The Study of Glycerol Plasticized Thermoplastic Sago Starch

2012 ◽  
Vol 576 ◽  
pp. 289-292 ◽  
Author(s):  
Ahmad Zuraida ◽  
A.R. Nur Humairah ◽  
A.W. Nur Izwah ◽  
Z. Siti Naqiah
Keyword(s):  
Hydrogen Bond ◽  
Tensile Strength ◽  
Moisture Content ◽  
Water Absorption ◽  
Weight Fraction ◽  
Maximum Load ◽  
Sago Starch ◽  
Melt Blending ◽  
Stable Hydrogen Bond ◽  
Preliminary Study

Thermoplastic sago starch (TPSS) was produced by plasticizing with glycerol through melt blending before being compression moulded. The investigated TPSS was prepared at glycerol/starch weight fraction of 40/60, 35/65 and 30/70. The functional groups composition, tensile strength, density, moisture content and water absorption were evaluated and compared at different glycerol/starch ratio. The compatibility of the glycerol as the plasticizer in the TPSS was proven by Fourier transform infrared spectroscopy (FTIR) where glycerol could form stable hydrogen bond with sago starch. This preliminary study demonstrated that the stress at maximum load was only applicable for lower glycerol/starch ratio of 30/70. The density of TPSS was inversely proportional to the increment of glycerol/starch ratio whereas moisture content and water absorption had opposite relationship.

scholarly journals Development and Characterization of Cornstarch-Based Bioplastics Packaging Film Using a Combination of Different Plasticizers

Polymers ◽  
2021 ◽  
Vol 13 (20) ◽  
pp. 3487
Author(s):  
Walid Abotbina ◽  
S. M. Sapuan ◽  
M. T. H. Sultan ◽  
M. F. M. Alkbir ◽  
R. A. Ilyas
Keyword(s):  
Tensile Strength ◽  
Moisture Content ◽  
Water Absorption ◽  
Food Packaging ◽  
The Other ◽  
Packaging Film ◽  
Film Properties ◽  
Selection Of

This work aims to develop cornstarch (CS) based films using fructose (F), glycerol (G), and their combination (FG) as plasticizers with different ratios for food packaging applications. The findings showed that F-plasticized film had the lowest moisture content, highest crystallinity among all films, and exhibited the highest tensile strength and thermostability. In contrast, G-plasticized films showed the lowest density and water absorption with less crystallinity compared to the control and the other plasticized film. In addition, SEM results indicated that FG-plasticized films had a relatively smoother and more coherent surface among the tested films. The findings have also shown that varying the concentration of the plasticizers significantly affected the different properties of the plasticized films. Therefore, the selection of a suitable plasticizer at an appropriate concentration may significantly optimize film properties to promote the utilization of CS films for food packaging applications.

scholarly journals Effect of temperature and moisture content on tensile behaviour of false banana fibre (Ensete ventricosum)

2017 ◽  
Vol 31 (3) ◽  
pp. 377-382 ◽  
Author(s):  
Cestmir Mizera ◽  
David Herak ◽  
Petr Hrabe ◽  
Abraham Kabutey
Keyword(s):  
Tensile Strength ◽  
Composite Materials ◽  
Relative Humidity ◽  
Moisture Content ◽  
Water Absorption ◽  
Mechanical Behaviour ◽  
Effect Of Temperature ◽  
Tensile Behaviour ◽  
Ensete Ventricosum ◽  
Banana Fibre

Abstract The mechanical behaviour of natural fibres as composite materials can be affected by changes in temperature and moisture content. The aim of this paper was to describe the effect of temperature and moisture content on tensile strength of false banana fibre (Ensete ventricosum) and to determine its water absorption. Samples of fibres were prepared and tested until rupture point with strain rate of 0.05 min−1 at temperature change between −20 and 220°C as well as moisture content between 10 and 90% wb. The water absorption and release of Ensete fibres at 60 and 90% relative humidity was also determined. Results showed that Ensete fibres exhibited stability of tensile strength in the temperature range from 0 to 100°C but the increase of temperature decreased statistically significantly the tensile strength. The effect of moisture content on tensile strength was not statistically significant. The equilibrium moisture content at 60% relative humidity and 25°C was determined.

