Bulk and In-Circuit Dielectric Characterization of LTCC Tape Systems Through Millimeter Wave Frequency Range

2011 ◽  
Vol 2011 (1) ◽  
pp. 000740-000746 ◽  
Author(s):  
Bradley Thrasher ◽  
Deepukumar Nair ◽  
James Parisi ◽  
Glenn Oliver ◽  
Michael A. Smith

Low Temperature Co-fired Ceramic (LTCC) material systems offer a highly versatile microwave and millimeter wave packaging platform. Extremely low microwave loss, excellent control of dielectric constant, uniform dielectric thickness, non-existent water absorption leading to very high hermeticity, ability to support multilayer structure leading to 3-dimensional packaging, ability to embed passive functions within the tape layers, availability of a wide range of metallizations, etc. are some of the key advantages of LTCC for microwave packaging. One of the important parameters which needs to be determined at the very early stages of circuit designs are the dielectric properties - dielectric constant and loss tangent, both of which are functions of frequency. These properties need to be known accurately over the entire frequency range of operation for the circuit. For LTCC based designs, the use of dielectric constant of bulk material can lead to deviations between the performance expected at the design stage and for the fabricated circuit. Such deviations are a significant concern for broadband circuits as well as for circuits with sharp resonant behavior such as filters. One of the significant sources of deviation between bulk LTCC and “in-circuit” dielectric constant is the nature of the thick film metallizations used in LTCC technology. Work described here is a comprehensive characterization of three DuPont™ GreenTape™ LTCC systems 951, 943, and 9K7 - in the frequency range 10 to 70 GHz. Both bulk and “in-circuit” dielectric properties with silver and gold metallizations are studied to quantify the deviations in dielectric properties. A Fabry-Perot open resonator technique is used for the bulk characterization while printed ring resonators are used for the in-circuit characterization. This comprehensive characterization will provide key design data for LTCC designers in the 10 – 70 GHz frequency range.

2013 ◽  
Vol 80 (12) ◽  
Author(s):  
Niels Haandbæk ◽  
Sebastian C. Bürgel ◽  
Flavio Heer ◽  
Andreas Hierlemann

AbstractThis article presents a novel microfluidic impedance cytometer enabling dielectric characterization of single cells at frequencies up to 500 MHz. The dielectric properties of cells at lower frequencies contain information about their size and membrane capacitance. The increased frequency range of the presented cytometer potentially allows for characterization of intracellular components, such as vacuoles or the cell nuclei. We demonstrate the overall capabilities of the cytometer through discrimination of polystyrene beads from Chinese hamster ovary (CHO) cells. The discrimination is based on the difference in dielectric properties at frequencies up to 500 MHz.


2013 ◽  
Vol 395-396 ◽  
pp. 29-32
Author(s):  
Jia Qi Lin ◽  
Pan Pan Zhang ◽  
Wen Long Yang

A novel polyimide (PI) films with three kinds of monomers was synthesized in this paper. The polyimide unit is derived from Pyromellitic dianhydride (PMDA), 3,3',4,4'-benzophenonetetracarboxylic dianhydride, (BTDA), and 4,4, -diaminodiphenyl ether (ODA). The dielectric properties of the films were measured. The dielectric spectra show that dielectric constant is about 3.7, which is larger than the PI with two kinds of monomers. In addition, the loss tangent and conductivity of the films is quite small, which is important for the practical use of them.


2015 ◽  
Vol 1107 ◽  
pp. 38-44
Author(s):  
Wong Yick Jeng ◽  
Hassan Jumiah ◽  
Mansor Hashim

The CaTiO3samples were prepared by high-energy ball milling process followed by sintering process from 1040 to 1200°C. X-ray diffraction (XRD), microstructural analysis, and dielectric properties over a wide range of frequency varying from 0.01 Hz to 1 GHz at room temperature were investigated. The formation of a single phase CaTiO3with orthorhombic structure was achieved at 1120°C and above. From a morphological point of view, sintering temperature promoted grain growth. Dielectric properties in the frequency range 0.01 Hz - 1 MHz revealed a relaxation-type process. Interfacial phenomena were the possible physical mechanisms that gave rise to these relaxation-type plots. Extending the frequencies above ~1 MHz yielded a frequency-independent characteristic of dielectric constant (ε'). These turned out to the relatively small dielectric loss (tan δ) values. The origin of the dielectric responses in the frequency range 1 MHz - 1 GHz was attributed to the domination of dipolar polarization. The grain size effect in sintered CaTiO3samples was prominent, notably in dielectric responses above ~1 MHz. Increase in sintering temperature remarkably led to an enhancement in dielectric constant values and reduction in dielectric loss values. Therefore, a significant correlation existed between microstructural features and dielectric properties.


Clay Minerals ◽  
2014 ◽  
Vol 49 (4) ◽  
pp. 551-558
Author(s):  
S. Gümüştas ◽  
K. Köseoğlu ◽  
E. E. Yalçinkaya ◽  
M. Balcan

AbstractThe purpose of this paper is to determine the effect of NaF and firing temperature on the dielectric properties (dielectric constant and dielectric loss) of talc, which is used in the electrical and electronic industries as a circuit element. A detailed characterization of the samples was made by XRD, FTIR, SEM and TG-DTG methods. Dielectric measurements were performed in the frequency range from 1 MHz to 80 MHz at room temperature. The dielectric constant value increased with an increase in firing temperature due to the removal of polarizable compounds from the talc structure. The higher dielectric constant values were obtained by addition of NaF. The dielectric loss of NaF doped talc decreased with the increase of firing temperature and increased with the increase of the amount of NaF.


