scholarly journals Experimental and Analytical Investigations on Tribological Properties of PTFE/AP Composites

Polymers ◽  
2021 ◽  
Vol 13 (24) ◽  
pp. 4295
Author(s):  
Hai Wang ◽  
Annan Sun ◽  
Xiaowen Qi ◽  
Yu Dong ◽  
Bingli Fan

The tribological properties of polytetrafluoroethylene (PTFE)/AP (poly(para-phenyleneterephthalamide) (PPTA) pulp) composites under different test conditions (load: 2N, 10N; frequency: 1 Hz, 4 Hz; amplitude: 2 mm, 8 mm) were holistically evaluated. PTFE/AP composites with different AP mass ratios of 3%, 6%, and 12% as a skeleton support material were prepared. The coefficient of friction (COF) and wear rate were determined on a ball-on-disk tribometer. Furthermore, the morphology, element composition, and chemical structure of the transfer membrane were analyzed accordingly. The relationships between load, frequency, amplitude, and tribological properties were further investigated. According to the wear mechanism, AP enables effective improvement in the stiffness and wear resistance, which is also conducive to the formation of transfer films.

2003 ◽  
Vol 125 (3) ◽  
pp. 661-669 ◽  
Author(s):  
Masaya Kurokawa ◽  
Yoshitaka Uchiyama ◽  
Tomoaki Iwai ◽  
Susumu Nagai

Tribological properties of several kinds of polyoxymethylene (POM) composites were evaluated for the purpose of developing a polymeric tribomaterial especially suited for mating with aluminum parts having low surface hardness. POM composites containing small amounts of silicon carbide (SiC), POM/SiC; those containing a small amount of calcium octacosanonoate besides SiC, POM/SiC/Ca-OCA; and the one blended with 24 wt % of polytetrafluoroethylene, POM/PTFE(24); were injection-molded into pin specimens and their tribological properties were tested by means of a pin-on-disk type wear apparatus using an aluminum (A5056) mating disk in comparison with a 303 stainless steel (SUS303) disk. Evaluation was focused on observation of the sliding surfaces of the pin specimens and the mating disks by a scanning electron microscope and an optical microscope together with the measurement of surface roughness. In the case of mating against a SUS303 disk having high surface hardness, all pin specimens did not roughen the disk surfaces even after long time of rubbing. Only POM/PTFE(24) composite obviously made a transfer film on the disk surface, while the other composites made an extremely thin one on it. POM/SiC(0.1)/Ca-OCA(1) composite, containing SiC 0.1 wt. % and Ca-OCA 1 wt. %, was found to show the lowest coefficient of friction and the lowest wear rate forming extremely thin transfer film on the mating disk. On the other hand, against an A5056 disk which has lower surface hardness than that of SUS303 disk, unfilled POM and POM composites except POM/SiC(0.1)/Ca-OCA(1) composite roughened the disk surfaces. However, the sliding surface of the A5056 disk rubbed with POM/SiC(0.1)/Ca-OCA(1) composite was significantly smoother and that of the pin specimen was also quite smooth in comparison with other pin specimens. Further, when each POM composite was rubbed against the A5056 disk, formation of transfer film was not obvious on the disk surfaces. For POM/SiC(0.1)/Ca-OCA(1) composite, the wear rate was the lowest of all POM composites, and the coefficient of friction was as low level as 60 percent of that of unfilled POM, but slightly higher than that of POM/PTFE(24) composite. For POM/SiC(0.1)/Ca-OCA(1) composite, the nucleating effect of SiC and Ca-OCA, which accelerated the crystallization of POM during its injection molding to form a matrix containing fine spherulites, must have resulted in increasing the toughness of the matrix and lowering the wear rate. Also, the lubricant effect of Ca-OCA should have lowered the coefficient of friction of the same matrix for rubbing against aluminum mating disk. POM/SiC(0.1)/Ca-OCA(1) composite was concluded as an excellent tribomaterial for mating with aluminum parts.