Characterization and Preparation of Sago Starch (SS) Based Reinforced with Silver Nanoparticle (SNP)

2015 ◽  
Vol 1115 ◽  
pp. 369-372
Author(s):  
Zuraida Ahmad ◽  
A.K. Ahmad Ulwi ◽  
Tajuddin Maisarah ◽  
A. Maisarah
Keyword(s):  
Wound Healing ◽  
Tensile Strength ◽  
Moisture Content ◽  
Amylose Content ◽  
Weight Ratio ◽  
Particle Sizes ◽  
Sago Starch ◽  
Weight Percentage ◽  
Particulate Reinforcement ◽  
Sliver Nanoparticles

This paper reported on the properties of sago starch (SS) films impregnated with different concentration of sliver nanoparticles (SNP) of 100, 2000, 5000 rpm with weight ratio of 1% and 10% to be used as wound healing material. The SS films were prepared through film moulding technique by mixing aqueous SNP with SS, glycerol and water at weight percentage of 6.5:3.5:90. The performance of SS-SNP films produced is studied. The morphology study shows the existence of SNP embedded in the SS particles. SNP with 2000ppm has the biggest particle width but small in particle sizes, which make the SS-SNP film of 2000ppm is superior in thickness, denser and has lower moisture content compared to other SS-SNP film with different composition. The highest water absorption occurred in the SS-SNP of 100ppm, due to the high existence of pores in the network of amylose content in starch. SNP act as particulate reinforcement in the SS film meaning higher number of ppm made the film more brittle and easy to rupture. Thus, the SS-SNP film of 5000ppm has the lowest tensile strength and modulus for tensile strength and modulus. It can be concluded that the SS-SNP film of 2000ppm is suitable to be used as wound healing material, as the addition of 2000ppm SNP inside the SS films help in improving the properties of SS-SNP film produced.

scholarly journals Utilization of Pitali (Trewia nudiflora) for Manufacturing Commercial Plywood in Bangladesh

1970 ◽  
Vol 43 (4) ◽  
pp. 581-587
Author(s):  
M Hasan Shahria ◽  
M Ashaduzzaman ◽  
M Iftekhar Shams ◽  
Arifa Sharmin ◽  
M Muktarul Islam
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Moisture Content ◽  
Physical Properties ◽  
Water Absorption ◽  
Linear Expansion ◽  
Urea Formaldehyde ◽  
Physical And Mechanical Properties ◽  
Thickness Swelling ◽  
Trewia Nudiflora

The study was conducted to find out the potentiality of Pitali (Trewia nudiflora) for manufacturing commercial plywood and evaluating its physical and mechanical properties. Two 9-ply plywood of 2.4m x 1.2m x 18mm size were manufactured using liquid urea formaldehyde adhesive. The physical and mechanical properties of T. nudiflora plywood were compared with the existing market available plywood manufactured by Simul (Bombax ceiba). It was found that density were 509.82 kg/m3 and 490.96 kg/m3, moisture content after curing were 10.67% and 17.61%, thickness swelling were 6.90% and 7.29%, linear expansion were 0.19% and 0.15%, water absorption were 50.89% and 64.79%, MOR were 29.94 N/mm2 and 27.05 N/mm2, MOE were 1613.89 N/mm2 and 1160.68 N/mm2, and tensile strength were 14.75 N/mm2 and 13.12 N/mm2 for T. nudiflora plywood and market plywood respectively. The evaluated physical and mechanical properties of T. nudiflora plywood were also compared with some relevant results and standards reported earlier. Key Words: Plywood, Trewia nudiflora, Physical properties, Mechanical properties. doi: 10.3329/bjsir.v43i4.2249 Bangladesh J. Sci. Ind. Res. 43(4),581-587, 2008

scholarly journals MECHANICAL AND PHYSICAL PROPERTIES OF THERMOPLASTIC CORN STARCH

2021 ◽  
Vol 83 (5) ◽  
pp. 119-127
Author(s):  
Nazri Huzaimi Zakaria ◽  
Ridhwan Jumaidin ◽  
Mohd Adrinata Shaharuzaman ◽  
Mohd Rody Mohamad Zin ◽  
Fudhail Abdul Munir
Keyword(s):  
Tensile Strength ◽  
Moisture Content ◽  
Physical Properties ◽  
Water Absorption ◽  
Corn Starch ◽  
Absorption Test ◽  
Physical Test ◽  
Biodegradable Composite ◽  
Mechanical And Physical Properties ◽  
Water Absorption Test

