Effects of Two-Step Tempering Treatment on the Microstructural Formation of T91 Ferritic Steels

2011 ◽  
Vol 172-174 ◽  
pp. 875-880 ◽  
Author(s):  
Chen Xi Liu ◽  
Ze Sheng Yan ◽  
Zhi Zhong Dong ◽  
Yong Chang Liu ◽  
Bao Qun Ning

As a representative type of high Cr ferritic heat-resistant steels, T91 steels (ASME SA-213 T91/P91) has been recognized as the preferable materials and widely used in high-temperature structural components such as header and main steam pipe in advanced power plants. For the service condition is tempered martensites, its corresponding microstructure and mechanical performance are mainly adjusted by the tempering treatment. After exploring the size and number of MX and M23C6precipitating particles and the width of martensitic lath as a function of tempering temperature, it is recognized that the high tempering temperature leads to an increase of secondary hardening effect, while the low tempering temperature brings a high dislocation density and a small martensitic lath. Hence, a two-step tempering treatment was developed after the traditional normalizing process, in which the T91 steels sample was firstly tempered at a low temperature in order to form some precipitates and then tempered at a high temperature. Those firstly-formed precipitates would pin the dislocations and martensitic laths on the subsequent tempering process, which finally leads to more precipitates, higher dislocation density and smaller martensitic lath width than that obtained from the traditional tempering process.

2016 ◽  
Vol 880 ◽  
pp. 29-32
Author(s):  
T.C. Chen ◽  
Wen Hao Chien ◽  
Yuan Tsung Wang ◽  
Ching Yuan Huang ◽  
Hung Wei Yen ◽  
...  

The demand for new materials that provide excellent structural performance while reducing weight and being cost-effectively manufactured is increasing. For applications with high strength requirements, ultra-high strength steels (UHSS) have been widely used. However, with such a high strength level, UHSS are very sensitive to the hydrogen that could be ease by the tempering process. In this research, the correlation of hydrogen and tempering process on commercial UHSS 15B30 has been studied. Results show that the tensile strength (TS) of as-quenched 15B30 is about 1900MPa. After tempering treatment of the quenched 15B30, the TS decreases from 1600MPa to 1200MPa with tempering temperature increased from 200°C to 400°C. The 15B30 specimens, being subjected to hydrogen charge, exhibit the dramatic reduction of mechanical strengths.


Materials ◽  
2021 ◽  
Vol 15 (1) ◽  
pp. 259
Author(s):  
Juntai Hu ◽  
Yu Liu ◽  
Ge Wang ◽  
Qiang Li ◽  
Jianyang Wen ◽  
...  

In this paper, the microstructure and mechanical properties of heavy-wall seamless bend pipe after quenching at different tempering temperatures, including 550 °C, 600 °C, 650 °C, and 700 °C, were studied. Microstructure and dislocations observations were characterized by means of an optical microscope, a scanning electron microscope, a transmission electron microscope, and X-ray diffraction. As the tempering temperature increases, the dislocation density in the test steel gradually decreases, and the precipitation behavior of (Nb, V)(C, N) increases. The sample tempered at 650 °C exhibits a granular bainite structure with a dislocation cell structure and a large number of smaller precipitates. The yield platforms of tempered samples at 650 °C and 700 °C are attributed to the pinning effect of the Cottrell atmosphere on dislocations. The sample tempered at 650 °C not only presents the highest strength, but also the highest uniform elongation, which is attributed to the higher strain-hardening rate and instantaneous work-hardening index. This is closely related to the multiplication of dislocations, the interaction between dislocations and dislocations, and the interaction between dislocations and precipitates during plastic deformation of the 650 °C-tempered samples with low dislocation density, which delays the occurrence of necking.


Author(s):  
Jilin Xue ◽  
Changyu Zhou ◽  
Jian Peng

P91 heat-resistant steel pipes are widely used at high temperature in power plants and nuclear power plants. The service condition and manufacturing process may produce defects of local wall thinning, which may result in stress redistribution of the pipes during the service process at elevated temperature. For the purpose of understanding the creep stress and strain accumulation affected by local wall thinning geometries under creep condition, three groups of models were calculated, using three-dimensional models based on finite element analyses (FEA) codes ABAQUS. In this study, monotonic internal pressure was conducted on P91 full-scale steel pipes at 625°C, with local wall thinning located at the inner surface. Then, the creep strain and stress of pipes after 100,000h could be obtained corresponding to different models. Based on the analysis, the figures of creep stress and strain varying with defect geometries were plotted. Then, the stress and strain of pipes with local wall thinning affected by defect geometries, including different defect depths, different defect axial lengths and different defect hoop angles, were discussed. The results indicate that creep stress and creep strain increase with defect geometries. The variation laws have been summarized. The research results can provide the possibility on safety assessment and structure integrity analysis of the pipe with local wall thinning at high temperature effectively.


