scholarly journals Characterization of Magnetic Minerals within Alkali and Tholeiitic Basalts in Penghu Islands of Taiwan

2020 ◽  
Author(s):  
Hun-Hao Lo ◽  
Yen-Hua Chen ◽  
Chorng-Shern Horng
2021 ◽  
Author(s):  
Francho Gracia Puzo ◽  
Charles Aubourg ◽  
Antonio Casas Sainz

<p>With the objective of mapping strain on the footwall of a thrust in an orogenic context (Leyre thrust, South Pyrenean Range), more than 1500 unoriented shale fragments (0.7-6.2 g) have been collected. Scalar data (degree of anisotropy P and shape parameter T), together with ellipse of confidence of individual axes provide a proxy of strain acquired by shales in the footwall of the main thrust (Saur et al. 2020).</p><p>Normally, sampling is done by two methods: collecting oriented decimetric hand specimens; or drilling 2.5 cm diameter cylinders. This presents the advantage to deal with oriented samples. However, those techniques are time consuming and it is difficult to collect numerous samples in loose materials such as shales. On the contrary, collecting rock fragments presents the net advantage to provide a much better statistical characterization of the site.</p><p>All samples belong to the Eocene shaly formations from the Jaca Basin. Rock fragments are mostly fractured according to the bedding and/or cleavage surfaces. We demonstrate that the anisotropy parameters P and T maintain their values, regardless the shape and size of fragments. Rock magnetism indicates that AMS is primarily governed by illite, with little contribution of magnetite. AMS provides therefore a proxy of illite organisation within the matrix.</p><p>In the footwall of the Sierra de Leyre we have defined up to 7 parallel sampling sections, whose traces are perpendicular to the direction of the main thrust. On average, each section is made up of about 10 sampling sites and about 15 fragments are collected per site, covering a few square meters.</p><p>We are restricted by the dimensions of AGICO holders (8cm<sup>3</sup> for cubes, or 10 cm<sup>3</sup> for cylinders). It is possible to use an empty 10 cm<sup>3</sup> cylinder, which can be filled with smaller fragments of rock. The automatic rotator allows a fast and precise description of the AMS tensor. We removed from analysis low susceptibility, carbonate-rich samples, that show a higher variety of magnetic minerals. All sites present homogenous results at the site scale, but with significant differences with respect to strain. P and T parameters are very sensitive to strain as illite is the dominant carrier. In addition, the ellipse of confidence of the minimum AMS axis (K3) provides a sensitive proxy to characterize the competition between bedding and cleavage.</p><p>The comparison between the different sections allows to map the areas of damage linked to the propagation of faults associated with the folds. 5 stages of development of the magnetic fabric allows the detection of damage gradients. The mapping has allowed the identification of hidden faults.    </p><p>This new approach is very promising, and allows much more detailed samplings in difficult areas, providing more robust statistical description of scalar AMS data. This methodology could be useful for the study of outcrops that are difficult to access, and more interestingly, from borehole cuttings.</p>


2019 ◽  
Vol 966 ◽  
pp. 282-289 ◽  
Author(s):  
Susilawati ◽  
Aris Doyan ◽  
Muhammad Taufik ◽  
Wahyudi ◽  
Eryn Ryantin Gunawan ◽  
...  