The awareness to produce biodegradable composite has increased rapidly because of non-toxic and reachable. However, fully biodegradable composite production still low due to the matrix used in the composite is not biodegradable. Thus, this paper presents the study on mechanical and physical properties for the mixtures of corn starch (CS) with different weight percentages of glycerol as thermoplastics corn starch (TPCS) matrix. The selected glycerol contents were at 30, 35 and 40 wt%. The mixtures of CS and different weight percentages of glycerol were made using hot compression moulding at 165°C for 15 minutes to produce the TPCS samples. The mechanical and physical properties were done: the tensile test, hardness test, water absorption test, moisture content test and microstructure analysis under the Scanning Electron Microscopes (SEM). Incorporating 30 wt% loadings of glycerol has increased the tensile strength and hardness. The results show that the addition of higher than 30 wt% loadings of glycerol has decreased the tensile strength and hardness of the TPCS. The physical test results for 30 wt% loadings of glycerol for water absorption test and moisture content show the lowest value than other TPCS samples. However, the density value for all wt% loadings of glycerol does not offer much difference. It reveals that 30 wt% loadings of glycerol in the mixture of CS have shown a good interaction in the TPCS mechanical properties. Based on this finding, the TPCS has huge potential to be used as a matrix to develop a fully biodegradable composite.

scholarly journals Mechanical Characteristic and Water Absorption Property of Bio Composite from Sago Starch and Jute Fiber (Boehmeria Nivea) as the filler

2021 ◽  
Vol 2 (1) ◽  
pp. 94-99
Author(s):  
Rozanna Dewi ◽  
Oktaviani Oktaviani ◽  
Zainuddin Ginting ◽  
Novi Sylvia
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Water Absorption ◽  
Modulus Of Elasticity ◽  
High Water ◽  
Thermoplastic Starch ◽  
Absorption Capacity ◽  
Sago Starch ◽  
Hemp Fiber ◽  
Water Absorption Property

Environmentally friendly plastics can be degraded biologically in an anaerobic environment. This plastic is synthesized from starch such as sago starch which is available in abundance. In the form of bioplastics, its mechanical properties are still not compared to conventional plastics derived from crude oil, so its application is limited. The incorporation of filler material increases its mechanical properties, one of the selected fillers is hemp fiber as used in this study. Thermoplastic starch from sago with flax fiber as a filler and the addition of Polypropylene to improve mechanical properties with a certain composition to maintain its natural biodegradability. The mechanical properties analyzed were tensile strength, elongation and modulus of elasticity. Water absorption tests were also carried out to observe the water resistance properties. The results of the tensile strength test showed that the best tensile strength value of 9.32 Mpa was obtained at the addition of 35% fiber with a TPS: PP ratio of 1:1.5. The same conditions were obtained for the percent elongation with the results of 10.16% and the modulus of elasticity was 91.73 Mpa. Water absorption showed that 55% filler gave the lowest water     absorption, namely 4.41% at a ratio of TPS: PP 1:0.5. The addition of fiber filler into the bio-composite affects the tensile strength,    elongation and modulus of elasticity, the higher the volume of filler entering the bio-composite, the lower the value of tensile strength, elongation and modulus of elasticity, or vice versa. The ratio of addition of polypropylene matrix is also influential, the higher the ratio contributes to the tensile strength, elongation and higher modulus of elasticity. High water absorption capacity will reduce the performance of biocomposite, so the lower the water absorption ability, the better the quality of the biocomposite product and the wider its application

scholarly journals Melt- vs. Non-Melt Blending of Complexly Processable Ultra-High Molecular Weight Polyethylene/Cellulose Nanofiber Bionanocomposite

Polymers ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 404
Author(s):  
Nur Sharmila Sharip ◽  
Hidayah Ariffin ◽  
Tengku Arisyah Tengku Yasim-Anuar ◽  
Yoshito Andou ◽  
Yuki Shirosaki ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Molecular Weight ◽  
Tensile Strength ◽  
Yield Strength ◽  
Young’S Modulus ◽  
High Molecular Weight ◽  
Melt Processing ◽  
Cellulose Nanofiber ◽  
Melt Blending ◽  
Ultra High Molecular Weight

