The Effect of Semi-Solid Parameters on the Microstructure and Hardness of High Chromium Cast Irons

2010 ◽  
Vol 457 ◽  
pp. 84-89 ◽  
Author(s):  
Arash Inanlou ◽  
S. Hossein Seyedein ◽  
M. Reza Aboutalebi
Keyword(s):  
Heat Treatment ◽  
Casting Process ◽  
Cast Irons ◽  
Inclined Plate ◽  
Cooling Plate ◽  
High Chromium ◽  
Primary Austenite ◽  
Heat Treated ◽  
Before And After ◽  
Semi Solid

High chromium cast iron samples of 14% Cr and 24% Cr were produced in sand and permanent mold using semi-solid casting process. A series of experiments were carried out to clarify the effect of copper cooling plate and mold cooling rate on microstructure, particularly morphology and sphericity of primary austenite, hardness and heat treatment cycles. Results show that for 14% Cr and 24% cast irons casting at 10 and 15 degrees of inclined plate result in better sphericity and distribution of primary austenite and carbides. Moreover hardness comparison of both semi-solid iron alloys using copper cooling plate at of this special morphologies resulted from cooling plate investigated by making them heat treat at 1050 centigrade °C for 1 and 2 hours. Hardness results show both heat treated 14 and 24% Cr alloy in 1 hours have hardness comparable with those alloys traditionally cast optimum angles with respect to conventional casting show higher hardness in every condition. Effect but heat treated in 2 hours. Finally X-Ray diffraction pattern taken from specimens before and after heat treatment confirmed with observed phases in optical microscopy before and after heat treatment.

Casting and Heat Treatment of Turbocharger Impellers Thixocast from Alloy 201

2012 ◽  
Vol 192-193 ◽  
pp. 556-561 ◽  
Author(s):  
Qiang Zhu ◽  
Stephen Midson ◽  
Chang Wei Ming ◽  
Helen V. Atkinson
Keyword(s):  
Heat Treatment ◽  
High Strength ◽  
Heat Treatment Condition ◽  
Hot Tearing ◽  
Alloy Casting ◽  
Heat Treated ◽  
Before And After ◽  
Optimum Heat ◽  
Semi Solid ◽  
Optimum Heat Treatment

Commercial semi-solid cast impellers are produced from Al-Si-Cu alloys heat treated to the T6 temper. The study described in this paper involved the identification of casting and heat treatment parameters to produce semi-solid processed turbocharger impellers from a silicon-free, higher strength 201 alloy. Casting parameters were identified which minimized hot tearing in the alloy 201 impellers. A series of heat treatment studies were performed to determine optimum heat treatment parameters. The T71 temper was identified as the preferred heat treatment condition to produce high strength as well as superior elongation. The results from mechanical property measurements conducted on the T71 heat treated impellers are reported. Optical and scanning electron microscopy (SEM) were also used to characterize the microstructure of alloy 201 impellers before and after heat treatment, and representative microstructures are presented.

scholarly journals Effect of Heat Treatment on the As-Cast Microstructure and Hardness of NiSi3B2 Alloy

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 539
Author(s):  
Gonçalo M. Gorito ◽  
Aida B. Moreira ◽  
Pedro Lacerda ◽  
Manuel F. Vieira ◽  
Laura M. M. Ribeiro
Keyword(s):  
Heat Treatment ◽  
Elevated Temperatures ◽  
Casting Process ◽  
X Ray Diffraction ◽  
Heat Treated ◽  
Energy Dispersive Microanalysis ◽  
Eutectic Constituent ◽  
Backscattered Electron ◽  
Corrosion And Oxidation ◽  
Cast Microstructure