2020 ◽  
Vol 992 ◽  
pp. 745-750
Author(s):  
A.P. Vasilev ◽  
T.S. Struchkova ◽  
A.G. Alekseev

This paper presents the results from the investigation of effect the carbon fibers with tungsten disulfide on the mechanical and tribological properties of PTFE. Is carried out a comparison of mechanical and tribological properties of polymer composites PTFE-based with carbon fibers and PTFE with complex filler (carbon fibers with tungsten disulfide). It is shown that at a content of 8 wt.% CF+1 wt.% WS2 in PTFE, wear resistance increases significantly while maintaining the tensile strength, relative elongation at break and low coefficient of friction at the level of initial PTFE. The results of X-ray analysis and investigation of SEM supramolecular structure and friction surfaces of PTFE and polymer composites are presented. It is shown that the degree of crystallinity of polymer composites increases in comparison with the initial PTFE. The images of scanning electron microscope reveal that particles of tungsten disulfide concentrating on the friction surface is likely responsible to a reduction in the coefficient of friction and increase the wear resistance of PTFE-based polymer composites with complex fillers.


2010 ◽  
Vol 97-101 ◽  
pp. 1665-1668 ◽  
Author(s):  
Xiao Peng ◽  
Li Zhuan ◽  
Xiong Xiang

Carbon fibre reinforced carbon and silicon carbide dual matrix composites (C/C-SiC) were fabricated by warm compacted in-situ reaction. The C/C-SiC composites microstructure and tribological properties at different brake speeds were investigated. The results indicated that the composites were composed of 58 wt% C, 37 wt% SiC and 5 wt% Si. The density and open porosity were 2.0 g•cm-3 and 10%, respectively. The C/C-SiC brake composites show excellent tribological performance, including a good stability of brake, the coefficient of friction between 0.57 and 0.67, and the wear rate less than 2.02 cm3•MJ-1. These results show that the C/C-SiC brake composites are the promising candidates for advanced brake and clutch systems.


1996 ◽  
Vol 436 ◽  
Author(s):  
K. T. Kern ◽  
K. C. Walter ◽  
S. Fayeulle ◽  
A. J. Griffin ◽  
H. Kung ◽  
...  

AbstractSamples of steel with high chrome content were implanted separately with 75 keV nitrogen ions and with 75 keV boron ions. Implanted doses of each ion species were 2-,4- and 8 × 1017 /cm2. Retained doses were measured using resonant non-Rutherford Backscattering Spectrometry. Tribological properties were determined using a pin-ondisk test with a 6-mm diameter ruby pin with a velocity of 0.94 m/min. Testing was done at 10% humidity with a load of 377g. Wear rate and coefficient of friction were determined from these tests. While reduction in the wear rate for nitrogen implanted materials was observed, greater reduction (more than an order of magnitude) was observed for boron implanted materials. In addition, reduction in the coefficient of friction for high-dose boron implanted materials was observed. Nano-indentation revealed a hardened layer near the surface of the material. Results from grazing incidence x-ray diffraction suggest the formation of Fe2N and Fe3N in the nitrogen implanted materials and Fe3B in the boron implanted materials. Results from transmission electron microscopy will be presented.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4217
Author(s):  
Üsame Ali Usca ◽  
Mahir Uzun ◽  
Mustafa Kuntoğlu ◽  
Serhat Şap ◽  
Khaled Giasin ◽  
...  

Tribological properties of engineering components are a key issue due to their effect on the operational performance factors such as wear, surface characteristics, service life and in situ behavior. Thus, for better component quality, process parameters have major importance, especially for metal matrix composites (MMCs), which are a special class of materials used in a wide range of engineering applications including but not limited to structural, automotive and aeronautics. This paper deals with the tribological behavior of Cu-B-CrC composites (Cu-main matrix, B-CrC-reinforcement by 0, 2.5, 5 and 7.5 wt.%). The tribological characteristics investigated in this study are the coefficient of friction, wear rate and weight loss. For this purpose, four levels of sliding distance (1000, 1500, 2000 and 2500 m) and four levels of applied load (10, 15, 20 and 25 N) were used. In addition, two levels of sliding velocity (1 and 1.5 m/s), two levels of sintering time (1 and 2 h) and two sintering temperatures (1000 and 1050 °C) were used. Taguchi’s L16 orthogonal array was used to statistically analyze the aforementioned input parameters and to determine their best levels which give the desired values for the analyzed tribological characteristics. The results were analyzed by statistical analysis, optimization and 3D surface plots. Accordingly, it was determined that the most effective factor for wear rate, weight loss and friction coefficients is the contribution rate. According to signal-to-noise ratios, optimum solutions can be sorted as: the highest levels of parameters except for applied load and reinforcement ratio (2500 m, 10 N, 1.5 m/s, 2 h, 1050 °C and 0 wt.%) for wear rate, certain levels of all parameters (1000 m, 10 N, 1.5 m/s, 2 h, 1050 °C and 2.5 wt.%) for weight loss and 1000 m, 15 N, 1 m/s, 1 h, 1000 °C and 0 wt.% for the coefficient of friction. The comprehensive analysis of findings has practical significance and provides valuable information for a composite material from the production phase to the actual working conditions.


