angle boundaries and a number of sub-boundaries or high density of dislocations inside, which contributes to an excellent combination of high strength and toughness. And the morphology of acicular ferrite does not show obvious change in tempering microstructure due to high temperature thermal stability, which plays an important part in keeping good mechanical properties for tempered specimens.


Author(s):  
S. Fujishiro

The mechanical properties of three titanium alloys (Ti-7Mo-3Al, Ti-7Mo- 3Cu and Ti-7Mo-3Ta) were evaluated as function of: 1) Solutionizing in the beta field and aging, 2) Thermal Mechanical Processing in the beta field and aging, 3) Solutionizing in the alpha + beta field and aging. The samples were isothermally aged in the temperature range 300° to 700*C for 4 to 24 hours, followed by a water quench. Transmission electron microscopy and X-ray method were used to identify the phase formed. All three alloys solutionized at 1050°C (beta field) transformed to martensitic alpha (alpha prime) upon being water quenched. Despite this heavily strained alpha prime, which is characterized by microtwins the tensile strength of the as-quenched alloys is relatively low and the elongation is as high as 30%.


2009 ◽  
Vol 24 (3) ◽  
pp. 647-651 ◽  
Author(s):  
M. Rester ◽  
C. Motz ◽  
R. Pippan

Electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) analyses of small indentations in copper single crystals exhibit only slight changes of the crystal orientation in the surroundings of the imprints. Far-reaching dislocations might be the reason for these small misorientation changes. Using EBSD and TEM technique, this work makes an attempt to visualize the far-propagating dislocations by introducing a twin boundary in the vicinity of small indentations. Because dislocations piled up at the twin boundary produce a misorientation gradient, the otherwise far-propagating dislocations can be detected.


2021 ◽  
Vol 1026 ◽  
pp. 84-92
Author(s):  
Tao Qian Cheng ◽  
Zhi Hui Li

Al-Zn-Mg-Cu alloy have been widely used in aerospace industry. However, there is still a lack of research on thermal stability of Al-Zn-Mg-Cu alloy products. In the present work, an Al-Zn-Mg-Cu alloy with T79 and T74 states was placed in the corresponding environment for thermal exposure experiments. Performance was measured by tensile strength, hardness and electrical conductivity. In this paper, precipitation observation was analyzed by transmission electron microscopy (TEM) and high-resolution transmission electron microscopy (HREM). The precipitations of T79 state alloy were GPⅡ zone, η' phase and η phase while the ultimate tensile strength, hardness and electrical conductivity were 571MPa, 188.2HV and 22.2MS×m-1, respectively. The mechanical property of T79 state alloy decreased to 530MPa and 168.5HV after thermal exposure. The diameter of precipitate increased and the precipitations become η' and η phase at the same time. During the entire thermal exposure, T74 state alloy had the same mechanical property trend as T79 state alloy. The precipitate diameter also increased while the types of precipitate did not change under thermal exposure. The size of precipitates affected the choice of dislocation passing through the particles to affect the mechanical properties.


2021 ◽  
Author(s):  
Olga Ageeva ◽  
Ge Bian ◽  
Gerlinde Habler ◽  
Rainer Abart

<p>Magnetite micro-inclusions in silicate minerals are important carriers of the remanent magnetization of rocks. Their shape orientation relationships (SOR) and crystallographic orientation relationships (COR) to the host crystal are of interest in the context of the bulk magnetic properties of the inclusion-host assemblage. We investigated the SOR and COR of magnetite (MT) micro-inclusions in plagioclase (PL) from oceanic gabbro using correlated optical microscopy, scanning electron microscopy, Electron backscatter diffraction analysis and Transmission electron microscopy.</p><p>In the mm-sized PL crystals of the investigated gabbros MT is present as equant, needle- and lath-shaped (sub)micrometer sized inclusions. More than 95% of the needle-shaped inclusions show SOR and specific COR to the plagioclase host. Most of the needles are elongated perpendicular to one of the MT{111} planes, which is aligned parallel to one of the (112), (1-12), (-312), (-3-12), (150), (1-50) or (100) planes of plagioclase. These inclusions are classified as “plane-normal type”. The needle elongation parallel to MT<111>, which is the easy direction of magnetization, ensures high magnetic susceptibility of these inclusions. The underlying formation mechanism is related to the parallel alignment of oxygen layers with similar lattice spacing across the MT-PL interfaces that are parallel to the elongation direction [1].</p><p>Apart from the SOR and the alignment of a MT{111} with one of the PL low index planes, the MT crystals rotate about the needle elongation direction. The rotation angles are statistically distributed with several maxima representing specific orientation relationships. In some cases one of the MT<001> axes is aligned with PL[14 10 7] or PL[-14 10 -7], which ensures that FeO<sub>6 </sub>octahedra of MT well fit into channels // [001] of PL, which are formed by six membered rings of SiO<sub>4</sub> and AlO<sub>4</sub> tetrahedra [2]. This COR is referred to as the “nucleation orientation” of magnetite with respect to PL. There are several other possibilities to fit FeO<sub>6</sub> octahedra into the [001] channels of PL, but the alignment stated above allows for the additional parallel alignment of one of the MT{111} with one of the above mentioned low index lattice planes of PL. MT crystals with one of these nucleation orientations can undergo directional growth to develop laths and needles. MT crystals with other nucleation orientations that do not allow for the parallel alignment of MT{111} with the above mentioned PL lattice planes, do not significantly grow and form the equant inclusions.</p><p>For some needles one or more of the MT{011} planes that are parallel to the needle elongation direction, are aligned with low-index planes of plagioclase such as PL (112), PL(150), PL(1-50) etc., and form MT facets. This situation corresponds to achievement of the best possible match between the two crystal lattices. This can either be generated during primary growth or during re-equilibration of the micro-inclusions and the plagioclase host.</p><p>Funding by RFBR project 18-55-14003 and Austrian Science fund (FWF): I 3998-N29 is acknowledged.</p><p>Reference</p><p>[1] Ageeva et al (2020) Contrib. Mineral. Petrol. 175(10), 1-16.</p><p>[2] Wenk et al (2011) Am. Min. 96, 1316-1324</p>