Cast Ni-Si-B alloys have the potential for high-temperature applications because of their high resistance to wear, impact, corrosion, and oxidation at elevated temperatures due to an appropriate balance of hard phases and austenite that ensures a good compromise between toughness and hardness. In this work, NiSi3B2 specimens, fabricated by the lost-wax casting process, were investigated. Given the complex multiphase cast microstructure, a differential scanning calorimeter (DSC-TGA) analysis was employed to characterize the reactions that occur during solidification and the resulting phases were characterized using scanning electron microscopy (SEM), with energy-dispersive microanalysis (EDS) and backscattered electron (BSE) image and X-ray diffraction (XRD). Due to the presence of hard phases, machining of the Ni-Si-B components can pose additional difficulties. Therefore, the conditions of the solution heat treatment, which might lead to the homogenization of the microstructure, consequently improving its machinability, were also investigated. The results of the heat-treated samples indicated that the dissolution of the eutectic constituent is accompanied by a significant decrease in the hardness (approximately 17%). It is important to emphasize that the solution heat treatments carried out reduced the hardness without affecting the percentage of borides, which will allow improving the machinability without adversely affecting the alloy performance in service.

Comparison of Microstructure and Mechanical Properties of Semi-Solid Castings Produced Using Billets Made by EMS and SEED

2014 ◽  
Vol 217-218 ◽  
pp. 332-339 ◽  
Author(s):  
Xiao Kang Liang ◽  
Da Quan Li ◽  
Pascal Côté ◽  
Stephen P. Midson ◽  
Qiang Zhu
Keyword(s):  
Mechanical Properties ◽  
Cross Section ◽  
Dendritic Structure ◽  
Casting Process ◽  
Grain Structure ◽  
High Quality ◽  
Microstructure And Mechanical Properties ◽  
Grain Structures ◽  
Heat Treated ◽  
Semi Solid

The spheroidal grains in billets used for semi-solid casting are generally manufactured by electromagnetic stirring (EMS) during the casting process. This method however, is not economically applicable for small quantities of the thixo billets. Swirled Enthalpy Equilibration Device (SEED) has been developed as a rheocasting process, and the SEED process is of interest for developing new thixo alloys, as well as for optimizing the thixocasting processes for high quality components. The objective of this paper is to compare the microstructure and mechanical properties of aluminum alloy 319s billets and castings produced using EMS and SEED feed materials. The experimental results show that for as-cast billets made from SEED process, a well-developed spheroidal grain structure is distributed throughout the cross-section of the billet, while for as-cast EMS billets, the grain structure is inhomogeneous, i.e., a dendritic structure was present adjacent to the surface of the billet, while a uniform, spheroidal structure was present at the centre. After the thixocasting process, however, the both SEED and EMS billets have well-developed, spheroidal grain structures. Mechanical properties of thixocast and T61 heat treated components are comparable for the both SEED and EMS billets.

Failure analysis of heat treated HSLA wheel bolt steels

2010 ◽  
Vol 6 (3) ◽  
pp. 373-382
Author(s):  
Ali Nazari ◽  
Shadi Riahi
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Failure Analysis ◽  
Heat Treating ◽  
Boron Steel ◽  
Content Type ◽  
Heat Treated ◽  
Before And After ◽  
Molybdenum Steel ◽  
Optimum Heat

PurposeThe aims of this study is to analyze failure of two types of high‐strength low‐alloy (HSLA) steels which are used in wheel bolts 10.9 grade, boron steel and chromium‐molybdenum steel, before and after heat treatment.Design/methodology/approachThe optimum heat treatment to obtain the best tensile behavior was determined and Charpy impact and Rockwell hardness tests were performed on the two steel types before and after the optimum heat treating.FindingsFractographic studies show a ductile fracture for heat‐treated boron steel while indicate a semi‐brittle fracture for heat‐treated chromium‐molybdenum steel. Formation of a small boron carbide amount during heat treating of boron steel results in increment the bolt's tensile strength while the ductility did not changed significantly. In the other hand, formation of chromium and molybdenum carbides during heat treating of chromium‐molybdenum steel increased the bolt's tensile strength with a considerable reduction in the final ductility.Originality/valueThis paper evaluates failure analysis of HSLA wheel bolt steels and compares their microstructure before and after the loading regime.

