scholarly journals Quickly Identifying High-Risk Variables of Ultrasonic Extraction Oil from Multi-Dimensional Risk Variable Patterns and a Comparative Evaluation of Different Extraction Methods on the Quality of Forsythia suspensa Seed Oil

Molecules ◽  
2019 ◽  
Vol 24 (19) ◽  
pp. 3445
Author(s):  
Liangshan Ming ◽  
Hao Huang ◽  
Yumao Jiang ◽  
Gengjinsheng Cheng ◽  
Daoying Zhang ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
High Risk ◽  
Experimental Design ◽  
Seed Oil ◽  
High Efficiency ◽  
Extraction Methods ◽  
Ultrasonic Extraction ◽  
Rapid Screening ◽  
Forsythia Suspensa ◽  
Extraction Processes

Generally, essential oils and components of interest are extracted from plants using organic solvent, distillation, ultrasound and supercritical extraction methods. Ultrasonic extraction (UE) has the advantage of high efficiency, but its process is complicated and it has numerous variables. In this study, an L18-Hunter experimental design was applied for the first time to investigate the practicability of applying UE to Forsythia suspensa seed oil. Six potential high-risk variables, including numerical and non-numeric types, were obtained from the risk analysis and their impacts on global yield and antioxidant activity were screened. Furthermore, oils obtained by different extraction processes (i.e., UE, supercritical fluid extraction (SFE), soxhlet extraction (SE) and hydrodistillation extraction (HD)) were analyzed. A comparative study of these oils was characterized and compared by FT-IR, GC-MS and antioxidant activity. The obtained results show that the type of solvent, solvent-to-solid ratio, extraction power and time were the significant variables affecting the extraction yield, whereas antioxidant activity was only affected by the type of solvent. The regression coefficients of the yield and antioxidant activity models were 0.79 and 0.91, and the ANOVA of the models were 0.013 and <0.0001, respectively. Beta-Pinene was the main abundant component in the oils for the UE, SFE, SE and HD methods and the content was about 46%~52.4%. In conclusion, the L18-Hunter design could be used as an effective experimental design method for rapid screening of high-risk variables. Regarding extraction efficiency, chemical composition and biological activity, UE not only offered a robust Forsythia suspensa seed oil extraction process, but also provided a time- and cost-effective advantage to the food and pharmaceutical industry when compared to the SFE, SE and HD extraction processes.

Evaluation of green extraction processes, lipid composition and antioxidant activity of pomegranate seed oil

2021 ◽  
Author(s):  
E. Rojo-Gutiérrez ◽  
O. Carrasco-Molinar ◽  
J. M. Tirado-Gallegos ◽  
A. Levario-Gómez ◽  
M. L. Chávez-González ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Lipid Composition ◽  
Seed Oil ◽  
Green Extraction ◽  
Pomegranate Seed Oil ◽  
Extraction Processes ◽  
Pomegranate Seed

scholarly journals Ultrasonic Extraction of Oil fromCaesalpinia spinosa(Tara) Seeds

2016 ◽  
Vol 2016 ◽  
pp. 1-6
Author(s):  
Zhan-jun Li ◽  
Feng-jian Yang ◽  
Lei Yang ◽  
Yuan-Gang Zu
Keyword(s):  
Fatty Acid ◽  
Seed Oil ◽  
Soxhlet Extraction ◽  
Extraction Methods ◽  
Ultrasonic Extraction ◽  
Particle Sizes ◽  
Extraction Temperature ◽  
Simple Method ◽  
Alternative Means ◽  
Fatty Acid Compositions

Oil extracted from the seeds ofCaesalpinia spinosa(common name: tara) can be used in a number of applications. In the present study, tara seed oil was obtained by ultrasonic extraction. The effects of different solvents, particle sizes in the ground seed samples, extraction times, ultrasonication powers, extraction temperatures, and liquid–solid ratios on the yield of tara seed oil were investigated. The yield from the ultrasonic extraction was compared with that from traditional Soxhlet extraction. The results showed that ultrasonic extraction could be completed in a shorter time with reduced solvent consumption. The yield of tara seed oil increased with increasing ultrasonication power and extraction temperature. Gas chromatography was used to analyze the fatty acid compositions of the oils extracted by the two methods. The fatty acid compositions of the oils from both extraction methods were similar, which indicates that ultrasonic extraction is a viable alternative means of extraction. It is a rapid, efficient, and simple method for production of lipids from tara seeds.

scholarly journals Comparison of the Effect of Various Extraction Methods on the Phytochemical Composition and Antioxidant Activity of Thymelaea hirsuta L. aerial parts in Tunisia

