Discovery of 40.5 ks Hard X-Ray Pulse-phase Modulations from SGR 1900+14

X-ray timing properties of the magnetar SGR 1900+14 were studied, using the data taken with Suzaku in 2009 and NuSTAR in 2016, for a time lapse of 114 and 242 ks, respectively. On both occasions, the object exhibited the characteristic two-component spectrum. The soft component, dominant in energies below ∼5 keV, showed a regular pulsation, with a period of P = 5.21006 s as determined with the Suzaku XIS, and P = 5.22669 with NuSTAR. However, in ≳ 6 keV where the hard component dominates, the pulsation became detectable with the Suzaku HXD and NuSTAR only after the data were corrected for periodic pulse-phase modulation, with a period of T = 40 − 44 ks and an amplitude of ≈1 s. Further correcting the two data sets for complex energy dependences in the phase modulation parameters, the hard X-ray pulsation became fully detectable, in 12–50 keV with the HXD and 6–60 keV with NuSTAR, using a common value of T = 40.5 ± 0.8 ks. Thus, SGR 1900+14 becomes a third example, after 4U 0142+61 and 1E 1547−5408, to show the hard X-ray pulse-phase modulation, and a second case of energy dependences in the modulation parameters. The neutron star in this system is inferred to perform free precession, as it is axially deformed by ≈ P/T = 1.3 × 10−4, presumably due to ∼ 1016 G toroidal magnetic fields. As a counterexample, the Suzaku data of the binary pulsar 4U 1626−67 were analyzed, but no similar effect was found. These results altogether argue against the accretion scenario for magnetars.

Magnetic characterization of magnetoactive elastomers containing magnetic hard particles using first-order reversal curve analysis

The use of new types of intelligent materials is becoming increasingly widespread. These include magnetoactive elastomers with hard magnetic filling components, which offer the unique chance to adapt active and passive material properties. In this context, this paper presents an overview of the experimental results on the study of the magnetic properties of elastic composites with a magnetic hard component. First-order reversal curves, which are recorded with a vibrating sample magnetometer, are used as method to characterize the magnetic material behavior. The influence of various parameters on the process of magnetization of composites is considered, including the stiffness of the polydimethylsiloxane-based matrix polymer, the particle ratio and the particle size as well as the so-called training effect.

High-temperature three-axis IRM Lowrie test

<p>The three-axis isothermal remanent magnetization (IRM) test (the Lowrie test; Lowrie, 1990, Geophys. Res. Lett., 17, 159-162) is a useful tool to identify ferromagnetic minerals by their coercivity and unblocking temperature spectra. In this study, we explore a variant of the Lowrie test in which measurements are conducted directly at elevated temperatures, and compare its performance with the results of the conventional stepwise procedure. IRM acquisition fields applied along three orthogonal axes were 1 T, 200 mT and 40 mT, respectively. The field value for the soft component was chosen so as to include ca. 90% of its coercivity spectrum. For the hard component the maximum available field was used. The test is applied to characterize the magnetic mineralogy of archaeological baked clays and bricks from Bulgaria and Russia. Bulgarian samples are baked clays from various Neolithic (5700-5300 BCE) archaeological sites and several bricks of the Roman epoch (III-IV c. AD). Samples from Russia are bricks originating from several regions with ages from XIII to early XIX c. AD.</p><p>The low- and intermediate-coercivity components of IRM in the studied samples are typically demagnetized by 520-550°C, compatible with substituted or cation-deficient magnetite or, possibly, maghemite. This is supported by the absence of the Verwey transition in studied samples (Kosterov et al., 2021, Geophys. J. Int., 224(2), 1256-1271). The high-coercivity component appears to be carried by two mineral phases with very distinct unblocking temperatures, 120-200°C and 500 to 640°C. The first phase is similar to the high coercivity, low unblocking temperature (HCSLT) phase described by McIntosh et al., 2007 (Geophys. Res. Lett., 34, L21302, doi: 10.1029/22007GL031168), and the second one appears to be hematite with variable degree of substitution.</p><p>Performance of the high-temperature variant of the Lowrie test compares favorably with the classical procedure, while the former is also significantly faster and yields a superior temperature resolution.</p><p>This study is supported by Russian Foundation of the Basic Research, grant 19-55-18006, and by Bulgarian National Science Fund, grant KP-06-Russia-10.</p>

