scholarly journals Central Composite Experiment Design (CCD)-Response Surface Method (RSM) to Optimize the Sintering Process of Ti-6Al-4V Alloy

Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 197
Author(s):  
Jing Xia ◽  
Shaopeng Liu ◽  
Bing Zhang ◽  
Yungui Chen
Keyword(s):  
Mechanical Properties ◽  
Response Surface ◽  
Significant Contribution ◽  
Mechanical Performance ◽  
Low Cost ◽  
High Porosity ◽  
Vacuum Sintering ◽  
Predicted Values ◽  
Experimental Values ◽  
Central Composite

It is widely acknowledged that the blended elemental (BE) powder metallurgy (PM) Ti6Al4V alloy attracted unusual due to its low cost and comprehensive mechanical properties. However, the high porosity and mediocre mechanical properties of traditional vacuum sintering limited its application. To achieve better mechanical performance, the central composite designs (CCDs) method was employed to analyze the influence of sintering parameters, such as sintering temperature (St), heating rate (Hr), and holding time (Ht). The results indicated that St makes the most significant contribution to compressive strength and sintering density, accounting for 95.5% and 86.54% respectively. In addition, Ht makes the most significant contribution to compression ratio, which accounted for 89.35%. Through the analysis of response surface methodology (RSM), the optimum sintering parameters (St, Ht, Hr) could be considered to be 1300 °C, 148 min and 5 °C/min. In addition, verification experiments were carried out under the optimum conditions, and the experimental results were in good agreement with the predicted values, since the deviation of the predicted and experimental values was less than 4.9%. Therefore, the results of this study could certify the reliability of CCDs method, which would contribute to the development of titanium alloys with low cost and high mechanical properties.

scholarly journals Viscosity and Sensory Acceptability of Almond Milkshake as Influenced by Sugar, Almond Paste and Corn Flour-A Response Surface Study

2021 ◽  
Vol 10 (3) ◽  
pp. 2483-2493
Keyword(s):  
Response Surface ◽  
Coefficient Of Determination ◽  
Confirmatory Test ◽  
Corn Flour ◽  
Sensory Score ◽  
Order Polynomial ◽  
Predicted Values ◽  
Experimental Values ◽  
Central Composite

The effect of variables such as sugar, almond paste, and cornflour on viscosity and a sensory score of almond milkshake samples were studied by response surface methodology. The central composite design was used to obtain optimum levels of variables. The values of viscosity and sensory scores obtained from different experiment runs were 170-1085cps and 6.2-7.7. The second-order polynomial model suggested by design expert software for viscosity and a sensory score of almond milkshake showed R2 (coefficient of determination) of 0.9871 and 0.9590, respectively. Whereas model F-values for viscosity and a sensory score of almond milkshake were 84.9 and 26.02, respectively. Optimum levels of sugar, almond paste, and cornflour suggested by models were 8%, 1% & 2%, respectively. Experimental values of responses obtained from the confirmatory test were almost similar to predicted values of responses suggested by models.

scholarly journals Multivariate Optimization of Pb2+ Adsorption onto Ethiopian Low-Cost Odaracha Soil Using Response Surface Methodology

Molecules ◽  
2021 ◽  
Vol 26 (21) ◽  
pp. 6477
Author(s):  
Yohanis Birhanu ◽  
Seyoum Leta
Keyword(s):  
Central Composite Design ◽  
Response Surface ◽  
Removal Efficiency ◽  
Interaction Effect ◽  
Contact Time ◽  
Low Cost ◽  
Design Model ◽  
Lead Ions ◽  
Experimental Result ◽  
Central Composite

Lead pollution is a severe health concern for humankind. Utilizing water contaminated with lead can cause musculoskeletal, renal, neurological, and fertility impairments. Therefore, to remove lead ions, proficient, and cost-effective methods are imperative. In this study, the Odaracha soil which is traditionally used by the local community of the Saketa District was used as a novel low-cost technology to adsorb lead ions. Odaracha adsorbent was characterized by scanning electron microscopy and Fourier transform infrared spectroscopy. The adsorption process followed the batch adsorption experiment. The response surface method was implemented to derive the operating variables’ binary interaction effect and optimize the process. According to the study’s experimental result, at optimum experimental conditions Odaracha adsorbent removes 98.17% of lead ions. Based on the result of the central composite design model, the Pb2+ ion removal efficiency of Odaracha was 97.193%, indicating an insignificant dissimilarity of the actual and predicted results. The coefficient of determination (R2) for Pb2+ was 0.9454. According to the factors’ influence indicated in the results of the central composite design model, all individual factors and the interaction effect between contact time and pH has a significant positive effect on lead adsorption. However, other interaction effects (contact time with dose and pH with dose) did not significantly influence the removal efficiency of lead ions. The adsorption kinetics were perfectly fitted with a pseudo-second-order model, and the adsorption isotherm was well fitted with the Freundlich isotherm model. In general, this study suggested that Odaracha adsorbent can be considered a potential adsorbent to remove Pb2+ ions and it is conceivable to raise its effectiveness by extracting its constituents at the industrial level.