2008 ◽  
Vol 2008 ◽  
pp. 1-9
Author(s):  
Shutang Zhu ◽  
Ying Tang ◽  
Kun Xiao ◽  
Zuoyi Zhang

This paper presents investigations on the possible combination of modular high-temperature gas-cooled reactor (MHTGR) technology with the supercritical (SC) steam turbine technology and the prospective deployments of the MHTGR SC power plant. Energy conversion efficiency of steam turbine cycle can be improved by increasing the main steam pressure and temperature. Investigations on SC water reactor (SCWR) reveal that the development of SCWR power plants still needs further research and development. The MHTGR SC plant coupling the existing technologies of current MHTGR module design with operation experiences of SC FPP will achieve high cycle efficiency in addition to its inherent safety. The standard once-reheat SC steam turbine cycle and the once-reheat steam cycle with life-steam have been studied and corresponding parameters were computed. Efficiencies of thermodynamic processes of MHTGR SC plants were analyzed, while comparisons were made between an MHTGR SC plant and a designed advanced passive PWR - AP1000. It was shown that the net plant efficiency of an MHTGR SC plant can reach 45% or above, 30% higher than that of AP1000 (35% net efficiency). Furthermore, an MHTGR SC plant has higher environmental competitiveness without emission of greenhouse gases and other pollutants.


2019 ◽  
Vol 4 (1) ◽  
pp. 286-294
Author(s):  
László Tóth ◽  
Réka Fábián

The X153CrMoV12 ledeburitic chromium steel characteristically has high abrasive wear resistance, due to their high carbon and high chromium contents with a large volume of carbides in the microstructure. This steel quality has high compression strength, excellent deep hardenability and toughness properties, dimensional stability during heat treatment, high resistance to softening at elevated temperatures. The higher hardness of cryogenic treated samples in comparison with conventional quenched samples mean lower quantity of retained austenite as at samples quenched to room temperature and tempered in similar condition. In the microstructure of samples were observed that the primary carbide did not dissolve at 1070°C and their net structure have not been changed during to heat treatment. During to tempering at high temperature the primary carbides have become more and more rounded. After low tempering temperature in martensite were observed some small rounded carbides also, increasing the tempering temperature the quantity of finely dispersed carbides increased, which result higher hardness. The important issues in heat treatment of this steels are the reduction or elimination of retained austenite due to cryogenic treatment.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4095
Author(s):  
Qing Chen ◽  
Zhiyuan Zhu ◽  
Rui Ma ◽  
Zhengwu Jiang ◽  
Yao Zhang ◽  
...  

In this paper, the mechanical performance of an ultra-high-performance concrete (UHPC) repaired cementitious composite system, including the old matrix and the new reinforcement (UHPC), under various high temperature levels (20 °C, 100 °C, 300 °C, and 500 °C) was studied. In this system, UHPC reinforced with different contents of steel fibers and polypropylene (PP) fibers was utilized. Moreover, the physical, compressive, bonding, and flexural behaviors of the UHPC repaired system after being exposed to different high temperatures were investigated. Meanwhile, X-ray diffraction (XRD), baseline evaluation test (BET), and scanning electron microscope (SEM) tests were conducted to analyze the effect of high temperature on the microstructural changes in a UHPC repaired cementitious composite system. Results indicate that the appearance of the bonded system changed, and its mass decreased slightly. The average percentage of residual mass of the system was 99.5%, 96%, and 94–95% at 100 °C, 300 °C, and 500 °C, respectively. The residual compressive strength, bonding strength, and flexural performance improved first and then deteriorated with the increase of temperature. When the temperature reached 500 °C, the compressive strength, bonding strength, and flexural strength decreased by about 20%, 30%, and 15% for the UHPC bonded system, respectively. Under high temperature, the original components of UHPC decreased and the pore structure deteriorated. The cumulative pore volume at 500 °C could reach more than three times that at room temperature (about 20 °C). The bonding showed obvious deterioration, and the interfacial structure became looser after exposure to high temperature.


Author(s):  
Changyu Zhou ◽  
Bo Wang ◽  
Zhigang Sun ◽  
Jilin Xue ◽  
Xiaohua He

High temperature pressure pipes are widely used in power stations, nuclear power plants, and petroleum refinery, which always bear combined effects of high temperature, high pressure, and corrosive media, so the local pits are the most common volume defects in pressure pipe. Due to various reasons, the defects usually appear on the internal or external wall of pipe. In this paper, the dimensions of a defect were characterized as three dimensionless factors: relative depth, relative gradient and relative length. The main objects of study were the pipe with an internal pit and pipe with an external pit. Orthogonal array testing of three factors at four different levels was applied to analyze the sequence of the influence of three parameters. In present study, when the maximum principal strain nearby the location of the defects reaches 2%, the corresponding load is defined as the limit load, which is classified as two kinds of load type: limit pressure and limit bending moment. According to this strain criterion and isochronous stress strain data of P91 steel, the limit load of high temperature pipe with a local pit was determined by using ABAQUS. And in the same load condition of the pipe with the same dimensionless factors, the limit load of the internal defected pipe was compared with that of the external defected pipe. The results of this study can provide a reference for safety assessment and structural integrity analysis of high temperature creep pressure pipe with pit defects.


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