A two-component Comptonisation model for the type-B QPO in MAXI J1348–630

Spectral-timing analysis of the fast variability observed in X-rays is a powerful tool to study the physical and geometrical properties of the accretion/ejection flows in black-hole binaries. The origin of type-B quasi-periodic oscillations (QPO), predominantly observed in black-hole candidates in the soft-intermediate state, has been linked to emission arising from the relativistic jet. In this state, the X-ray spectrum is characterised by a soft-thermal blackbody-like emission due to the accretion disc, an iron emission line (in the 6–7 keV range), and a power-law like hard component due to Inverse-Compton scattering of the soft-photon source by hot electrons in a corona or the relativistic jet itself. The spectral-timing properties of MAXI J1348–630 have been recently studied using observations obtained with the NICER observatory. The data show a strong type-B QPO at ∼4.5 Hz with increasing fractional rms amplitude with energy and positive lags with respect to a reference band at 2–2.5 keV. We use a variable-Comptonisation model that assumes a sinusoidal coherent oscillation of the Comptonised X-ray flux and the physical parameters of the corona at the QPO frequency, to fit simultaneously the energy-dependent fractional rms amplitude and phase lags of this QPO. We show that two physically-connected Comptonisation regions can successfully explain the radiative properties of the QPO in the full 0.8–10 keV energy range.

Mechano-chemistry of human femoral diaphysis revealed by correlative Brillouin–Raman microspectroscopy

Brillouin–Raman microspectroscopy is presented as an innovative label-free all-optical investigation approachable to characterize the chemical composition and the mechanical properties of human tissues at micrometric resolution. Brillouin maps unveil mechanical heterogeneities in a human femoral diaphysis, showing a ubiquitous co-existence of hard and soft components, even in the most compact sections. The novel correlative analysis of Brillouin and Raman maps shows that the relative intensity of Brillouin peaks is a good proxy for the fraction of mineralized fibers and that the stiffness (longitudinal elastic modulus) of the hard component is linearly dependent on the hydroxyapatite concentration. For the soft component, a gradient of composition is found, ranging from an abundance of proteins in the more compact, external, bone to abundance of lipids, carotenoids, and heme groups approaching the trabecular, inner, part of the diaphysis. This work unveils the strong potential of correlative mechano-chemical characterization of human tissues at a micrometric resolution for both fundamental and translational research.

Mapping and identification of soft corona proteins at nanoparticles and their impact on cellular association

The current understanding of the biological identity that nanoparticles may acquire in a given biological milieu is mostly inferred from the hard component of the protein corona (HC). The composition of soft corona (SC) proteins and their biological relevance have remained elusive due to the lack of analytical separation methods. Here, we identify a set of specific corona proteins with weak interactions at silica and polystyrene nanoparticles by using an in situ click-chemistry reaction. We show that these SC proteins are present also in the HC, but are specifically enriched after the capture, suggesting that the main distinction between HC and SC is the differential binding strength of the same proteins. Interestingly, the weakly interacting proteins are revealed as modulators of nanoparticle-cell association mainly through their dynamic nature. We therefore highlight that weak interactions of proteins at nanoparticles should be considered when evaluating nano-bio interfaces.