Mechanical Properties of ABS Embedded with Basalt Fiber Fillers

2016 ◽  
Vol 16 (2) ◽  
pp. 69-74 ◽  
Author(s):  
Ayman M. M. Abdelhaleem ◽  
Mohammed Y. Abdellah ◽  
Hesham I. Fathi ◽  
Montasser Dewidar
Keyword(s):  
Mechanical Properties ◽  
Mechanical Performance ◽  
Low Cost ◽  
Basalt Fiber ◽  
Acrylonitrile Butadiene Styrene ◽  
Hardness Test ◽  
Basalt Fibers ◽  
Notched Strength ◽  
The Cost ◽  
Plastic Injection

AbstractAcrylonitrile-butadiene-styrene (ABS) has great verity applications in aerospace and automobiles industries. Mechanical strength of the ABS is superior to even that of impact resistant polystyrene. In addition metallic coatings can be applied to the surface of ABS moldings. The main aim of the present work is to investigate the mechanical properties of additives of basalt fibers (BF) to ABS with (5, 10, and 15) wt% embedded into the polymer matrix by using plastic injection molding technique. This new perceptions has been done on basalt fibers that have a potential low cost with its good mechanical performance. The ultimate tensile strength that obtained from the composite with 15 wt% is 56.67 MPa with 40.52 % increase value than neat ABS, Young’s modulus gradually increases with increasing the amount of additives. Impact un-notched strength decreases with a reported increment of 24.617 KJ.m–2. A Rockwell hardness test is also used and with the increases of additives the amount of hardness of the composite increases. A scan electron microscopy (SEM) on the fracture surface is captured to check the morphologies structure of the composite comparable with a neat ABS. and it is showed a very good distribution and bonding of the B.F. with the pure ABS. As well as the cost of the ABS and BF is reduced by a percentage of 15 %.

Optimization of a Whole-Stalk Operating System after Sugarcane Base Cutting

2019 ◽  
Vol 62 (1) ◽  
pp. 157-166
Author(s):  
Luxin Xie ◽  
Jun Wang ◽  
Shaoming Cheng ◽  
Jinbing Hu
Keyword(s):  
Operating System ◽  
Response Surface Methodology ◽  
Central Composite Design ◽  
Response Surface ◽  
Fracture Rate ◽  
Cleaning Performance ◽  
Abrasion Rate ◽  
Leaf Stripping ◽  
Predicted Values ◽  
Central Composite

Abstract. Leaf stripping and top breaking are the key procedures in whole-stalk sugarcane harvesting. In this study, a whole-stalk operating system after sugarcane base cutting was developed and tested to improve the leafy trash cleaning performance and adaptability of a whole-stalk harvester. A leaf shredding procedure was proposed before leaf stripping, and an anti-float top breaking device was developed for breaking cane tops. The rotational speeds of the leaf shredding (RL), leaf stripping (RS), and top breaking (RT) rollers were regarded as experimental factors, and the leafy trash content (including leaves, leaf sheaths, and tops in this study), top breaking rate, abrasion rate, and non-fracture rate of the middle or bottom parts were selected as indices. Central composite design combined with response surface methodology and comprehensive evaluation method were employed to conduct experiments and explore the interaction effects of factors on indices. The optimal operating parameters were nonlinearly optimized and determined to be RL of 512.9 rpm, RS of 418.8 rpm, and RT of 307.0 rpm. Under these conditions, the predicted values of leafy trash content, top breaking rate, abrasion rate, and non-fracture rate were 4.98%, 88.39%, 5.19%, and 96.21%, respectively. Verification experiments indicated that the observed values were in agreement with the predicted values. Results suggested that the leaf shredding device and anti-float top breaking device developed in this study were effective for improving the leafy trash cleaning performance and adaptability of the whole-stalk operating system, and there was a good potential for performance improvement of whole-stalk sugarcane harvesters. Keywords: Central composite design, Leaf shredding, Leaf stripping, Response surface methodology, Top breaking, Whole-stalk harvester.

