Manufacture and Tribological Properties of C/C-SiC Brake Composites Fabricated by Warm Compacted In Situ Reaction

2010 ◽  
Vol 97-101 ◽  
pp. 1665-1668 ◽  
Author(s):  
Xiao Peng ◽  
Li Zhuan ◽  
Xiong Xiang

Carbon fibre reinforced carbon and silicon carbide dual matrix composites (C/C-SiC) were fabricated by warm compacted in-situ reaction. The C/C-SiC composites microstructure and tribological properties at different brake speeds were investigated. The results indicated that the composites were composed of 58 wt% C, 37 wt% SiC and 5 wt% Si. The density and open porosity were 2.0 g•cm-3 and 10%, respectively. The C/C-SiC brake composites show excellent tribological performance, including a good stability of brake, the coefficient of friction between 0.57 and 0.67, and the wear rate less than 2.02 cm3•MJ-1. These results show that the C/C-SiC brake composites are the promising candidates for advanced brake and clutch systems.

2012 ◽  
Vol 268-270 ◽  
pp. 59-62
Author(s):  
Zhuan Li ◽  
Peng Xiao ◽  
Xiang Xiong

C/C-SiC brake composites, based on reinforcement of carbon fiber and dual matrix of carbon and silicon carbide, were fabricated by warm compacted-in situ reacted process. Rules about the influence of different components on the friction and wear characteristics of the C/C-SiC composites are ascertained. As hard particle, the SiC has the function to the formation of friction film, which is in favor of increasing the coefficient of friction (COF) and decreasing the wear rate. The resin carbon plays the role of enhancing the COF, but they are easy to be cut and increase the wear rate. The graphite plays the lubrication function, and right volume content of graphite is helpful to forming friction film to reduce the wear rate. The C/C-SiC composite fabricated by the warm compacted-in situ reaction can with best tribological performance when the components volume fraction of carbon fibre, SiC, graphite and resin carbon are 15.5%, 37.0%, 22.1% and 20.8%, respectively, which the COF and the wear rate can reach the maximum and the minimun value of 0.44 and 1.1μm/cycle respectively.


2003 ◽  
Vol 125 (3) ◽  
pp. 661-669 ◽  
Author(s):  
Masaya Kurokawa ◽  
Yoshitaka Uchiyama ◽  
Tomoaki Iwai ◽  
Susumu Nagai

Tribological properties of several kinds of polyoxymethylene (POM) composites were evaluated for the purpose of developing a polymeric tribomaterial especially suited for mating with aluminum parts having low surface hardness. POM composites containing small amounts of silicon carbide (SiC), POM/SiC; those containing a small amount of calcium octacosanonoate besides SiC, POM/SiC/Ca-OCA; and the one blended with 24 wt % of polytetrafluoroethylene, POM/PTFE(24); were injection-molded into pin specimens and their tribological properties were tested by means of a pin-on-disk type wear apparatus using an aluminum (A5056) mating disk in comparison with a 303 stainless steel (SUS303) disk. Evaluation was focused on observation of the sliding surfaces of the pin specimens and the mating disks by a scanning electron microscope and an optical microscope together with the measurement of surface roughness. In the case of mating against a SUS303 disk having high surface hardness, all pin specimens did not roughen the disk surfaces even after long time of rubbing. Only POM/PTFE(24) composite obviously made a transfer film on the disk surface, while the other composites made an extremely thin one on it. POM/SiC(0.1)/Ca-OCA(1) composite, containing SiC 0.1 wt. % and Ca-OCA 1 wt. %, was found to show the lowest coefficient of friction and the lowest wear rate forming extremely thin transfer film on the mating disk. On the other hand, against an A5056 disk which has lower surface hardness than that of SUS303 disk, unfilled POM and POM composites except POM/SiC(0.1)/Ca-OCA(1) composite roughened the disk surfaces. However, the sliding surface of the A5056 disk rubbed with POM/SiC(0.1)/Ca-OCA(1) composite was significantly smoother and that of the pin specimen was also quite smooth in comparison with other pin specimens. Further, when each POM composite was rubbed against the A5056 disk, formation of transfer film was not obvious on the disk surfaces. For POM/SiC(0.1)/Ca-OCA(1) composite, the wear rate was the lowest of all POM composites, and the coefficient of friction was as low level as 60 percent of that of unfilled POM, but slightly higher than that of POM/PTFE(24) composite. For POM/SiC(0.1)/Ca-OCA(1) composite, the nucleating effect of SiC and Ca-OCA, which accelerated the crystallization of POM during its injection molding to form a matrix containing fine spherulites, must have resulted in increasing the toughness of the matrix and lowering the wear rate. Also, the lubricant effect of Ca-OCA should have lowered the coefficient of friction of the same matrix for rubbing against aluminum mating disk. POM/SiC(0.1)/Ca-OCA(1) composite was concluded as an excellent tribomaterial for mating with aluminum parts.


