scholarly journals Studies on Amorphous Alloy Dispersed Aluminium Matrix Composite Prepared by High Pressure Torsion

2015 ◽  
Vol 5 (1) ◽  
pp. 89
Author(s):  
S. Hembrom ◽  
B. N. Roy ◽  
N. Khobragade ◽  
D. Roy
Keyword(s):  
High Pressure ◽  
Amorphous Alloy ◽  
High Pressure Torsion ◽  
Base Alloy ◽  
Hardness Measurement ◽  
Aluminium Matrix ◽  
Wear Property ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Aluminium Matrix Composite

<p class="1Body">Aluminium-based composite reinforced with Cu base amorphous alloy dispersed composite was prepared by means of high pressure torsion between a powder mix of aluminium and amorphous Cu base alloy. The X-ray diffraction pattern of powdered and consolidated composites shows the aluminium phase while the thermal stability of the amorphous alloy was studied with the aid of differential scanning calorimetry (DSC). The microstructural feature of the composite through scanning electron microscope reveals the well-distributed reinforcements in the host aluminium matrix. The hardness measurement on the as prepared composites shows significant increase in hardness with increase in reinforced amorphous alloy. Wear property of the synthesized composites were measured by using ball on plate wear tester which shows increase in wear resistance with increase in reinforced amorphous alloys.</p>

Phase Transformation in Ni-Ti Shape Memory and Superelastic Alloys Subjected to High Pressure Torsion

2010 ◽  
Vol 123-125 ◽  
pp. 1007-1010 ◽  
Author(s):  
Karimbi Koosappa Mahesh ◽  
Francisco M. Braz Fernandes ◽  
Gheorghe Gurau
Keyword(s):  
High Pressure ◽  
Phase Transformation ◽  
Shape Memory ◽  
High Pressure Torsion ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
One Stage ◽  
Heating And Cooling ◽  
Ti Alloys ◽  
M Phase

A systematic study on the phase transformation of Ni-Ti shape memory and superelastic alloys subjected to Severe Plastic Deformation (SPD) – High Pressure Torsion (HPT) technique has been carried out. Ni-Ti alloys of three compositions were chosen for the study. Specimens of these alloys in as-received (AR) condition and after HPT have been subjected to Differential Scanning Calorimetry (DSC) and X-ray Diffraction (XRD) analyses. In this study, while comparing the results of DSC thermograms and XRD spectra for the same sample conditions, some differences were observed. In the case of NiTi-H alloy after HPT, there appeared one stage phase transformation with DSC both while heating and cooling suggesting Martensite↔Austenite transformation but, with respect to XRD spectra while cooling, at the intermediate temperature of 55°C, the R-phase peaks corresponding to (1 1 2)R and (3 0 0)R planes appeared. In the thermogram obtained for the NiTi-B alloy subjected to HPT, it is observed that, while cooling, the Austenite to R-phase transformation is merged with R-phase to Martensite transformation. The results of the XRD obtained at -180°C show the presence of R-phase along with M-phase. The DSC curve of the NiTi-S alloy subjected to HPT corresponds to one stage phase transformation both while heating and cooling but, the diffractogram of the sample obtained at -180°C corresponds to the presence of both R-phase and M-phase.

Effect of High Pressure Torsion on Crystal Orientation to Improve the Thermoelectric Property of a Bi2Te3-Based Thermoelectric Semiconductor

2010 ◽  
Vol 89-91 ◽  
pp. 41-46 ◽  
Author(s):  
Maki Ashida ◽  
Takashi Hamachiyo ◽  
Kazuhiro Hasezaki ◽  
Hirotaka Matsunoshita ◽  
Z. Horita
Keyword(s):  
High Pressure ◽  
Power Factor ◽  
Crystal Orientation ◽  
High Pressure Torsion ◽  
Preferred Orientation ◽  
Orientation Factor ◽  
X Ray Diffraction ◽  
Fine Grain ◽  
Maximum Value ◽  
P Type

A Bi2Te3-based thermoelectric semiconductor was subjected by high pressure torsion (HPT). Sample disks of p-type Bi0.5Sb1.5Te3.0 were cut from sintered compacts that were made by mechanically alloying (MA) followed by hot pressing. Disks were subjected by HPT with 1, 5 and 10 turns at 473 K under 6.0 GPa of pressure. Crystal orientation was investigated by X-ray diffraction. Microstructures were characterized using scanning electron microscopy. Results indicated that HPT disks after 5 turns had a preferred orientation and a fine grain compared with pre-HPT disks while the orientation factor was decreased after HPT using 10 turns. The power factor had a maximum value at 5 turns as determined by measuring its thermoelectric properties. A maximum power factor of 4.30×10-3 Wm-1K-2 was obtained for HPT disks after 5 turns. This value was larger than that for the pre-HPT disk. The over-HPT of 10 turns was found to have caused a decrease in the preferred orientation leading to a low power factor.