The major hurdle in melt-processing of ultra-high molecular weight polyethylene (UHMWPE) nanocomposite lies on the high melt viscosity of the UHMWPE, which may contribute to poor dispersion and distribution of the nanofiller. In this study, UHMWPE/cellulose nanofiber (UHMWPE/CNF) bionanocomposites were prepared by two different blending methods: (i) melt blending at 150 °C in a triple screw kneading extruder, and (ii) non-melt blending by ethanol mixing at room temperature. Results showed that melt-processing of UHMWPE without CNF (MB-UHMWPE/0) exhibited an increment in yield strength and Young’s modulus by 15% and 25%, respectively, compared to the Neat-UHMWPE. Tensile strength was however reduced by almost half. Ethanol mixed sample without CNF (EM-UHMWPE/0) on the other hand showed slight decrement in all mechanical properties tested. At 0.5% CNF inclusion, the mechanical properties of melt-blended bionanocomposites (MB-UHMWPE/0.5) were improved as compared to Neat-UHMWPE. It was also found that the yield strength, elongation at break, Young’s modulus, toughness and crystallinity of MB-UHMWPE/0.5 were higher by 28%, 61%, 47%, 45% and 11%, respectively, as compared to the ethanol mixing sample (EM-UHMWPE/0.5). Despite the reduction in tensile strength of MB-UHMWPE/0.5, the value i.e., 28.4 ± 1.0 MPa surpassed the minimum requirement of standard specification for fabricated UHMWPE in surgical implant application. Overall, melt-blending processing is more suitable for the preparation of UHMWPE/CNF bionanocomposites as exhibited by their characteristics presented herein. A better mechanical interlocking between UHMWPE and CNF at high temperature mixing with kneading was evident through FE-SEM observation, explains the higher mechanical properties of MB-UHMWPE/0.5 as compared to EM-UHMWPE/0.5.

scholarly journals Influence of Mechanical Vibration Moulding Process on the Tensile Properties of TiC Reinforced LM6 Alloy Composite Castings

2011 ◽  
Vol 66-68 ◽  
pp. 1207-1212 ◽  
Author(s):  
Mohd Sayuti ◽  
Shamsuddin Sulaiman ◽  
B.T. Hang Tuah Baharudin ◽  
M.K.A.M. Arifin ◽  
T.R. Vijayaram ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Titanium Carbide ◽  
Tensile Properties ◽  
Mechanical Vibration ◽  
Weight Fraction ◽  
Tensile Tests ◽  
Alloy Matrix ◽  
Remarkable Effect ◽  
Moulding Process ◽  
Particulate Reinforced

Vibrational moulding process has a remarkable effect on the properties of castings during solidification processing of metals, alloys, and composites. This research paper discusses on the investigation of mechanical vibration mould effects on the tensile properties of titanium carbide particulate reinforced LM6 aluminium alloy composites processed with the frequencies of 10.2 Hz, 12 Hz and 14 Hz. In this experimental work, titanium carbide particulate reinforced LM6 composites were fabricated by carbon dioxide sand moulding process. The quantities of titanium carbide particulate added as reinforcement in the LM6 alloy matrix were varied from 0.2% to 2% by weight fraction. Samples taken from the castings and tensile tests were conducted to determine the tensile strength and modulus of elasticity. The results showed that tensile strength of the composites increased with an increase in the frequency of vibration and increasing titanium carbide particulate reinforcement in the LM6 alloy matrix.

scholarly journals Effect of Moisture Content on the Processing and Mechanical Properties of a Biodegradable Polyester

Polymers ◽  
2021 ◽  
Vol 13 (10) ◽  
pp. 1616
Author(s):  
Vincenzo Titone ◽  
Antonio Correnti ◽  
Francesco Paolo La Mantia
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Moisture Content ◽  
Mechanical Testing ◽  
Hydrolytic Degradation ◽  
Slight Reduction ◽  
Biodegradable Polyester ◽  
Molding Process ◽  
Elongation At Break ◽  
Effect Of Moisture

This work is focused on the influence of moisture content on the processing and mechanical properties of a biodegradable polyester used for applications in injection molding. The pellets of the biodegradable polyester were exposed under different relative humidity conditions at a constant temperature before being compression molded. The compression-molded specimens were again placed under the above conditions before the mechanical testing. With all these samples, it is possible to determine the effect of moisture content on the processing and mechanical properties separately, as well as the combined effect of moisture content on the mechanical properties. The results obtained showed that the amount of absorbed water—both before processing and before mechanical testing—causes an increase in elongation at break and a slight reduction of the elastic modulus and tensile strength. These changes have been associated with possible hydrolytic degradation during the compression molding process and, in particular, with the plasticizing action of the moisture absorbed by the specimens.

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