Tribologia ◽  
2019 ◽  
Vol 285 (3) ◽  
pp. 79-87 ◽  
Author(s):  
Jerzy MYALSKI ◽  
Andrzej Posmyk ◽  
Bartosz HEKNER ◽  
Marcin GODZIERZ

Carbon with an amorphous structure was used as a component to modify the tribological properties of engineering plastics. Its construction allows the formation of carbon-based wear products during friction, adhesively bonded to the surface of cooperating machine parts, acting as a solid lubricant. The work compares the tribological properties of two groups of composites with an aluminium alloy matrix in which glassy carbon appeared in the form of particles and an open cell foam fulfilling the role of strengthening the matrix. The use of spatial structures of reinforcement provides, in comparison with the strengthening of particles, homogeneity of carbon distribution in the entire volume of the composite. The tests carried out on a pin-disc tester showed that the use of spatial carbon structures in the composite ensures a greater coefficient of friction stability than when reinforcing with particles, and the coefficient of friction with a small proportion of carbon foams (about 1 wt%) is comparable with the coefficient of friction in the contact with composites containing 5-10% carbon particles in granular form.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3127 ◽  
Author(s):  
Xiaojie Wang ◽  
Xiumin Yao ◽  
Hui Zhang ◽  
Xuejian Liu ◽  
Zhengren Huang

Mesocarbon microbead–silicon carbide (MCMB–SiC) composites with 0–30 wt % MCMBs were prepared by pressureless sintering (PLS) method at 2200 °C in Ar. The microstructure and tribological properties of the prepared composites were investigated. The results show that there was a finer grain size of SiC with the increase in MCMB content because MCMBs hinder the growth of SiC grains. The hardness of the composites decreased with increasing MCMB content, whereas the fracture toughness fluctuated showing a complex trend. The tribological properties of the composites under dry friction conditions were evaluated using the pin-on-disk method against a SiC counterpart. We found that the tribological properties of the samples were influenced by the oxide film or lubricating film that formed during the wear process on wear surfaces. Different wear mechanisms were found to be associated with differing MCMB contents.


Tribology ◽  
2005 ◽  
Author(s):  
Abdulhaqq Q. Hamid ◽  
Sataish C. Jain ◽  
Prakriti K. Ghosh ◽  
Subrata Ray

Aluminum alloy-based cast in-situ composite has been synthesized by dispersion of externally added molybdenum trioxide particles (MoO3) in molten aluminum at the processing temperature of 850 °C. During processing, displacement reaction between molten aluminum and MoO3 particles, results in formation of alumina particles in-situ also releases molybdenum into molten aluminum. A part of this molybdenum forms solid -solution with aluminum and the remaining part reacts with aluminum to form intermetallic phase Mo(Al1−xFex)12 of different morphologies. Magnesium (Mg) is added to the melt in order to help wetting of alumina particles generated in-situ, by molten aluminum and help to retain these particles inside the melt. The mechanical properties (ultimate tensile stress, yield stress, percentage elongation and hardness) of the cast in-situ composite are relatively higher than those observed either in cast commercial aluminum or in cast Al-Mo alloys. The wear and friction of the resulting cast in-situ Al(Mg, Mo)Al2O3(MoO3) composites have been investigated using a pin-on-disc wear testing machine, at different normal loads of 9.8, 14.7, 19.6, 24.5, 29.4, 34.3 and 39.2 N and a constant sliding speed of 1.05 m/s, under dry sliding conditions. The results indicate that the cumulative volume loss and wear rate of cast in-situ composites are significantly lower than those observed either in cast commercial aluminum or in cast Al-Mo alloy, under similar load and sliding conditions. Beyond about 30-35 N loads, there appears to be a higher rate of increase in the wear rate in the cast in-situ composite as well as in cast commercial aluminum and cast Al-Mo alloy. For a given normal load, the coefficient of friction of cast in-situ composite is significantly lower than those observed either in cast commercial aluminum or cast Al-Mo alloy. The coefficient of friction of cast in-situ composite increases gradually with increasing normal load while those observed in cast commercial aluminum or cast Al-Mo alloy remain more or less the same. Beyond a critical normal load of about 30-35 N, the coefficient of friction decreases with increasing normal load in all the three materials.


Polymers ◽  
2021 ◽  
Vol 13 (24) ◽  
pp. 4295
Author(s):  
Hai Wang ◽  
Annan Sun ◽  
Xiaowen Qi ◽  
Yu Dong ◽  
Bingli Fan

The tribological properties of polytetrafluoroethylene (PTFE)/AP (poly(para-phenyleneterephthalamide) (PPTA) pulp) composites under different test conditions (load: 2N, 10N; frequency: 1 Hz, 4 Hz; amplitude: 2 mm, 8 mm) were holistically evaluated. PTFE/AP composites with different AP mass ratios of 3%, 6%, and 12% as a skeleton support material were prepared. The coefficient of friction (COF) and wear rate were determined on a ball-on-disk tribometer. Furthermore, the morphology, element composition, and chemical structure of the transfer membrane were analyzed accordingly. The relationships between load, frequency, amplitude, and tribological properties were further investigated. According to the wear mechanism, AP enables effective improvement in the stiffness and wear resistance, which is also conducive to the formation of transfer films.


