Tribological Properties of Nano-Al2O3/PEEK Composites

2007 ◽  
Vol 330-332 ◽  
pp. 1239-1242 ◽  
Author(s):  
Dang Sheng Xiong ◽  
Jian Ming Lin ◽  
Ling Ling Liu

Wear is the primary cause of failure of joint replacement prostheses. Poly(ether-ether-ketone)(PEEK) was reinforced with nano-Al2O3 particals of various mass fractions in this study. The effect of nanometer Al2O3 mass fractions on the contacted angle of the reinforced PEEK composites was investigated. Tribological properties of composites under distilled water and physiological saline lubrication condition was measured. And the morphologies of the worn surfaces were observed with optical microscope. The results shows that the wettability and wear resistance were all improved with appropriate nano-Al2O3.The wear resistance of composites filled with 7% nano-Al2O3 was the best under both distilled water and physiological saline lubrication. In addition, it can be found that there is serious plough on the surface of pure PEEK. This indicated that serious fatigue wear occurred on the worn surface of pure PEEK. Moreover, there are only light fatigue wear on the worn surfaces of PEEK composites filled with nano-Al2O3.

2005 ◽  
Vol 288-289 ◽  
pp. 629-632 ◽  
Author(s):  
Dang Sheng Xiong ◽  
Na Wang ◽  
Jian Ming Lin ◽  
He Guo Zhu ◽  
Dong Li Fan

Wear is the primary cause of the failure of joint replacement prostheses. In this paper, the ultra-high molecular weight polyethylene (UHMWPE) as an artificial joint acetabular material was filled with nano-powder of SiO2 of various mass fractions. The effect of SiO2 mass fraction on the tensile strength, tensile modulus, wetting property and tribological properties of the SiO2-UHMWPE composites were investigated when sliding against Ti-6Al-4V under lubrication of physiological saline water. The morphologies of the worn surfaces of composites were observed with optical microscope. As a result, the tensile strength, tensile modulus, wettability and wear resistance of the composites were all improved by filling with SiO2, and the composites had largely decreased friction coefficients under lubrication of physiological saline water compared with the unfilled UHMWPE. This was attributed to the reinforcing function of the nano-powder of SiO2 in the composites and the lubricating action of the water boundary film. The wear of pure UHMWPE was dominated by plowing, plastic deformation, while the SiO2-UHMWPE was characterized the mild fatigue wear.


2012 ◽  
Vol 557-559 ◽  
pp. 534-537 ◽  
Author(s):  
Yong Ping Niu ◽  
Sa Li ◽  
Jun Kai Zhang ◽  
Li Hua Cai ◽  
Yong Zhen Zhang

Polytetrafluoroethylene (PTFE) nanocomposites filled with alumina nanoparticles were prepared by compression molding and follow-up sintering. The tribological behaviors of PTFE nanocomposites sliding against GCr15 steel were evaluated using ball-on-disk tribology test rig. The worn surfaces of the unfilled and filled PTFE nanocomposite were investigated using a scanning electron microscope (SEM). The wear behavior of the PTFE nanocomposites was explained in terms of the topography of worn surfaces. It was found that the addition of alumina nanoparticles was effective in enhancing the wear resistance of the PTFE nanocomposite.


2007 ◽  
Vol 330-332 ◽  
pp. 1215-1218 ◽  
Author(s):  
Jian Kong ◽  
Dang Sheng Xiong ◽  
Jian Liang Li ◽  
Qun Xing Yuan

Metallic biomaterials are used as bone plate, dental implant, wire, electrode, and so on. For the purpose of providing the medical services with higher quality, the frictional and wear behavior of Cu47Ti34Zr11Ni8, (Cu47Ti34Zr11Ni8)99Si, Zr41Ti14Cu12.5Ni10Be22.5 and Zr57Nb5Cu15.4Ni12.6Al10 bulk metallic glasses (BMG) against ceramic ( Si3N4) at room temperature under dry sliding and lubrication of fresh plasma, distilled water, and physiological saline conditions were investigated on a pin-on-disc testing machine. Under identical sliding condition, the steady state friction coefficients of BMGs were observed with values ranging from 0.6 to 0.9 under dry sliding, 0.5 to 0.8 under lubrication with distilled water, 0.5 to 0.7 under lubrication with physiological saline, and 0.3 to 0.7 under lubrication with fresh plasma, respectively. Wear rates of BMGs indicated significant difference that the Cu-based metallic glasses exhibited higher wear resistance than that of Zr-based glasses. The surface tracks indicated the existence of viscous flow and the material transfer occurred from BMG rod to the ceramic disc. Since tribological properties are not intrinsic properties, those results demonstrated the influences of the environment and the characteristics of BMGs on the frictional behaviors, and furthermore indicated that BMGs may be one of the promising biomaterials in the future.