scholarly journals Crystallization of Cu60Zr20Ti20 bulk metallic glass by high pressure torsion

2019 ◽  
Vol 58 (1) ◽  
pp. 304-312
Author(s):  
Ádám Révész ◽  
András Horváth ◽  
Gábor Ribárik ◽  
Erhard Schafler ◽  
David J. Browne ◽  
...  
Keyword(s):  
High Pressure ◽  
Metallic Glass ◽  
Crystallite Size ◽  
Bulk Metallic Glass ◽  
High Pressure Torsion ◽  
Average Crystallite Size ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Microstructural Parameters ◽  
Profile Fitting

Abstract Bulk metallic glass of Cu60Zr20Ti20 composition has been synthesized by copper mold casting. Slices of the as-cast glass has been subjected to severe plastic deformation by high-pressure torsion for different whole turns. The microstructure and the thermal behavior of the deformed disks have been investigated by X-ray diffraction and differential scanning calorimetry. It was confirmed that the initial compression preceding the high pressure torsion induces crystallized structure, which shows only minor further changes upon the severe plastic shear deformation achieved by twisting the sample. The X-ray line profiles have been evaluated by the Convolutional Whole Profile Fitting algorithm in order to determine the evolution of the microstructural parameters, such as the median and variance of the crystallite size distribution, average crystallite size and dislocation density as a function of the number of revolutions. Hardness measurements by nanoindentation have also been carried out on the as-cast alloys and the deformed disks.

Correlation between microstructural evolution during high-pressure torsion and isothermal heat treatment of amorphous Al85Gd8Ni5Co2 alloy

2010 ◽  
Vol 25 (7) ◽  
pp. 1388-1397 ◽  
Author(s):  
Péter Henits ◽  
Ádám Révész ◽  
Erhard Schafler ◽  
Péter J. Szabó ◽  
János L. Lábár ◽  
...  
Keyword(s):  
Heat Treatment ◽  
High Pressure ◽  
High Pressure Torsion ◽  
Thermal Sensitivity ◽  
Heat Treatments ◽  
Isothermal Heat Treatment ◽  
X Ray Diffraction ◽  
Continuous Heat Treatment ◽  
Isothermal Heat Treatments ◽  
Continuous Heat

Al85Gd8Ni5Co2 metallic glass was subjected to partial devitrification by high-pressure torsion, continuous heat treatment, and isothermal annealing. The fully amorphous alloy exhibits a well-defined transition in its first devitrification product during isothermal heat treatments from τm + α-Al phase mixture to primary α-Al by increasing the annealing temperature above 555 K. This thermal sensitivity predestinates the composition to identify the controversial thermal contribution of the plastic deformation in metallic glasses. Thermal stability and structure of the partially devitrified samples were systematically analyzed and compared by calorimetry, x-ray diffraction, and electron microscopy. It seems that the effect of severe deformation cannot be singled out by a simple isothermal heat treatment; i.e., high-pressure torsion acts as a spectrum of heat treatments performed at different annealing temperatures.

Amorphous-Alloy-Based Composites Prepared by High-Pressure Torsion

2019 ◽  
Vol 2019 (10) ◽  
pp. 994-1001 ◽  
Author(s):  
I. E. Permyakova ◽  
E. N. Blinova ◽  
I. V. Shchetinin ◽  
E. S. Savchenko
Keyword(s):  
High Pressure ◽  
Amorphous Alloy ◽  
High Pressure Torsion

scholarly journals Crystallization Features of Amorphous Rapidly Quenched High Cu Content TiNiCu Alloys upon Severe Plastic Deformation

Materials ◽  
2019 ◽  
Vol 12 (17) ◽  
pp. 2670
Author(s):  
Alexander Glezer ◽  
Nikolay Sitnikov ◽  
Roman Sundeev ◽  
Alexander Shelyakov ◽  
Irina Khabibullina
Keyword(s):  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Copper Content ◽  
Melt Spinning ◽  
High Pressure Torsion ◽  
Amorphous State ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Cu Content ◽  
Rapid Melt Quenching