Materials ◽  
2020 ◽  
Vol 13 (17) ◽  
pp. 3869
Author(s):  
Mengmeng Wang ◽  
Jiang Ju ◽  
Jingjing Li ◽  
Yang Zhou ◽  
Haiyang Lv ◽  
...  

A periodic-layered structure was observed in solid-(Cr, Fe)2B/liquid-Al diffusion couple at 750 °C. The interface morphology, the reaction products, and the potential formation mechanism of this periodic-layered structure were investigated using an electron probe microanalyzer (EPMA), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), transmission electron microscopy (TEM), and energy-dispersive spectroscopy (EDS). The results indicate that the reaction between (Cr, Fe)2B and liquid Al is a diffusion-controlled process. The formation of intermetallics involves both the superficial dissolution of Fe and Cr atoms and the inward diffusion of Al at the interface. The layered structure, as characterized by various experimental techniques, is alternated by a single FeAl3 layer and a (FeAl3 + Cr3AlB4) dual-phase layer. A potential mechanism describing the formation process of this periodic-layered structure was proposed based on the diffusion kinetics based on the experimental results.


2007 ◽  
Vol 539-543 ◽  
pp. 4375-4380
Author(s):  
Dagoberto Brandão Santos ◽  
Élida G. Neves ◽  
Elena V. Pereloma

The multiphase steels have complex microstructures containing polygonal ferrite, martensite, bainite, carbide and a small amount of retained austenite. This microstructure provides these steels with a high mechanical strength and good ductility. Different thermal cycles were simulated in the laboratory in order to create the microstructures with improved mechanical properties. The samples were heated to various annealing temperatures (740, 760 or 780°C), held for 300 s, and then quickly cooled to 600 or 500°C, where they were soaked for another 300 s and then submitted to the accelerated cooling process, with the rates in the range of 12-30°C/s. The microstructure was examined at the end of each processing route. The mechanical behavior evaluation was made by microhardness testing. The microstructural characterization involved optical microscopy (OM), X-ray diffraction (XRD), scanning electron microscopy (SEM) with electron backscattering diffraction (EBSD) and transmission electron microscopy (TEM). The use of multiple regression analysis allowed the establishment of quantitative relationship between the microstructural parameters, cooling rates and mechanical properties of the steel.


Minerals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1018
Author(s):  
Sejin Jung ◽  
Takafumi Yamamoto ◽  
Jun-ichi Ando ◽  
Haemyeong Jung

Amphibole peridotite samples from Åheim, Norway, were analyzed to understand the deformation mechanism and microstructural evolution of olivine and amphibole through the Scandian Orogeny and subsequent exhumation process. Three Åheim amphibole peridotite samples were selected for detailed microstructural analysis. The Åheim amphibole peridotites exhibit porphyroclastic texture, abundant subgrain boundaries in olivine, and the evidence of localized shear deformation in the tremolite-rich layer. Two different types of olivine lattice preferred orientations (LPOs) were observed: B- and A-type LPOs. Electron backscatter diffraction (EBSD) mapping and transmission electron microscopy (TEM) observations revealed that most subgrain boundaries in olivine consist of dislocations with a (001)[100] slip system. The subgrain boundaries in olivine may have resulted from the deformation of olivine with moderate water content. In addition, TEM observations using a thickness-fringe method showed that the free dislocations of olivine with the (010)[100] slip system were dominant in the peridotites. Our data suggest that the subgrain boundaries and free dislocations in olivine represent a product of later-stage deformation associated with the exhumation process. EBSD mapping of the tremolite-rich layer revealed intracrystalline plasticity in amphibole, which can be interpreted as the activation of the (100)[001] slip system.


2014 ◽  
Vol 67 (5) ◽  
pp. 790
Author(s):  
Jiang Wang ◽  
Jian Li ◽  
Youwen Wang

One-dimensional PbTiO3 nanowires 40–500 nm in diameter and ~400 μm in length were synthesized via a hydrothermal strategy and characterized by X-ray diffraction, electron backscatter diffraction, scanning electron microscopy, and transmission electron microscopy. The results show that the PbTiO3 nanowires exhibit a new acicular crystal structure, which is a tetragonal superstructure composed of a large unit cell of 40 atoms (Pb : Ti : O = 1 : 1 : 3) with a = 12.35 Å, c = 3.83 Å. The PbTiO3 has a feature of unidirectional bending when observed through transmission electron microscopy several times. The bending can be controlled by the electron beam intensity in transmission electron microscopy and the bending process is reversible. Moreover, a possible mechanism for the bending behaviour was also studied, which indicates that macroscopic polarization is in the {110} plane and the direction is not consistent with the electric field, giving the possible driving force for the bending.


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