2013 ◽  
Vol 423-426 ◽  
pp. 939-943 ◽  
Author(s):  
Qi Feng Jing ◽  
Ye Fa Tan ◽  
Hui Yong Ji ◽  
Xiao Long Wang ◽  
Li Gao ◽  
...  

Setellite21 cobalt-based alloy coating was deposited on 45 steel by electro-spark deposition. Microstructure and phase composition of the coating were analyzed. Wear resistance and wear mechanism of the coating were researched. The results indicate that the coating with compact structure is mainly composed of Co, Co6W6C, CoCx and CoCr. Average microhardness of the coating is 445.34 HV0.5, which is about 2 times to that of the substrate. The coating presents excellent wear resistance with no obvious peelings and scratches. Wear resistance of the coating is about 2.3~2.7 times to that of the substrate. Wear mechanism of the coating mainly contains abrasive wear and fatigue wear, and along with oxidization wear.


2011 ◽  
Vol 133 (4) ◽  
Author(s):  
Licai Fu ◽  
Jun Yang ◽  
Qinling Bi ◽  
Weimin Liu

The dry-sliding tribological properties of the dendrite composite eutectic Fe-B alloys (Fe94.3B5.7, Fe75B25 Fe67B33) were studied comparatively with various sliding speeds. The friction coefficient of the Fe-B alloy changes slightly with the boron content. The wear rate of the Fe94.3B5.7 alloy with about 30 vol. % dendrite t-Fe2B is only one third of Fe75B25 alloy with 15 vol. % dendrite and Fe67B33 alloy with 90 vol. % dendrite in the high sliding speed. First, a hard t-Fe2B phase reduced the wear of the Fe-B alloy directly. Second, the compactly oxide layers resulting from oxidation of the α-Fe on the worn surfaces also decreases the wear rate of Fe-B alloys. On the whole, the wear rate of the Fe94.3B5.7 is lower than Fe67B33 and Fe75B25.


2021 ◽  
Vol 2130 (1) ◽  
pp. 012023
Author(s):  
A Skic ◽  
K Beer-Lech ◽  
M Szala ◽  
M Kamiński ◽  
Z Krzysiak ◽  
...  

Abstract The crisis related to the COVID 19 pandemic caused an increase in nickel prices on the global markets. From this perspective, it seems promising to search for the possibilities of effective recycling of nickel-based alloys as biomaterials. The topic of the recasting of Ni-Cr dental alloys is currently being broadly described in the literature. Nonetheless, there are still no conclusive results on the impact of recasting on the quality of the cast dentures. Considering the aforementioned, for research, the effect of recasting on the wear resistance and microstructure of NiCrMo dental alloy was investigated. The Heraenium NA alloy was used for testing. Abrasion resistance was tested by the ball on disc method. Microstructure and wear trace were observed using an optical microscope and a scanning electron microscope. The tests showed a higher wear resistance of the re-casted material. The average coefficient of friction for the initially cast alloys was 0.664, while for the remelted samples the mean value was 0.441. The tested samples are characterised by an abrasive-adhesive wear mechanism. Piling up of the wear tracks edges was observed – the highest for H100. For the H100 samples, a slightly lower average hardness value (HV10) was observed – 226 compared to 233 (HV10) for the samples made from the re-casted alloy (H0). The presence of a dendritic structure of alloys was demonstrated. Blocky eutectic precipitations are visible against the matrix. The observed growth of interdendritic precipitations constitute a natural barrier for the counterpart material and increases its tribological properties. Obtained results suggest that alloy recasting does not constitute a limitation to its use.