Author(s):  
S Rambabu ◽  
N Ramesh Babu

This article covers the efforts on characterising ice-bonded abrasive polishing tool in terms of the mechanical and tribological properties such as hardness, coefficient of friction, and wear rate. These studies were attempted on the tools prepared at different temperatures ranging from −10 °C to 0 °C with a view to identify the condition suitable to prepare ice-bonded abrasive polishing tool for effective polishing of Ti–6Al–4V alloy specimen. It also presents the methods adopted to determine various properties of ice-bonded abrasive polishing tool. Hardness was estimated from the measured penetration depth of cone shape indenter into the tool, coefficient of friction was determined from the change in power drawn by the motor rotating the tool mould, and wear behaviour of tool was assessed from the melting rate of the tool determined from the change in height of ice-bonded abrasive polishing tool at different stages of polishing. From the results of this study, it is clear that ice-bonded abrasive polishing tool prepared at −4 °C has possessed sufficient hardness, coefficient of friction, and reasonable wear rate suitable for polishing of Ti–6Al–4V specimens. This article also covers the details of low-temperature coolant supply unit developed to prepare the ice-bonded abrasive polishing tool at any desired temperature between 0 °C and −40 °C and thus to maintain it for a long time. Polishing studies with such ice-bonded abrasive polishing tool showed 72% improvement in finish after 90 min of polishing of Ti–6Al–4V specimen with tool, prepared at −4 °C.


Author(s):  
M.N. Obaid ◽  
S.H. Radhi

Purpose: The number of people suffering from Degenerative Disc Disease (DDD) is increasing. The disease causes heavy pain and restrict a number of day-to-day life activities. In extreme cases, the degraded disc is removed under total disc replacement which is usually made up of Ultra-High Molecular Weight Polyethylene (UHMWPE). The material has astounding biocompatible characteristics mechanical properties and wear resistance. However, these characteristics are insufficient in arthroplasty application. Therefore, research investigations are ongoing to improve tribological properties through reinforcement that may result in a composite material of UHMWPE. Thus the current study is aimed at reinforcing UHMWPE with short fibres of polyesters to enhance the tribological properties and surface characteristic so as to improve wear resistance and nourish the fibroblast cells on synthetic disc. Design/methodology/approach: The researcher prepared UHMWPE composite material, reinforced with different weight fractions of short polyester fibres (2, 4, 6, 8 and 10% following hot press method. Further pin-on-disc device was used to study the tribological properties (coefficient of friction and volume of wear). The study tested surface roughness and surface characteristics by atomic force microscopy (AFM) device, hardness by shore D device, contact angle to study the effect of polyester short fibres on wettability of UHMWPE surface and tested the thermal properties and crystalline degree using Differential Scanning Calorimetry measurement (DSC) device. Findings: The results infer that the wear resistance got improved when using 2% w.t polyester though it got decreased initially. However, the value was still more than neat UHMWPE. There was a decrease observed in coefficient of friction, but after 4 w.t% polyester, the coefficient of friction got increased due to increasing percentage of fibres which make it harder and stiff compared to UHMWPE. There was a decline observed in surface roughness due to alignment of the fibres with smooth surface. The contact angle got increased in a moderate range while the roughness enhanced the growth of fibroblast cell. The hardness of composite material got increased, because the fibres turned stiffer and harder than the matrix. DSC results infer the improvements in thermal stability due to high thermal properties of polyester fibres compared to UHMWPE. The degree of crystallinity got increased which in turn enhanced wear resistance, especially at 6 w.t % polyester fibres. There was a mild increase observed in density since the density of polyester is higher than polymer. Research limitations/implications: The major challenge was the dispersion of fibres. Uniform distribution of fibres within the matrix (UHMWPE) was achieved through two steps of mixing processes such as mechanical mixture and twin extruder. In future studies, fatigue tests must be conducted to study the behaviour of prepared composite materials under fatigue cycle. Practical implications: A significant objective is how to connect among different properties to obtain good improvement in tribological and surface properties so as to enhance wear resistance and growth of fibrolase cells. Originality/value: In this study, polymeric short fibres were used as reinforcement with polymeric matrix to enhance the wettability of fibres with matrix. In this way, the bonding among them got increased which supports the tribological, surface, and crystalline behaviour.