The research was conducted to examine the content of Fe and other metal in natural sand of beach Ampenan, Mataram, Indonesia which is expected to be used as microwave absorbent material. Characterizations of the electrical and magnetic properties Barium M-Hexaferrite (BaM) with Zn-Mn doping (BaFe12-2xZnxMnxO19) are biosynthesized. Research carried out among others tested the metal content of Fe and other metals, synthesize BaFe12-2xZnxMnxO19. The samples were characterized using Vibrating Sample Magnetometer (VSM) and Network Vector Analyzer (VNA) for the test properties of electricity and magnetism, as well as the absorption of microwaves. The results from the AAS (Atomic Absorption Spectroscopy) testing showed that each gram of magnetic minerals in the natural sand containing 16.27 mg Fe, which states that the majority of metal components content is 69.80% Fe metal with the Magnetite and Hematite phases. The result from VSM showed that the coercivity value decreased when doping ion concentration and calcination temperature increased (0.16 Tesla at 600°C for x = 0.0 and 0.09 Tesla at 800°C for x = 1.0). Value of magnetic saturation and the magnetic remanence decreased with increasing ion concentration (Ms= 4.94 emu/g at x = 0.0 decreased to 0.31 emu/g at x = 1.0) and Mr = 3.43 emu/g for x = 0.0 decreased to 0.06 emu/g at x=1.0. These indicates that the sample has been soft magnetic. The result from VNA showed that the electrical conductivity values measured in the range 8.0-15.0 GHz indicate that the sample is a semiconductor (1.62×10-2 S/cm). The result from VNA showed that the microwave absorption properties increased at higher concentration of doping ions and the calcination temperature would increase the value of Reflection Loss (RL). Maximum RL value of the sample is -14.37 dB at 15 GHz and the absorption coefficient of 96.34%. These results indicate that the BaFe10.8Zn0.6Mn0.6O19 sample can be applied as a microwave absorbent material on X-band to Ku- band frequency. Keyword: Characterization, Barium M-Hexaferrite, doping, microwave, absorbent.


2014 ◽  
Vol 119 (8) ◽  
pp. 6136-6158 ◽  
Author(s):  
Liao Chang ◽  
Andrew P. Roberts ◽  
Michael Winklhofer ◽  
David Heslop ◽  
Mark J. Dekkers ◽  
...  

Author(s):  
B. L. Soloff ◽  
T. A. Rado

Mycobacteriophage R1 was originally isolated from a lysogenic culture of M. butyricum. The virus was propagated on a leucine-requiring derivative of M. smegmatis, 607 leu−, isolated by nitrosoguanidine mutagenesis of typestrain ATCC 607. Growth was accomplished in a minimal medium containing glycerol and glucose as carbon source and enriched by the addition of 80 μg/ ml L-leucine. Bacteria in early logarithmic growth phase were infected with virus at a multiplicity of 5, and incubated with aeration for 8 hours. The partially lysed suspension was diluted 1:10 in growth medium and incubated for a further 8 hours. This permitted stationary phase cells to re-enter logarithmic growth and resulted in complete lysis of the culture.


Author(s):  
A.R. Pelton ◽  
A.F. Marshall ◽  
Y.S. Lee

Amorphous materials are of current interest due to their desirable mechanical, electrical and magnetic properties. Furthermore, crystallizing amorphous alloys provides an avenue for discerning sequential and competitive phases thus allowing access to otherwise inaccessible crystalline structures. Previous studies have shown the benefits of using AEM to determine crystal structures and compositions of partially crystallized alloys. The present paper will discuss the AEM characterization of crystallized Cu-Ti and Ni-Ti amorphous films.Cu60Ti40: The amorphous alloy Cu60Ti40, when continuously heated, forms a simple intermediate, macrocrystalline phase which then transforms to the ordered, equilibrium Cu3Ti2 phase. However, contrary to what one would expect from kinetic considerations, isothermal annealing below the isochronal crystallization temperature results in direct nucleation and growth of Cu3Ti2 from the amorphous matrix.


Author(s):  
B. H. Kear ◽  
J. M. Oblak

A nickel-base superalloy is essentially a Ni/Cr solid solution hardened by additions of Al (Ti, Nb, etc.) to precipitate a coherent, ordered phase. In most commercial alloy systems, e.g. B-1900, IN-100 and Mar-M200, the stable precipitate is Ni3 (Al,Ti) γ′, with an LI2structure. In A lloy 901 the normal precipitate is metastable Nis Ti3 γ′ ; the stable phase is a hexagonal Do2 4 structure. In Alloy 718 the strengthening precipitate is metastable γ″, which has a body-centered tetragonal D022 structure.Precipitate MorphologyIn most systems the ordered γ′ phase forms by a continuous precipitation re-action, which gives rise to a uniform intragranular dispersion of precipitate particles. For zero γ/γ′ misfit, the γ′ precipitates assume a spheroidal.


