scholarly journals Effect of Electropulsing Treatment on Microstructure and Mechanical Properties of a Deformed ZrTiAlV Alloy

Materials ◽  
2019 ◽  
Vol 12 (21) ◽  
pp. 3560 ◽  
Author(s):  
Zhi Nan Yang ◽  
Feng Jiang ◽  
Xu Biao Wang ◽  
Lin Qu ◽  
Yan Guo Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Heating Temperature ◽  
Transformation Process ◽  
Heating Process ◽  
Positive Effects ◽  
Β Phase ◽  
Treatment Processes ◽  
Conventional Heat Treatment ◽  
Electropulsing Treatment ◽  
Electron Wind

In contrast to conventional heat treatment processes, electropulsing not only heats an alloy, but also exerts some other positive effects during the heating process. In this paper, the microstructural evolution and mechanical properties of a deformed Zr40Ti5Al4V alloy after electropulsing treatment were investigated. The results showed that when the charging voltage was 2 kV, there was a slight decrease in dislocation density due to the electron wind which softened the alloy even though the highest temperature of the specimen during the treatment was only 86 °C. Increasing the charging voltage to 6 kV not only further increased the heating temperature, but accelerated the phase transformation process of α″ → β → α. The presence of the α phase strengthened the alloy but notably deteriorated its ductility. A full and refined β phase microstructure could be obtained when the charging voltage was increased to 8 kV. This simultaneously increased the strength and ductility of the alloy.

scholarly journals Correlation between Microstructural Alteration, Mechanical Properties and Manufacturability after Cryogenic Treatment: A Review

Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3302 ◽  
Author(s):  
Abbas Razavykia ◽  
Cristiana Delprete ◽  
Paolo Baldissera
Keyword(s):  
Mechanical Properties ◽  
Phase Transfer ◽  
Cryogenic Treatment ◽  
Future Research ◽  
Treatment Processes ◽  
Current Review ◽  
Conventional Heat Treatment ◽  
Refinement Process ◽  
Properties Of Materials ◽  
Quenching And Tempering

Cryogenic treatment is a supplemental structural and mechanical properties refinement process to conventional heat treatment processes, quenching, and tempering. Cryogenic treatment encourages the improvement of material properties and durability by means of microstructural alteration comprising phase transfer, particle size, and distribution. These effects are almost permanent and irreversible; furthermore, cryogenic treatment is recognized as an eco-friendly, nontoxic, and nonexplosive process. In addition, to encourage the application of sustainable techniques in mechanical and manufacturing engineering and to improve productivity in current competitive markets, cryo-treatment can be considered as a promising process. However, while improvements in the properties of materials after cryogenic treatment are discussed by the majority of reported studies, the correlation between microstructural alteration and mechanical properties are unclear, and sometimes the conducted investigations are contradictory with each other. These contradictions provide different approaches to perform and combine cryogenic treatment with pre-and post-processing. The present literature survey, mainly focused on the last decade, is aimed to address the effects of cryogenic treatment on microstructural alteration and to correlate these changes with mechanical property variations as a consequence of cryo-processing. The conclusion of the current review discusses the development and outlines the trends for the future research in this field.

Influence of the Ageing Temperature on the Selected Mechanical Properties of the Ti6Al7Nb Alloy

2015 ◽  
Vol 641 ◽  
pp. 120-123 ◽  
Author(s):  
Robert Dąbrowski ◽  
Janusz Krawczyk ◽  
Edyta Rożniata
Keyword(s):  
Mechanical Properties ◽  
Impact Strength ◽  
Volume Fraction ◽  
Heating Temperature ◽  
Ageing Temperature ◽  
Sample Length ◽  
Two Phase ◽  
Β Phase ◽  
Α Phase ◽  
The Impact

The results of investigations of the influence of the ageing temperature on the selected mechanical properties i.e. hardness, fracture toughness (examined by the linear elastic fracture mechanics - KIctest) and impact strength (KV) of two-phase Ti6Al7Nb alloy, are presented in the hereby paper. Investigations were performed in the ageing temperatures range: 450÷650°C of the alloy previously undercooled from the selected heating temperature (in two-phase range) - equal 970°C. The heating temperature was determined on the basis of the dilatometric curve of the alloy heating in the system ΔL = f ((T), where: ΔL – change of the sample length, T – temperature, which was then differentiated in the system: ΔL/ΔT = f (T). The dilatometer L78 R.I.T.A of the LINSEIS Company was used in the tests. Investigations of the alloy microstructure in the ageing temperatures range 450÷650°C were carried out by means of the light microscope Axiovert 200 MAT of the Carl Zeiss Company. It was found that nearly equiaxial grains of the primary α phase occur in the microstructure (of the volume fraction app. 30%) and that the volume fraction of the new lamellar α phase - formed from the supersaturated β phase - increases. With an increase of the alloy ageing temperature, in the mentioned above range, a small increase of its hardness from 305 to 324HV as well as a decrease of stress intensity factor KIcfrom 67.3 to 48.6 MPa x m1/2and impact strength (KV) from 40.2 to 31.3 J. The impact tests results were supplemented by the fractographic documentation. It was found, that the characteristic features of the fractures of impact test samples do not exhibit essential differences in dependence of the ageing temperature and material hardness. The fractographic investigations were performed by means of the scanning electron microscope NovaNanoSEM 450.