In recent years, the methods of severe plastic deformation and rapid melt quenching have proven to be an effective tool for the formation of the unique properties of materials. The effect of high-pressure torsion (HPT) on the structure of the amorphous alloys of the quasi-binary TiNi–TiCu system with a copper content of more than 30 at.% produced by melt spinning technique has been analyzed using the methods of scanning electron microscopy, X-ray diffraction analysis, and differential scanning calorimetry (DSC). The structure examinations have shown that the HPT of the alloys with a Cu content ranging from 30 to 40 at.% leads to nanocrystallization from the amorphous state. An increase in the degree of deformation leads to a substantial change in the character of the crystallization reflected by the DSC curves of the alloys under study. The alloys containing less than 34 at.% Cu exhibit crystallization peak splitting, whereas the alloys containing more than 34 at.% Cu exhibit a third peak at lower temperatures. The latter effect suggests the formation of regions of possible low-temperature crystallization. It has been established that the HPT causes a significant decrease in the thermal effect of crystallization upon heating of the alloys with a high copper content relative to that of the initial amorphous melt quenched state.

scholarly journals Hardness and Wear Property of SiCp Reinforced Aluminium Matrix Composite.

1997 ◽  
Vol 44 (2) ◽  
pp. 198-201
Author(s):  
Kenzo Fukaura ◽  
Hisakichi Sunada ◽  
Yoshihiko Yokoyama ◽  
Tomohiro Tsukaguchi
Keyword(s):  
Matrix Composite ◽  
Aluminium Matrix ◽  
Wear Property ◽  
Aluminium Matrix Composite

scholarly journals Effect of the High-Pressure Torsion (HPT) and Subsequent Isothermal Annealing on the Phase Transformation in Biomedical Ti15Mo Alloy

Metals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1194 ◽  
Author(s):  
Kristína Bartha ◽  
Josef Stráský ◽  
Anna Veverková ◽  
Pere Barriobero-Vila ◽  
František Lukáč ◽  
...  
Keyword(s):  
High Pressure ◽  
High Pressure Torsion ◽  
Phase Evolution ◽  
High Energy ◽  
Phase Precipitation ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solution Treated ◽  
Α Phase ◽  
Element Partitioning

Ti15Mo metastable beta Ti alloy was solution treated and subsequently deformed by high-pressure torsion (HPT). HPT-deformed and benchmark non-deformed solution-treated materials were annealed at 400 °C and 500 °C in order to investigate the effect of UFG microstructure on the α-phase precipitation. Phase evolution was examined using laboratory X-ray diffraction (XRD) and by high-energy synchrotron X-ray diffraction (HEXRD), which provided more accurate measurements. Microstructure was observed by scanning electron microscopy (SEM) and microhardness was measured for all conditions. HPT deformation was found to significantly enhance the α phase precipitation due the introduction of lattice defects such as dislocations or grain boundaries, which act as preferential nucleation sites. Moreover, in HPT-deformed material, α precipitates are small and equiaxed, contrary to the α lamellae in the non-deformed material. ω phase formation is suppressed due to massive α precipitation and consequent element partitioning. Despite that, HPT-deformed material after ageing exhibits the high microhardness exceeding 450 HV.

Crystal Polymorphs and Multiple Crystallization Pathways of Highly Pressurized 1-Ethyl-3-Methylimidazolium Nitrate

2019 ◽  
Vol 72 (2) ◽  
pp. 87 ◽  
Author(s):  
Hiroshi Abe ◽  
Takahiro Takekiyo ◽  
Yukihiro Yoshimura ◽  
Nozomu Hamaya ◽  
Shinichiro Ozawa
Keyword(s):  
Differential Scanning Calorimetry ◽  
High Pressure ◽  
Room Temperature ◽  
Ambient Pressure ◽  
Optical Microscope ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Low Temperature Crystallization ◽  
Temperature Crystallization

Crystal polymorphs and multiple crystallization pathways of a room-temperature ionic liquid (RTIL) were observed only under high pressure (HP). The RTIL was 1-ethyl-3-methylimidazolium nitrate, [C2mim][NO3]. The HP-crystal polymorphs were related to conformations of the C2mim+ cation, and the HP-crystal pathways determined by the presence or absence of the planar′ (P′) conformation of the C2mim+ cation were switched at the bifurcation pressure (PB). Above PB, modulated crystal structures derived from the HP-inherent P′ conformer. Simultaneous X-ray diffraction and differential scanning calorimetry measurements, accompanied by optical microscope observations, confirmed the normal low-temperature crystallization of [C2mim][NO3] under ambient pressure.

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