scholarly journals Modeling of Degradation of Diazo Dye in Swirl-Flow Photocatalytic Reactor: Response Surface Approach

Catalysts ◽  
2020 ◽  
Vol 10 (12) ◽  
pp. 1418
Author(s):  
Waleed Jadaa ◽  
Anand Prakash ◽  
Ajay K. Ray
Keyword(s):  
Light Intensity ◽  
Response Surface ◽  
Swirl Flow ◽  
Quadratic Model ◽  
Catalyst Loading ◽  
Random Pattern ◽  
Photocatalytic Reactor ◽  
Degradation Reactions ◽  
Predicted Values ◽  
Experimental Values

Photocatalytic degradation of Direct Blue 15 (DB15), an azo dye, was studied using a swirl-flow monolithic reactor under UV irradiation. The degradation reactions were carried out to investigate effects of initial dye concentration, catalyst loading, and light intensity at an optimal pH. The experiments were designed and mathematically modelled by CCD-RSM (central composite design-response surface methodology) approach. It was found that the selected parameters significantly affect DB15 degradation. In terms of the linear term, catalyst loading and light intensity had a synergistic effect, while dye concentration registered the opposite effect. Strong interaction was observed between catalyst loading and both light intensity and initial dye concentration compared with the interaction of light intensity and initial dye concentration. Based on the experimental results, a quadratic model was developed to predict the percentage removal of DB15. The predicted values of the model were in good agreement with the experimental values (R2 = 0.987), indicating the model fits well for the parameter space for which experiments were performed. According to diagnostic plots, the model credibility was valid because its residuals were distributed normally and exhibited a random pattern based on their examination versus the predicted values. The results revealed that the initial dye concentration and catalyst concentration have a significant effect on the mineralization time.

scholarly journals On the Use of Biobased Waxes to Tune Thermal and Mechanical Properties of Polyhydroxyalkanoates–Bran Biocomposites

Polymers ◽  
2020 ◽  
Vol 12 (11) ◽  
pp. 2615
Author(s):  
Vito Gigante ◽  
Patrizia Cinelli ◽  
Maria Cristina Righetti ◽  
Marco Sandroni ◽  
Giovanni Polacco ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Wheat Bran ◽  
Mechanical Performance ◽  
Low Cost ◽  
Impact Resistance ◽  
Mechanical Analysis ◽  
Polymeric Matrix ◽  
Flour Milling ◽  
Mechanical Performances ◽  
Analytic Models

In this work, processability and mechanical performances of bio-composites based on poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) containing 5, 10, and 15 wt % of bran fibers, untreated and treated with natural carnauba and bee waxes were evaluated. Wheat bran, the main byproduct of flour milling, was used as filler to reduce the final cost of the PHBV-based composites and, in the same time, to find a potential valorization to this agro-food by-product, widely available at low cost. The results showed that the wheat bran powder did not act as reinforcement, but as filler for PHBV, due to an unfavorable aspect ratio of the particles and poor adhesion with the polymeric matrix, with consequent moderate loss in mechanical properties (tensile strength and elongation at break). The surface treatment of the wheat bran particles with waxes, and in particular with beeswax, was found to improve the mechanical performance in terms of tensile properties and impact resistance of the composites, enhancing the adhesion between the PHBV-based polymeric matrix and the bran fibers, as confirmed by predictive analytic models and dynamic mechanical analysis results.

scholarly journals Fabrication Technique for Bio-Composite Patch Repair on Laminated Structures of CFRP Plate

2014 ◽  
Vol 564 ◽  
pp. 366-371 ◽  
Author(s):  
M.K.H. Muda ◽  
Faizal Mustapha ◽  
K.D. Mohd Aris ◽  
Mohamed Thariq Hameed Sultan
Keyword(s):  
Mechanical Properties ◽  
Composite Structures ◽  
Mechanical Performance ◽  
Low Cost ◽  
Natural Fibre ◽  
Patch Repair ◽  
Fabrication Technique ◽  
Composite Surface ◽  
Wide Range ◽  
Laminated Structures