scholarly journals Study on the Properties of Transparent Bamboo Prepared by Epoxy Resin Impregnation

Polymers ◽  
2020 ◽  
Vol 12 (4) ◽  
pp. 863 ◽  
Author(s):  
Yan Wu ◽  
Yajing Wang ◽  
Feng Yang ◽  
Jing Wang ◽  
Xuehua Wang
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Visible Light ◽  
Epoxy Resin ◽  
Raw Materials ◽  
Light Transmittance ◽  
Advantages And Disadvantages ◽  
Heat Treated ◽  
Before And After ◽  
Different Parts

In this paper, Moso bamboo (Phyllostachys heterocycle) before and after heat treatment were used as raw materials to prepare transparent bamboo (TB). In an acidic environment, the lignin contained in the bamboo material was removed to obtain a bamboo template, and an epoxy resin similar to the cellulose refractive index was used for vacuum impregnation into the bamboo template to obtain a transparent bamboo material. The purpose of this study was to compare the physical and chemical properties of TB and original bamboo and the differences between TBs before and after heat treatment, taken from different parts of bamboo, in order to explore the performance advantages and disadvantages of TB as a new material. The Fourier transform infrared spectroscopy analysis (FTIR), scanning electron microscope testing (SEM), three elements analysis, light transmittance testing, and mechanical strength testing were used to study the molecular composition, microstructure, chemical composition, light transmittance, and tensile strength of the TB samples. The results showed that the lignin content of the delignified bamboo templates was greatly reduced. In addition, the SEM images showed that a large amount of epoxy resin (type E51 and type B210 curing agent) was covered on the cross-section surface and pores of the TB samples. The FTIR showed that the epoxy molecular groups appeared on the TB, and the delignified bamboo template and the resin had a good synergy effect. According to the light transmittance testing, the original bamboo samples hardly contained light transmittance under visible light. The transmittance of transparent inner bamboo (TIB) and transparent heat-treated inner bamboo (THIB) could reach about 11%, and the transmittance of transparent outer bamboo (TOB) and transparent heat-treated outer bamboo (THOB) was about 2%. The light transmittance had been significantly improved when compared with the original bamboo samples. The transmittances of the TB samples before and after heat treatment in different parts of bamboo were different. In the visible light irradiation range, the light transmittances of TB samples were as follows: TIB > THIB and THOB > TOB. Meanwhile, the tensile strength of TB was reduced, especially for TOB and THOB. In addition, TB has a wide range of raw materials, and the preparation process is environmentally friendly. It can be used for decorative materials in homes, buildings, etc., and has a great application potential.

The Microstructure and Compression Behavior of Multi-Step Forging Ti-45Al-8Nb Alloy after Annealing at 1100 °C

2013 ◽  
Vol 747-748 ◽  
pp. 111-114
Author(s):  
Lin Song ◽  
Xiang Jun Xu ◽  
Jun Pin Lin ◽  
Lai Qi Zhang
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Annealing Treatment ◽  
Air Cooling ◽  
Test Machine ◽  
Compressive Properties ◽  
Compression Behavior ◽  
Microstructure Change ◽  
Heat Treated ◽  
Before And After

Effects of annealing treatment on microstructure and the compressive properties of hot-worked Ti-45Al-8Nb-(W, B, Y) alloy were investigated. Microstructure of the extrusion plus multi-step forging pancake before and after heat treatment was analyzed by SEM and TEM, respectively. The annealing was conducted by holding samples at 1100°C for 2hrs, and followed by air cooling and furnace cooling. The mechanical properties were measured by Instron test machine. The microstructure evolution during compressive deformation was analyzed by TEM. The results showed that after the annealing the microstructure change could not be observed under SEM but can be observed under TEM. Many dislocation clusters were removed by heat treatment. The heat treated samples had similar compression behaviors with the pancake. TEM investigation showed that the numerous twin intersections occured in γ matrix during compression. The twin spaces tended to decrease as the deformation and the intersection increasing.