Fabrication of Hard–Soft Microfluidic Devices Using Hybrid 3D Printing

Widely accessible, inexpensive, easy-to-use consumer 3D printers, such as desktop stereolithography (SLA) and fused-deposition modeling (FDM) systems are increasingly employed in prototyping and customizing miniaturized fluidic systems for diagnostics and research. However, these 3D printers are generally limited to printing parts made of only one material type, which limits the functionality of the microfluidic devices without additional assembly and bonding steps. Moreover, mating of different materials requires good sealing in such microfluidic devices. Here, we report methods to print hybrid structures comprising a hard, rigid component (clear polymethacrylate polymer) printed by a low-cost SLA printer, and where the first printed part is accurately mated and adhered to a second, soft, flexible component (thermoplastic polyurethane elastomer) printed by an FDM printer. The prescribed mounting and alignment of the first-printed SLA-printed hard component, and its pre-treatment and heating during the second FDM step, can produce leak-free bonds at material interfaces. To demonstrate the utility of such hybrid 3D-printing, we prototype and test three components: i) finger-actuated pump, ii) quick-connect fluid coupler, and iii) nucleic acid amplification test device with screw-type twist sealing for sample introduction.

Fabrication of Highly Filled Composites with an Innovative Miniaturized Spouted Bed

In nature bio-composites such as nacre show remarkable mechanical properties due to their complex hierarchical structure and high-volume fraction of its hard component. These composites are highly interesting for structural applications in different branches of industries for mechanical engineering and process technology. The aim of this work was to provide a scalable method for the production of highly filled composites by mimicking the structure of bio-composites. Therefore, composites from iron oxide (Fe2O3) and SBC-polymer (styrene-butadiene block copolymer) were fabricated by using a miniaturized spouted bed with an innovative fluidization gap design. Small iron oxide particles (25–45 μm) were fluidized in the spouted bed and coated with a polymer solution via a bottom spray nozzle. Afterwards the coated granules were hot-pressed and the mechanical properties of the obtained composites were tested. By this method composites with a bending strength of up to 6 MPa were fabricated. Although the mechanical properties of these artificial composites are still lower than those of the natural role models, it was shown that the spouted bed is a suitable technique for the fabrication of highly filled composites. For further optimization of the mechanical properties more complex and tailor-made starting materials will be used in following studies.

Mapping and identification of soft corona proteins at nanoparticles and their impact on cellular association

The current understanding of the biological identity that nanoparticles may acquire in a given biological milieu is mostly inferred from the hard component of the protein corona (HC). The composition of soft corona (SC) proteins and their biological relevance have remained elusive due to the lack of analytical separation methods. Here, we identified a set of specific corona proteins with weak interactions at silica and polystyrene nanoparticles by using an in situ click-chemistry reaction. We show that these SC proteins are present also in the HC, but are specifically enriched after the capture, suggesting that the main distinction between HC and SC is the differential binding strength of the same proteins. Interestingly, the weakly interacting proteins in the SC are revealed as modulators of nanoparticle-cell association, in spite of their short residence time. We therefore highlight that weak interactions of proteins at nanoparticles should be considered when evaluating nano-bio interfaces.

XMM-Newton observations of the symbiotic recurrent nova T CrB: evolution of X-ray emission during the active phase

ABSTRACT We present an analysis of the XMM-Newton observations of the symbiotic recurrent nova T CrB, obtained during its active phase which started in 2014–2015. The XMM-Newton spectra of T CrB have two prominent components: a soft one (0.2–0.6 keV), well represented by blackbody emission, and a heavily absorbed hard component (2–10 keV), well matched by optically-thin plasma emission with high temperature (kT ≈ 8 keV). The XMM-Newton observations reveal evolution of the X-ray emission from T CrB in its active phase. Namely, the soft component in its spectrum is decreasing with time, while the opposite is true for the hard component. Comparison with data obtained in the quiescent phase shows that the soft component is typical only for the active phase, while the hard component is present in both phases but it is considerably stronger in the quiescent phase. Presence of stochastic variability (flickering) on time-scales of minutes and hours is confirmed both in X-rays and UV (UVM2 filter of the XMM-Newton optical monitor). On the other hand, periodic variability of 6000–6500 s is found for the first time in the soft X-ray emission (0.2–0.6 keV) from T CrB. We associate this periodic variability with the rotational period of the white dwarf in this symbiotic binary.