Laminated structures are assembled so that the fibre orientation provides most of desired mechanical properties and the matrix largely determines the environmental performance. Composites laminate structures are used in a wide range of applications in aerospace, marine, automotive, surface transport and sports equipment markets. Damage to composite components is not always visible to the naked eye and the extent of damage is best determined for structural components by suitable Non Destructive Test (NDT) methods. Alternatively the damaged areas can be located by simply tapping the composite surface and listening to the sound. The damaged areas give a dull response to the tapping, and the boundary between the good and damaged composite can easily be mapped to identify the area for repair. Awareness of and inspection for composite damage should be included in the regular maintenance schedules for composite structures. Particular attention would be made to areas which are more prone to damage. The repair can be done by using composite itself or bio-composite. Bio-composite is a reinforcement of natural fibre such as plant and a material that formed by matrix or resin. Then repairs to aircraft structures are controlled and should be carried out according to the Aircraft Structural Repair Manual (SRM). For other applications the repaired components would normally be expected to meet the original specifications and mechanical performance requirements. This paper presents the fabrication technique including patch repair by using bio-composite which is kenaf and its aim to give a general approach to composite fabrication on patch repair in all applications. Through the described approach, the life of the structure is expanded and met the properties requirements such as low cost, fairly good mechanical properties, high specific strength, non-abrasive, eco-friendly and bio-degradability characteristics.

scholarly journals Optimization of chlorite and talc flotation using experimental design methodology: Case study of the MCG plant, Morocco

2020 ◽  
Vol 120 (12) ◽  
Author(s):  
K. Boujounoui ◽  
A. Abidi ◽  
A. Baçaoui ◽  
K. El Amari ◽  
A. Yaacoubi
Keyword(s):  
Response Surface Methodology ◽  
Central Composite Design ◽  
Response Surface ◽  
Desirability Functions ◽  
Sulphide Ore ◽  
Experimental Values ◽  
Experimental Design Methodology ◽  
Central Composite ◽  
Good Agreement

SYNOPSIS Response surface methodology (RSM), central composite design (CCD), and desirability functions were used for modelling and optimization of the operating factors in chlorite and talc (collectively termed 'mica') flotation. The influence of pulp pH, cyanide (NaCN) consumption, and particle size was studied with the aim of optimizing ssilicate flotation while minimizing recoveries of galena, chalcopyrite, and sphalerite. Flotation tests were carried out on a representative sample of a complex sulphide ore from Draa Sfar mine (Morocco). The model predictions for the flotation of each of the minerals concerned were found to be in good agreement with experimental values, with R2 values of 0.91, 0.98, 0.99, and 0.90 for mica, galena, chalcopyrite, and sphalerite recoveries, respectively. RSM combined with desirability functions and CCD was successfully applied for the modelling of mica flotation, considering simultaneously the four flotation responses to achieve the maximum recovery of mica and minimal loss of Pb, Cu, and Zn to the flotation concentrate. Keywords: chlorite, talc, flotation, response surface methodology, central composite design, optimization.

scholarly journals Removal of Hg2+ with Polypyrrole-Functionalized Fe3O4/Kaolin: Synthesis, Performance and Optimization with Response Surface Methodology

Nanomaterials ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 1370
Author(s):  
Zhenfeng Lin ◽  
Ziwei Pan ◽  
Yuhao Zhao ◽  
Lin Qian ◽  
Jingtao Shen ◽  
...  
Keyword(s):  
Response Surface Methodology ◽  
Response Surface ◽  
Adsorption Process ◽  
Low Cost ◽  
Solution Ph ◽  
Central Composite Designs ◽  
Pseudo Second Order ◽  
Composite Designs ◽  
Central Composite ◽  
Relevant Factors

PPy-Fe3O4/Kaolin was prepared with polypyrrole functionalized magnetic Kaolin by a simple, green, and low cost method to improve the agglomeration and low adsorption capacity of Kaolin. PPy-Fe3O4/Kaolin was employed to remove Hg2+ and the results were characterized by various methods. Relevant factors, including solution pH, dosage of adsorbent, concentration (C0), and temperature (T), were optimized by Response Surface Methodology (RSM) and Central Composite Designs (CCD). The optimal results show that the importance for adsorption factors is pH > T > C0 > dosage, and the optimal adsorption conditions of PPy-Fe3O4/Kaolin are pH = 7.2, T = 315 K, C0 = 50 mg/L, dosage of 0.05 g/L, and the capacity is 317.1 mg/g. The adsorption process conforms to the pseudo-second-order and Langmuir models. Dubinin–Radushkevich model shows that adsorption process is spontaneous and endothermic. Moreover, the adsorption of mercury by PPy-Fe3O4/Kaolin was achieved mainly through electrostatic attraction, pore diffusion, and chelation between amino functional groups and Hg2+. PPy-Fe3O4/Kaolin has excellent reproducibility, dispersity, and chemical stability, and it is easy to be separated from solution through an external magnetic field. The experiments show that PPy-Fe3O4/Kaolin is an efficient and economical adsorbent towards mercury.

Sign in / Sign up

Export Citation Format

Share Document