Electropulsing-Induced α to β Phase Transformation of Ti–6Al–4V

2019 ◽  
Vol 141 (11) ◽  
Author(s):  
Jihui Huang ◽  
Zhutian Xu ◽  
Yujun Deng ◽  
Linfa Peng
Keyword(s):  
Phase Transformation ◽  
Transformation Process ◽  
Transformation Rate ◽  
Avrami Model ◽  
Β Phase ◽  
Specific Effects ◽  
Heating Treatment ◽  
Transus Temperature ◽  
Lower Temperature ◽  
Electropulsing Treatment

Abstract Electrically assisted forming (EAF) has been increasingly utilized as an effective auxiliary processing technology to improve the formability of hard-to-deform metals. Previous works have revealed that the phase transformation of titanium alloys subjected to electropulsing treatment (EPT) can occur at a lower temperature and in a remarkably shorter time compared with those subjected to the traditional heating treatment (THT). However, an in-depth experimental verification and further analysis is still missing so far. Therefore, to characterize the specific effects of EPT on α → β transformation process, both EPT and THT experiments were conducted on Ti–6Al–4V sheet specimens. After that, a calculation method based on the analysis of optical microscopic (OM) metallographs was developed to characterize the amount of phase transformation in EPT and THT. According to the results, it was found that the pulse current can significantly reduce the phase transus temperature and accelerate the transformation process in EPT compared with that in THT. Furthermore, the specific effects of EPT on transus temperature and phase transformation rate were investigated in detail. Based on that, the transformation kinetics of the electropulsing-induced α → β phase transformation was also analyzed using the Johnson–Mehl–Avrami model. It is revealed that the activation energies of both nucleation and growth of phase transformation are reduced by electric current. Hence, the phase transformation can start at a lower temperature and with a higher rate in EPT. The mechanism behind the effects was also discussed in detail in the present work.

Improved ductility of aged Mg-9Al-1Zn alloy strip by electropulsing treatment

2009 ◽  
Vol 24 (5) ◽  
pp. 1810-1814 ◽  
Author(s):  
Yanbin Jiang ◽  
Guoyi Tang ◽  
Chanhung Shek ◽  
Yaohua Zhu ◽  
Lei Guan ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Atomic Diffusion ◽  
Alloy Strip ◽  
Β Phase ◽  
Microstructure And Mechanical Properties ◽  
Elongation To Failure ◽  
Electropulsing Treatment

The effect of electropulsing treatment (EPT) on the microstructure and mechanical properties of aged Mg-9Al-1Zn alloy strip was studied. EPT was found to accelerate tremendously the β phase spheroidization in the aged Mg-9Al-1Zn alloy. This improved microstructure exhibits excellent mechanical properties, that is, increasing elongation to failure significantly without loss of tensile strength. The spheroidization of the β phase during EPT was attributed to the reduction of the nucleation thermodynamic barrier and enhancement of atomic diffusion.

Influence of Thermal History on Microstructure and Mechanical Properties of Steels for Hot Stamping

2010 ◽  
Vol 654-656 ◽  
pp. 330-333 ◽  
Author(s):  
Takehide Senuma ◽  
Yoshito Takemoto
Keyword(s):  
Mechanical Properties ◽  
Heating Rate ◽  
Heating Temperature ◽  
Hot Stamping ◽  
High Strength ◽  
Heating Process ◽  
High Heating Rate ◽  
Transformation Behavior ◽  
Microstructure And Mechanical Properties ◽  
Heat Treated

Hot stamping is an attractive method to produce extra high strength automotive components. In the conventional hot stamping, the furnace heating is employed and the heating rate is quite low. To improve the productivity of the hot stamping technology, the reduction of time for the heating process is required. In this study, the influence of the heating rate in a range up to 200°C/s, heating temperatures between 650°C and 950°C and cooling condition on microstructure and mechanical properties of 0.22% C -3%Mn steel has been investigated. The steel is a promising material for the highly productive new hot stamping technology because this steel transformed into martensite from austenite even at cooling in free air. The specimens heat-treated at a high heating rate and for short holding time at the heating temperature just above Ac3 show significantly fine martensite microstructure and a good strength-toughness balance. In this paper, the α→ γ transformation behavior and the γ→ α transformation behavior after inter-critical annealing are discussed to explain the evolution of the microstructures and mechanical properties.