1996 ◽  
Vol 436 ◽  
Author(s):  
K. T. Kern ◽  
K. C. Walter ◽  
S. Fayeulle ◽  
A. J. Griffin ◽  
H. Kung ◽  
...  

AbstractSamples of steel with high chrome content were implanted separately with 75 keV nitrogen ions and with 75 keV boron ions. Implanted doses of each ion species were 2-,4- and 8 × 1017 /cm2. Retained doses were measured using resonant non-Rutherford Backscattering Spectrometry. Tribological properties were determined using a pin-ondisk test with a 6-mm diameter ruby pin with a velocity of 0.94 m/min. Testing was done at 10% humidity with a load of 377g. Wear rate and coefficient of friction were determined from these tests. While reduction in the wear rate for nitrogen implanted materials was observed, greater reduction (more than an order of magnitude) was observed for boron implanted materials. In addition, reduction in the coefficient of friction for high-dose boron implanted materials was observed. Nano-indentation revealed a hardened layer near the surface of the material. Results from grazing incidence x-ray diffraction suggest the formation of Fe2N and Fe3N in the nitrogen implanted materials and Fe3B in the boron implanted materials. Results from transmission electron microscopy will be presented.


2000 ◽  
Vol 122 (4) ◽  
pp. 809-814 ◽  
Author(s):  
Masaya Kurokawa ◽  
Yoshitaka Uchiyama ◽  
Susumu Nagai

Tribological properties of polyoxymethylene (POM) composites containing a trace amount of silicon carbide (SiC) and/or calcium salt of octacosanoic acid (Ca-OCA) as well as containing polytetrafluoroethylene (PTFE) were investigated by means of a pin-on-disk type wear apparatus. The spherulite size of POM composites was measured using a polarizing microscope. Mechanical properties and gear performance of the composites were also evaluated. It was found that the coefficient of friction was drastically lowered due to the lubricant effect of Ca-OCA added to POM/SiC composites. Further, the wear rate was also decreased by the nucleating effect of SiC and Ca-OCA. Especially, POM/SiC(0.1)/Ca-OCA(1) composite containing SiC 0.1 wt.% and Ca-OCA 1 wt.% showed the coefficient of friction as low as that of POM/PTFE(24) composite containing PTFE 24 wt.%, keeping higher wear resistance. Also, its mechanical properties were found to be the same level as those of unfilled POM, except that its izod impact strength became higher than that of unfilled POM. Furthermore, its gear performance was confirmed to be satisfactory without generating noise under the dry running condition, when the same gears were combined below 13 MPa of bending stress. [S0742-4787(00)00304-0]


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4217
Author(s):  
Üsame Ali Usca ◽  
Mahir Uzun ◽  
Mustafa Kuntoğlu ◽  
Serhat Şap ◽  
Khaled Giasin ◽  
...  

Tribological properties of engineering components are a key issue due to their effect on the operational performance factors such as wear, surface characteristics, service life and in situ behavior. Thus, for better component quality, process parameters have major importance, especially for metal matrix composites (MMCs), which are a special class of materials used in a wide range of engineering applications including but not limited to structural, automotive and aeronautics. This paper deals with the tribological behavior of Cu-B-CrC composites (Cu-main matrix, B-CrC-reinforcement by 0, 2.5, 5 and 7.5 wt.%). The tribological characteristics investigated in this study are the coefficient of friction, wear rate and weight loss. For this purpose, four levels of sliding distance (1000, 1500, 2000 and 2500 m) and four levels of applied load (10, 15, 20 and 25 N) were used. In addition, two levels of sliding velocity (1 and 1.5 m/s), two levels of sintering time (1 and 2 h) and two sintering temperatures (1000 and 1050 °C) were used. Taguchi’s L16 orthogonal array was used to statistically analyze the aforementioned input parameters and to determine their best levels which give the desired values for the analyzed tribological characteristics. The results were analyzed by statistical analysis, optimization and 3D surface plots. Accordingly, it was determined that the most effective factor for wear rate, weight loss and friction coefficients is the contribution rate. According to signal-to-noise ratios, optimum solutions can be sorted as: the highest levels of parameters except for applied load and reinforcement ratio (2500 m, 10 N, 1.5 m/s, 2 h, 1050 °C and 0 wt.%) for wear rate, certain levels of all parameters (1000 m, 10 N, 1.5 m/s, 2 h, 1050 °C and 2.5 wt.%) for weight loss and 1000 m, 15 N, 1 m/s, 1 h, 1000 °C and 0 wt.% for the coefficient of friction. The comprehensive analysis of findings has practical significance and provides valuable information for a composite material from the production phase to the actual working conditions.


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