Author(s):  
R. E. Herfert

Studies of the nature of a surface, either metallic or nonmetallic, in the past, have been limited to the instrumentation available for these measurements. In the past, optical microscopy, replica transmission electron microscopy, electron or X-ray diffraction and optical or X-ray spectroscopy have provided the means of surface characterization. Actually, some of these techniques are not purely surface; the depth of penetration may be a few thousands of an inch. Within the last five years, instrumentation has been made available which now makes it practical for use to study the outer few 100A of layers and characterize it completely from a chemical, physical, and crystallographic standpoint. The scanning electron microscope (SEM) provides a means of viewing the surface of a material in situ to magnifications as high as 250,000X.


Author(s):  
D. F. Blake ◽  
L. F. Allard ◽  
D. R. Peacor

Echinodermata is a phylum of marine invertebrates which has been extant since Cambrian time (c.a. 500 m.y. before the present). Modern examples of echinoderms include sea urchins, sea stars, and sea lilies (crinoids). The endoskeletons of echinoderms are composed of plates or ossicles (Fig. 1) which are with few exceptions, porous, single crystals of high-magnesian calcite. Despite their single crystal nature, fracture surfaces do not exhibit the near-perfect {10.4} cleavage characteristic of inorganic calcite. This paradoxical mix of biogenic and inorganic features has prompted much recent work on echinoderm skeletal crystallography. Furthermore, fossil echinoderm hard parts comprise a volumetrically significant portion of some marine limestones sequences. The ultrastructural and microchemical characterization of modern skeletal material should lend insight into: 1). The nature of the biogenic processes involved, for example, the relationship of Mg heterogeneity to morphological and structural features in modern echinoderm material, and 2). The nature of the diagenetic changes undergone by their ancient, fossilized counterparts. In this study, high resolution TEM (HRTEM), high voltage TEM (HVTEM), and STEM microanalysis are used to characterize tha ultrastructural and microchemical composition of skeletal elements of the modern crinoid Neocrinus blakei.


Author(s):  
Simon Thomas

Trends in the technology development of very large scale integrated circuits (VLSI) have been in the direction of higher density of components with smaller dimensions. The scaling down of device dimensions has been not only laterally but also in depth. Such efforts in miniaturization bring with them new developments in materials and processing. Successful implementation of these efforts is, to a large extent, dependent on the proper understanding of the material properties, process technologies and reliability issues, through adequate analytical studies. The analytical instrumentation technology has, fortunately, kept pace with the basic requirements of devices with lateral dimensions in the micron/ submicron range and depths of the order of nonometers. Often, newer analytical techniques have emerged or the more conventional techniques have been adapted to meet the more stringent requirements. As such, a variety of analytical techniques are available today to aid an analyst in the efforts of VLSI process evaluation. Generally such analytical efforts are divided into the characterization of materials, evaluation of processing steps and the analysis of failures.


Author(s):  
R. J. Lauf

Fuel particles for the High-Temperature Gas-Cooled Reactor (HTGR) contain a layer of pyrolytic silicon carbide to act as a miniature pressure vessel and primary fission product barrier. Optimization of the SiC with respect to fuel performance involves four areas of study: (a) characterization of as-deposited SiC coatings; (b) thermodynamics and kinetics of chemical reactions between SiC and fission products; (c) irradiation behavior of SiC in the absence of fission products; and (d) combined effects of irradiation and fission products. This paper reports the behavior of SiC deposited on inert microspheres and irradiated to fast neutron fluences typical of HTGR fuel at end-of-life.


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