Tensile Properties of Semi-Solid Die Cast AC4C Aluminum Alloy

2014 ◽  
Vol 680 ◽  
pp. 11-14
Author(s):  
Ke Ren Shi ◽  
Sirikul Wisutmethangoon ◽  
Jessada Wannasin ◽  
Thawatchai Plookphol
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Aluminum Alloy ◽  
Die Casting ◽  
Casting Process ◽  
Al Alloy ◽  
Die Cast ◽  
Die Casting Process ◽  
Semi Solid ◽  
Strength And Ductility

In this study, semi-solid Al-Mg-Si alloy (AC4C) was produced by using the Gas Induced Semi-Solid (GISS) die casting process. The tensile strength and ductility of the semi-solid die cast Al alloy (GISS-DC) after T6 heat treatment were investigated and compared with those of the conventional liquid die casting (CLDC). The microstructures of GISS-DC and CLDC observed by an optical microscopy were presented. The ultimate tensile strength (UTS) and yield strength (0.2% YS) of GISS-DC are compatible with those of the CLDC. However, the GISS-DC has better ductility than the CLDC, this may be due to the smaller and more globular primary α-Al phase and rounder shaped-Si particle microstructures presented in the GISS-DC. Common shrinkage pores and defects were also observed by SEM from the fracture surfaces of both alloys.

Formation of Globular Microstructure in A380 Aluminum Alloy by Cooling Slope Casting

2011 ◽  
Vol 264-265 ◽  
pp. 272-277 ◽  
Author(s):  
Nurşen Saklakoğlu ◽  
S. Gencalp ◽  
Şefika Kasman ◽  
İ.E. Saklakoğlu
Keyword(s):  
Aluminum Alloy ◽  
Slope Angle ◽  
Casting Process ◽  
Solid Particles ◽  
Inclined Plate ◽  
Pouring Temperature ◽  
Cooling Slope ◽  
Semi Solid ◽  
Cooling Slope Casting ◽  
The Many

Thixoforming and related semi-solid processing (SSP) methods require thixotropic materials. One of the many SSP techniques is the cooling slope (CS) casting process, which is simple and has minimal equipment requirements, and which is able to produce feedstock materials for semisolid processing. When the feedstock is reheated to the semisolid temperature range, non-dendritic, spheroidal solid particles in a liquid matrix suitable for thixoforming are obtained. In this study, equipment for the CS technique was first established, and then the effects of the pouring temperature and inclined slope angle on the microstructures of A380 aluminum alloy (ISOAlSi8Cu3Fe) were studied. Optimum parameters for thixoforming experiments were selected, and it was found that the microstructure produced by the inclined plate depended on its angle and the pouring temperature.

Wettability of Heat-Treated Wood

Holzforschung ◽  
2003 ◽  
Vol 57 (3) ◽  
pp. 301-307 ◽  
Author(s):  
M. Pétrissans ◽  
P. Gérardin ◽  
I. El bakali ◽  
M. Serraj
Keyword(s):  
Heat Treatment ◽  
Water Drop ◽  
Chemical Change ◽  
Treated Wood ◽  
Untreated Wood ◽  
Adsorbed Water ◽  
Inert Atmosphere ◽  
Contact Angles ◽  
Heat Treated ◽  
Before And After

Summary The aim of this work was to study the wettability and chemical composition of heat-treated wood. Heat treatment was performed at 240°C under inert atmosphere on four European wood species (pine, spruce, beech and poplar). Contact angle measurements before and after treatment indicated a significant increase in wood hydrophobicity. Advancing contact angles of a water drop were in all cases systematically higher for heat-treated than for untreated wood. Chemical modifications of wood after heat treatment were investigated using FTIR and 13C NMR analysis. FTIR spectra indicated little structural change which could be attributed either to carbon-carbon double bond formation or to adsorbed water. NMR spectra also revealed little chemical change except for the degree of cellulose crystallinity which was considerably higher in heat-treated wood and could explain the higher contact angles.

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