Effect of electropulsing treatment on solid solution behavior of an aged Mg alloy AZ61 strip

2008 ◽  
Vol 23 (10) ◽  
pp. 2685-2691 ◽  
Author(s):  
Yanbin Jiang ◽  
Guoyi Tang ◽  
Lei Guan ◽  
Shaonan Wang ◽  
Zhuohui Xu ◽  
...  
Keyword(s):  
Solid Solution ◽  
Solution Process ◽  
Solution Treatment ◽  
Mg Alloy ◽  
X Ray Diffraction ◽  
Solution Behavior ◽  
Β Phase ◽  
Solid Solution Treatment ◽  
Conventional Heat Treatment ◽  
Electropulsing Treatment

The effect of electropulsing treatment (EPT) on the solution behavior of aged Mg alloy AZ61 strip was investigated using scanning electron microscope (SEM) and x-ray diffraction (XRD). It was found that EPT accelerated tremendously the dissolution of β phase into α matrix in an aged Mg alloy AZ61 strip. The dissolution of β phase took place in less than 4 s at relatively low temperature under EPT, compared with that in conventional heat treatment. A mechanism for rapid solid solution process during EPT was proposed based on the coupling of the thermal and athermal effects. The results in this investigation indicated that EPT played an important role in the nonequilibrium microstructural evolution in the alloy. It is supposed that EPT can provide a highly efficient approach for solid solution treatment of the alloy.

INFLUENCE THE QUENCHING AND TEMPERING ON THE MICROSTRUCTURE, MECHANICAL PROPERTIES AND SURFACE ROUGHNESS, OF MEDIUM CARBON STEEL

2018 ◽  
Vol 18 (1) ◽  
pp. 125-135
Author(s):  
Sattar H A Alfatlawi
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Surface Roughness ◽  
Carbon Steel ◽  
Cold Water ◽  
Medium Carbon Steel ◽  
Medium Carbon ◽  
Heating And Cooling ◽  
Treatment Processes ◽  
Quenching And Tempering

One of ways to improve properties of materials without changing the product shape toobtain the desired engineering applications is heating and cooling under effect of controlledsequence of heat treatment. The main aim of this study was to investigate the effect ofheating and cooling on the surface roughness, microstructure and some selected propertiessuch as the hardness and impact strength of Medium Carbon Steel which treated at differenttypes of heat treatment processes. Heat treatment achieved in this work was respectively,heating, quenching and tempering. The specimens were heated to 850°C and left for 45minutes inside the furnace as a holding time at that temperature, then quenching process wasperformed in four types of quenching media (still air, cold water (2°C), oil and polymersolution), respectively. Thereafter, the samples were tempered at 200°C, 400°C, and 600°Cwith one hour as a soaking time for each temperature, then were all cooled by still air. Whenthe heat treatment process was completed, the surface roughness, hardness, impact strengthand microstructure tests were performed. The results showed a change and clearimprovement of surface roughness, mechanical properties and microstructure afterquenching was achieved, as well as the change that took place due to the increasingtoughness and ductility by reducing of brittleness of samples.

scholarly journals Design and Manufacturing of a Disposable, Cyclo-Olefin Copolymer, Microfluidic Device for a Biosensor †

Sensors ◽  
2019 ◽  
Vol 19 (5) ◽  
pp. 1178 ◽  
Author(s):  
Jorge Prada ◽  
Christina Cordes ◽  
Carsten Harms ◽  
Walter Lang
Keyword(s):  
Microfluidic Device ◽  
Heating Temperature ◽  
Low Cost ◽  
Reaction Chamber ◽  
Microfluidic System ◽  
Heating Process ◽  
Design And Manufacturing ◽  
On Chip ◽  
Working Parameters ◽  
Auto Fluorescence

This contribution outlines the design and manufacturing of a microfluidic device implemented as a biosensor for retrieval and detection of bacteria RNA. The device is fully made of Cyclo-Olefin Copolymer (COC), which features low auto-fluorescence, biocompatibility and manufacturability by hot-embossing. The RNA retrieval was carried on after bacteria heat-lysis by an on-chip micro-heater, whose function was characterized at different working parameters. Carbon resistive temperature sensors were tested, characterized and printed on the biochip sealing film to monitor the heating process. Off-chip and on-chip processed RNA were hybridized with capture probes on the reaction chamber surface and identification was achieved by detection of fluorescence tags. The application of the mentioned techniques and materials proved to allow the development of low-cost, disposable albeit multi-functional microfluidic system, performing heating, temperature sensing and chemical reaction processes in the same device. By proving its effectiveness, this device contributes a reference to show the integration potential of fully thermoplastic devices in biosensor systems.

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