2020 ◽  
Vol 4 (141) ◽  
pp. 157-163
Author(s):  
IL’YA ROMANOV ◽  
◽  
ROMAN ZADOROZHNIY

When applying coatings using various methods on the surfaces of moving parts that work in joints, it is important to make sure that the coatings are strong and wear-resistant in order to return them to their original resource. All existing hardening technologies and materials used to perform coatings have their own characteristics, therefore, the quality of the resulting coatings can be judged only after specific tests. (Research purpose) The research purpose is in evaluating the properties of the coating obtained by the method of electric spark hardening, and its ability to resist friction and mechanical wear. (Materials and methods) Authors conducted tests on the basis of the "Nano-Center" center for collective use. A coating was applied on the BIG-4M unit with a VK-8 hard alloy electrode, tribological properties were evaluated on a CSM Instruments TRB-S-DE-0000 tribometer, the width of the friction track was measured after the test using an inverted OLYMPUS gx51 optical microscope, and samples were weighed before and after the test on a VLR-200 analytical balance. Conducted research in accordance with GOST 23.224-86 and RD 50-662-88 guidelines. (Results and discussion) The article presents performed tests on the run-in and wear resistance of the coating. The samples were worked on with a step-by-step increase in the load. During the tests, the friction force was drawed on the diagram. Authors compared the results with the reference sample, an uncoated surface. (Conclusions) The resulting coating has better run-in and wear resistance compared to the standard, and the increase in wear resistance in dry friction conditions is very significant.


Coatings ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 670
Author(s):  
Gifty Oppong Boakye ◽  
Arna María Ormsdóttir ◽  
Baldur Geir Gunnarsson ◽  
Sandeep Irukuvarghula ◽  
Raja Khan ◽  
...  

The selection of electroless nickel-phosphorus plating (ENP) has been inclined towards their properties and advantages with complex geometry applications. These properties include coating uniformity, low surface roughness, low wettability, high hardness, lubricity, and corrosion- and wear-resistance. Materials used in geothermal environments are exposed to harsh conditions such as high loads, temperature, and corrosive fluids, causing corrosion, scaling, erosion and wear of components. To improve the corrosion- and wear-resistance and anti-scaling properties of materials for geothermal environment, a ENP duplex coating with PTFE nanoparticles was developed and deposited on mild steel within the H2020 EU Geo-Coat project. ENP thin adhesive layer and ENP+PTFE top functional layer form the duplex structure of the coating. The objective of this study was to test the mechanical and tribological properties of the developed ENP-PTFE coatings with varying PTFE content. The microstructural, mechanical and tribological properties of the as-deposited coating with increasing PTFE content in the top functional layer in the order: ENP1, ENP2 and ENP3 were evaluated. The results showed maximum wear protection of the substrates at the lowest load; however, increasing load and sliding cycles increased the wear rates, and 79% increased lubrication was recorded for the ENP2 duplex coating. The wear performance of ENP3 greatly improved with a wear resistance of 8.3 × 104 m/mm3 compared to 6.9 × 104 m/mm3 for ENP2 and 2.1 × 104 m/mm3 for ENP1. The results are applicable in developing low friction, hydrophobic or wear-resistive surfaces for geothermal application.


2013 ◽  
Vol 372 ◽  
pp. 507-511
Author(s):  
Hitonobu Koike ◽  
Kenji Kanemasu ◽  
Kiyoto Itakura ◽  
Shota Okazaki ◽  
Masahiro Takamiya ◽  
...  

In this work, wear of reinforced poly-ether-ether-ketone (PEEK) polymer bushes in friction against 7075 aluminium alloy cam plates or titanium crankshafts is investigated in order to establish the application possibilities in transmission parts in humanoid robot joints under high load torque. The PEEK bush wear requires close examination as well as the input axis-output axis transmission error (backlash). Sliding wear tests were performed on bushes under 4000 kgfcm (392 Nm) load torque, while the cam plate oscillated in the humanoid robot leg joint evaluation system. The robot joint using PEEK bush achieved quite small backlash after the fatigue wear test.


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