2017 ◽  
Vol 14 (3) ◽  
pp. 997-1007 ◽  
Author(s):  
Maroua Yahyaoui ◽  
Nessrine Ghazouani ◽  
Ines Sifaoui ◽  
Manef Abderrabba
Keyword(s):  
Antioxidant Activity ◽  
Radical Scavenging ◽  
Extraction Methods ◽  
Antioxidant Power ◽  
Aerial Parts ◽  
Ferric Reducing Antioxidant Power ◽  
Soxhlet Method ◽  
Thymelaea Hirsuta ◽  
Extraction Processes

The present study aims to evaluate the effect of extraction methods namely soxhlet and cold maceration on the quality of T. hirsuta extracts, collected from different geographic regions within Tunisia. Hexane, ethyl acetate and methanol were used as solvent for both extraction processes. Yields varied considerably (from 0.61 to 8.11 %) according to sampling region, organic solvent and extraction method. The various chemical contents extracts were estimated by colorimetric methods, revealing important amounts of polyphenols (from 29.37 ± 1.34 to 259.63 ± 3.17 mg GAE/g) and flavonoids (from 26.22 ± 6.06 to 163.64 ± 3.32 mg QE/g). The antioxidant activity was measured using the DPPH-radical scavenging, the ABTS-radical scavenging and the ferric reducing antioxidant power (FRAP) assays. The antioxidant analysis showed that the methanol extract obtained by both processes exhibited the uppermost capacity to scavenge free radicals. However, the cold maceration technique leads to the richest extract in phenolic compounds compared to soxhlet method.

scholarly journals Optimization of Ultrasound Extraction of Cactus Pear(Opuntia ficus indica)Seed Oil Based on Antioxidant Activity and Evaluation of Its Antimicrobial Activity

2017 ◽  
Vol 2017 ◽  
pp. 1-9 ◽  
Author(s):  
María de los Angeles Ortega-Ortega ◽  
Nelly del Socorro Cruz-Cansino ◽  
Ernesto Alanís-García ◽  
Luis Delgado-Olivares ◽  
José Alberto Ariza-Ortega ◽  
...  
Keyword(s):  
Antimicrobial Activity ◽  
Antioxidant Activity ◽  
Extraction Method ◽  
Seed Oil ◽  
Extraction Methods ◽  
Seed Oils ◽  
Cactus Pear ◽  
Ultrasound Extraction ◽  
Conventional Extraction ◽  
Amplitude Level

The purpose of the present study was to determine the optimal ultrasound conditions (amplitude level and time) for the extraction of cactus pear seed oil with the highest antioxidant activity using a closed system. Seed oil was analyzed for yield, antioxidant activity by ABTS and DPPH, and antimicrobial activity. Conventional extraction methods were assessed for comparison. Amplitude level significantly affected antioxidant activity in linear terms (p< 0.0001 DPPH andp< 0.001 ABTS, resp.) so, at lower amplitudes, the higher antioxidant activity was achieved. The optimum ultrasound extraction conditions were of 78% amplitude for 10 min and yielded antioxidant activity values of 66.25 mg AAE/100 g and 289 µmol TE/100 g for ABTS and DPPH, respectively. Compared with conventional extraction methods, ultrasound exhibited lower oil yield and antioxidant activity but had the potential to achieve comparable results if multiple ultrasound extractions are performed in the time needed by conventional methods. Seed oils showed similar antimicrobial activity despite the extraction method and were more effective againstEscherichia coli. The results demonstrated that ultrasound can be an alternative extraction method of seed oils from fruits such as cactus pear.

Polyphenol, Flavonoid Content and Antioxidant Activity of the Garlic (Allium sativum L.) Extract Obtained by Two Different Extraction Processes

2022 ◽  
Vol 1048 ◽  
pp. 493-501
Author(s):  
Khanh Duy Huynh ◽  
Van Thinh Pham ◽  
Van Khang Tran ◽  
Hoang Danh Pham ◽  
Tri Nhut Pham
Keyword(s):  
Antioxidant Activity ◽  
Western Medicine ◽  
Allium Sativum ◽  
Quality Parameters ◽  
Ultrasonic Extraction ◽  
Flavonoid Content ◽  
Ultrasonic Assisted ◽  
Extraction Processes ◽  
Extraction Parameters ◽  
Conventional Methods

Garlic is a globally used spice due to its pungent taste and a fishy deodorant and digestive stimulator. Owing to the widespread use of garlic in both Oriental and Western medicine, further investigations on garlic extracts might carry important implications in the industry. In this study, we conducted extraction of garlic extraction by two conventional methods and an ultrasonic assisted method. The processes were optimized with respect to various quality parameters including polyphenol, flavonoid content, and antioxidant activity. The results showed that extracting garlic under the ultrasonic support will show higher efficiency than the non-ultrasonic extraction. The optimal extraction parameters are: 70% ethanol solvent, 10/1 solvent / material ratio, 40 °C temperature and 40 minutes time. Keywords: Allium Sativum L., Garic, Polyphenol, Flavonoid, Antioxidant

scholarly journals Implementation of the extraction method for the separation of Fe3+ and Ni2+ ions on cascade of mixing-settling extractors