2008 ◽  
Vol 368-372 ◽  
pp. 123-125
Author(s):  
Jie Li ◽  
Hao Xue ◽  
Zhao Xian Xiong

CaCu3Ti4O12 (CCTO) ceramics were prepared by cold isostatic press (CIP) forming combined with the conventional sintering method. The effects of calcining temperature on properties of CCTO ceramics were investigated. The dielectric properties as the function of temperature at typical frequencies were measured in the temperature range from 243 to 363 K. In addition, the dielectric properties and complex impedances at room temperature were analyzed in a frequency range from 20 Hz to 106 Hz. The results showed that CCTO ceramics with dielectric constant higher than 104 were obtained. Compared with the dry press forming, CCTO ceramics prepared by CIP had more homogeneous grains, less porosity and better dielectric properties.


2017 ◽  
Vol 07 (01) ◽  
pp. 1720001 ◽  
Author(s):  
Jinwu Chen ◽  
Chunchun Li ◽  
Dan Wang ◽  
Huaicheng Xiang ◽  
Liang Fang

Single phase Li2W2O7 with anorthic structure was prepared by the conventional solid-state reaction method at 550[Formula: see text]C and the anorthic structure was stable up to 660[Formula: see text]C. The dielectric properties at radio frequency (RF) and microwave frequency range were characterized. The sample sintered at 640[Formula: see text]C exhibited the optimum microwave dielectric properties with a relative permittivity of 12.2, a quality factor value of 17,700[Formula: see text]GHz (at 9.8[Formula: see text]GHz), and a temperature coefficient of the resonant frequency of [Formula: see text]232[Formula: see text]ppm/[Formula: see text]C as well as a high relative density [Formula: see text]94.1%. Chemical compatibility measurement indicated Li2W2O7 did not react with aluminum electrodes when sintered at 640[Formula: see text]C for 4[Formula: see text]h.


Energies ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 4861
Author(s):  
Fabio Fanari ◽  
Giacomo Muntoni ◽  
Chiara Dachena ◽  
Renzo Carta ◽  
Francesco Desogus

Microwave heating offers a lot of advantages compared to conventional heating methods in the chemical reactions field due to its positive effects on reaction time and selectivity. Dielectric properties, and in particular permittivity, of substances and mixtures, are important for the optimization of microwave heating processes; notwithstanding this, specific databases are poor and far from being complete, and in the scientific literature very little data regarding these properties can be found. In this work, impedance measurements were carried out using a specially designed system to get the real and imaginary parts of the dielectric constant. The apparatus was tested in the estimation of permittivity of water–ethanol and water–NaCl mixtures, varying their composition to obtain a wide range of permittivity values. The results were compared to literature data and fitted with available literature models to verify the correspondence between them, finding that permittivity dependence on mixture composition can be effectively described by the models.


1990 ◽  
Vol 180 ◽  
Author(s):  
G. Teowee ◽  
J.M. Boulton ◽  
H.H. Fox ◽  
A. Koussa ◽  
T. Gudgel ◽  
...  

ABSTRACTPolycerams are an emergent class of hybrid, multifunctional materials which combine the properties of organic and inorganic materials. Films have been prepared from silicon alkoxides and reactive, functionalized polymers such as triethoxysilyl modified polybutadiene (MPBD), (N-triethoxysilylpropyl)O polyethylene oxide urethane (MPEOU) and trimethoxysilylpropyl substituted polyethyleneimine (MPEI). Characterization of dielectric constant and tan δ of the films has been carried out over a range of frequency from 500 Hz to 100 kHz; and the results are used to consider the potential of Polycerams as dielectric materials.


Frequenz ◽  
2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Soumya Sundar Pattanayak ◽  
Soumen Biswas

Abstract The quality of agricultural products can be remotely sensed and enhanced by determining the dielectric properties. This paper studies the dielectric properties of banana leaf and banana peel over the frequency range 1–20 GHz using the open-ended coaxial probe (OCP) method. A new curve fitting model is proposed to characterize the dielectric properties of banana leaf and banana peel. The different moisture content (MC) levels are considered for both banana leaf and banana peel samples and, their dielectric properties are characterized. Further, the banana leaf and banana peel’s measurement data are compared with the data obtained using the proposed model. In addition, Root Mean Square Error (RMSE) and R-squared (R 2) are calculated to validate the performance of the proposed model. In case of banana leaf at 68.26% MC, the dielectric constant achieves the value of R 2 and RMSE of 0.98 and 0.0648, respectively. Similarly, dielectric loss achieves the value of R 2 and RMSE of 0.88 and 0.0795, respectively. Further, for banana peel at 80.89% MC, the dielectric constant achieves the value of R 2 and RMSE of 0.99 and 0.2989, respectively. Similarly, dielectric loss achieves the value of R 2 and RMSE of 0.96 and 0.6132, respectively.


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