2020 ◽  
Author(s):  
Alexey Vereschaka ◽  
Sergey Grigoriev ◽  
Vladimir Tabakov ◽  
Mars Migranov ◽  
Nikolay Sitnikov ◽  
...  

The chapter discusses the tribological properties of samples with multilayer composite nanostructured Ti-TiN-(Ti,Cr,Al,Si)N, Zr-ZrN-(Nb,Zr,Cr,Al)N, and Zr-ZrN-(Zr,Al,Si)N coatings, as well as Ti-TiN-(Ti,Al,Cr)N, with different values of the nanolayer period λ. The relationship between tribological parameters, a temperature varying within a range of 20–1000°C, and λ was investigated. The studies have found that the adhesion component of the coefficient of friction (COF) varies nonlinearly with a pronounced extremum depending on temperature. The value of λ has a noticeable influence on the tribological properties of the coatings, and the nature of the mentioned influence depends on temperature. The tests found that for the coatings with all studied values of λ, an increase in temperature first caused an increase and then a decrease in COF.


2017 ◽  
Vol 25 (3) ◽  
pp. 193-198 ◽  
Author(s):  
A. Madhanagopal ◽  
S. Gopalakannan

This study determines the friction and the wear properties of the unidirectional glass epoxy composite with Gr, SiC TiO2 powder by using pin on disk apparatus. This tribological data is obtained in dry sliding condition for a constant sliding time of 30 minutes. Test specimens are prepared using hand lay-up process and by varying the different (2, 5, 7) percentage each of graphite and SiC, TiO2 particles addition for the combination of fiber and matrix. The tests are performed by varying the operating parameters of contact pressure (p) and velocity (v). The composites (2% 5%, and 7%) are worn by dry sliding at the steel counter face under ambient conditions. The coefficient of friction reaches maximum of 0.78 at 2 kg load, 2 m/s velocity with testing time duration of 24 min. whereas 5%, 7% sample shows the coefficient of friction 0.28, 0.25 respectively. The specific wear rate value drops to 0.79 (mm3/N-m×10−6) at 2 kg load at 2 m/s velocity for the 5% specimen. The maximum reduction in the specific wear rate at 3 kg load, 1m/s velocity is 32.7 percentages, 5.63 percentages for the 5,7 percentage specimen compared to 2% specimen for the graphite and SiC, TiO2 particle filled composite specimen respectively. The SEM images are also taken to support the results.


2013 ◽  
Vol 712-715 ◽  
pp. 7-11 ◽  
Author(s):  
Mazhyn Skakov ◽  
Bauyrzhan Rakhadilov ◽  
Michael Sсheffler

This paper presents research of influence electrolyte plasma carbonitriding on tribological properties of R6M5 high-speed steel. Shows perspectiveness of carbonitriding high-speed steels in electrolyte plasma. The results of research demonstrated increasing wear-resistance of R6M5 steel after carbonitriding in electrolyte plasma. Under the same test conditions by the method of scratch-test have been determined that the depth of the scar of a modified layer has become less in comparison with the original sample, which indicates a significant increase of wear-resistance and hardness of the surface carbonitriding layer R6М5 steel. It was set that after electrolytic-plasma carbonitriding abrasive wear-resistance of the surface layers of R6M5 steel is increased by 25%. Introduction


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