2022 ◽  
Vol 1212 (1) ◽  
pp. 012014
Author(s):  
N.A. Milevskii ◽  
Y.A. Klychevskikh ◽  
V.O. Solov’ev ◽  
I.V. Zinov’eva ◽  
M.I. Fedorova
Keyword(s):  
Hydrochloric Acid ◽  
Acid Solution ◽  
Hydrochloric Acid Solution ◽  
Manufacturing Process ◽  
Extraction Method ◽  
High Efficiency ◽  
Extraction Methods ◽  
Technological Solution ◽  
Extraction Scheme ◽  
Extraction Processes

Abstract Extraction processes are one of the most efficient methods of purification and separation of compounds. However, laboratory-developed methods commonly are not a complete technique that can be applied to the real manufacturing process with its extraction equipment. The extraction method for the separation of Fe3+ and Ni2+ ions using hydrochloric acid solution on a cascade of mixing-settling extractors has been determined. The extraction scheme chosen provides high efficiency of a cascade by using liquid pseudomembranes (LPM). Besides its extraction scheme simplicity, the LPM method is more economically beneficial compared to classical extraction methods. The process includes stages of Fe3+ ions extraction into the feed, followed by reextraction into the water and the feed purification for reusing it later on. The consumption of solvents and the stirring speed for the stable and efficient cascade work have been optimized. The described process is a complete technological solution for recycling processed battery waste.

Antioxidant Activity and Protective Effect against Oxidative Stress on Hippocampal HT22 Cells of Tea Seed Oil

2018 ◽  
Vol 24 (1) ◽  
pp. 53-59
Author(s):  
Jong Min Kim ◽  
Seon Kyeong Park ◽  
Jin Yong Kang ◽  
Seong-kyeong Bae ◽  
Ga-Hee Jeong ◽  
...  
Keyword(s):  
Oxidative Stress ◽  
Antioxidant Activity ◽  
Protective Effect ◽  
Seed Oil ◽  
Ht22 Cells ◽  
Tea Seed Oil

Comparison of Bioactive Compounds of Matricaria recutita Extracted by Ultrasound and Maceration and their Effects on Preventing Sunflower Oil During Frying

2019 ◽  
Vol 15 (2) ◽  
pp. 156-164 ◽  
Author(s):  
Reza Farahmandfar ◽  
Maryam Asnaashari ◽  
Yegane Asadi ◽  
Batool Beyranvand
Keyword(s):  
Antioxidant Activity ◽  
Gallic Acid ◽  
Bioactive Compounds ◽  
Sunflower Oil ◽  
Radical Scavenging ◽  
Stability Index ◽  
Acid Value ◽  
Extraction Methods ◽  
Oil Stability Index ◽  
Matricaria Recutita

Background: It is important to study about the use of natural antioxidants as alternatives to synthetic ones due to the possibility of carcinogenic effects of synthetic antioxidants. This study is comparing the effect of the ultrasound-assisted and maceration extraction methods on antioxidant activity of Matricaria recutita. Methods: Bioactive compounds including phenolic, tocopherol, flavonoid and tannins and antioxidant activity of the extracts were evaluated. Moreover, extracts obtained from ultrasound and maceration methods were added to sunflower oil without any antioxidants at level of 200, 500 and 800 ppm, after that samples were heated at 180°C. Oxidation of the samples were evaluated after 0, 4, 8, 12, 16, 20 and 24 hours by measuring Peroxide Value (PV), Conjugated Diene (CD), Iodine Value (IV), Carbonyl Value (CV), Total Polar Compounds (TPC), Oil Stability Index (OSI), Color Index (CI) and acid value (AV). Results: The result showed total phenol (42.90 mg gallic acid/g extract), tocopherol (120.46 &#181;g &#945; - tocopherol/ml extract), flavonoid (2.64 mg/100 g extract) and tannins (3.89 mg gallic acid/g extract) of ultrasound extracts were higher than maceration extracts. Antioxidant activity of the extract was evaluated by DPPH assay which indicated 800 ppm of the Matricaria recutita extracted by ultrasound was the highest radical scavenging ability. Conclusion: Result indicated both ultrasound and maceration extracts could increase the oil oxidative stability but could not increase compared to BHA. In most cases, the extract samples by ultrasound had a better effect on stabilizing of sunflower oil during frying.

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