scholarly journals Experimental Investigation on Mechanical Properties of In Situ Cemented Paste Backfill Containing Coal Gangue and Fly Ash

2020 ◽  
Vol 2020 ◽  
pp. 1-12
Author(s):  
Xinguo Zhang ◽  
Shichuan Zhang

Cemented paste backfill containing coal gangue and fly ash (CGFACPB) is an emerging backfill technique for coal mines that allows environmentally hazardous coal gangue and fly ash to be reused in the underground goaf. Meanwhile, CGFACPB can provide an efficient ground support and reduce the surface subsidence. Due to the difference of consolidation environment between the laboratory and the field, the mechanical properties of the cemented paste backfill vary significantly. In this paper, the core specimens were collected from an underground coal mine where the CGFACPB was used for coal mining, and the mechanical properties of the collected specimens were investigated. The cores were obtained from the underground coal mine, and then the standard cylinders or discs were prepared in laboratory. The uniaxial compressive strength (UCS), Young’s modulus, and Poisson’s ratio were determined by the compression tests, and the tensile strength was achieved by the Brazilian test. Then the internal friction angle and cohesion were calculated using the improved Mohr–Coulomb strength criterion. The results showed the development of UCS can be divided into four stages, and the final long-term stable value was about 5.1 MPa. The development of Young’s modulus had similar trend. Young’s modulus had a range from 550 MPa to 750 MPa and the mean value of 675 MPa. Poisson’s ratio gradually increased with the underground curing duration and eventually approached the stable value of 0.18. The failure type of compression samples was mainly single-sided shear failure. The development of tensile strength can be divided into two stages, and the stable value of the tensile strength was about 1.05 MPa. The development of cohesion can be divided into four stages, and the stable value was about 1.75 MPa. The stable value of the internal friction angle was about 25°. This study can provide significant references for not only the long-term stability evaluation of CGFACPB in the field but also the design of optimal recipe of the cemented paste backfill (CPB).

2019 ◽  
Vol 9 (1) ◽  
Author(s):  
Numan Salah ◽  
Abdulrahman Muhammad Alfawzan ◽  
Abdu Saeed ◽  
Ahmed Alshahrie ◽  
Waleed Allafi

AbstractCarbon nanotubes (CNTs) are widely investigated for preparing polymer nanocomposites, owing to their unique mechanical properties. However, dispersing CNTs uniformly in a polymer matrix and controlling their entanglement/agglomeration are still big technical challenges to be overcome. The costs of their raw materials and production are also still high. In this work, we propose the use of CNTs grown on oil fly ash to solve these issues. The CNTs of oil fly ash were evaluated as reinforcing materials for some common thermoplastics. High-density polyethylene (HDPE) was mainly reinforced with various weight fractions of CNTs. Xylene was used as a solvent to dissolve HDPE and to uniformly disperse the CNTs. Significantly enhanced mechanical properties of HDPE reinforced at a low weight fraction of these CNTs (1–2 wt.%), mainly the tensile strength, Young’s modulus, stiffness, and hardness, were observed. The tensile strength and Young’s modulus were enhanced by ~20 and 38%, respectively. Moreover, the nanoindentation results were found to be in support to these findings. Polycarbonate, polypropylene, and polystyrene were also preliminarily evaluated after reinforcement with 1 wt.% CNTs. The tensile strength and Young’s Modulus were increased after reinforcement with CNTs. These results demonstrate that the CNTs of the solid waste, oil fly ash, might serve as an appropriate reinforcing material for different thermoplastics polymers.


2012 ◽  
Vol 3 (1) ◽  
pp. 13-26
Author(s):  
Myrtha Karina ◽  
Lucia Indrarti ◽  
Rike Yudianti ◽  
Indriyati

The effect of castor oil on the physical and mechanical properties of bacterial cellulose is described. Bacterial cellulose (BC) was impregnated with 0.5–2% (w/v) castor oil (CO) in acetone–water, providing BCCO films. Scanning electron micrographs revealed that the castor oil penetrated the pores of the bacterial cellulose, resulting in a smoother morphology and enhanced hydrophilicity. Castor oil caused a slight change in crystallinity indices and resulted in reduced tensile strength and Young's modulus but increased elongation at break. A significant reduction in tensile strength and Young's modulus was achieved in BCCO films with 2% castor oil, and there was an improvement in elongation at break and hydrophilicity. Impregnation with castor oil, a biodegradable and safe plasticiser, resulted in less rigid and more ductile composites.


2021 ◽  
Author(s):  
Yanhong Jin ◽  
Yuanyuan Jing ◽  
Wenxin Hu ◽  
Jiaxian Lin ◽  
Yu Cheng ◽  
...  

Abstract Lignin has been used as a sustainable and eco-friendly filler in composite fibers. However, lignin aggregation occurred at high lignin content, which significantly hindered the further enhancement of fiber performance. The incorporation of graphene oxide (GO) enhanced the mechanical properties of the lignin/poly(vinyl alcohol) (PVA) fibers and affected their structure. With the GO content increasing from 0 to 0.2%, the tensile strength of 5% lignin/PVA fibers increased from 491 MPa to 631 MPa, and Young's modulus increased from 5.91 GPa to 6.61 GPa. GO reinforced 30% lignin/PVA fibers also showed the same trend. The tensile strength increased from 455 MPa to 553 MPa, and Young's modulus increased from 5.39 GPa to 7 GPa. The best mechanical performance was observed in PVA fibers containing 5% lignin and 0.2% GO, which had an average tensile strength of 631 MPa and a Young’s modulus of 6.61 GPa. The toughness values of these fibers are between 9.9-15.6 J/g, and the fibrillar and ductile fracture microstructure were observed. Structure analysis of fibers showed that GO reinforced 5% lignin/PVA fibers had higher crystallinity, and evidence of hydrogen bonding among GO, lignin, and PVA in the gel fibers was revealed. Further, water resistance and swelling behavior of composite PVA fibers were studied to further evidence the structure change of composite fibers.


2020 ◽  
Author(s):  
Jackie E. Kendrick ◽  
Lauren N. Schaefer ◽  
Jenny Schauroth ◽  
Andrew F. Bell ◽  
Oliver D. Lamb ◽  
...  

Abstract. Volcanoes represent one of the most critical geological settings for hazard modelling due to their propensity to both unpredictably erupt and collapse, even in times of quiescence. Volcanoes are heterogeneous at multiple scales, from porosity which is variably distributed and frequently anisotropic to strata that are laterally discontinuous and commonly pierced by fractures and faults. Due to variable and, at times, intense stress and strain conditions during and post-emplacement, volcanic rocks span an exceptionally wide range of physical and mechanical properties. Understanding the constituent materials' attributes is key to improving the interpretation of hazards posed by the diverse array of volcanic complexes. Here, we examine the spectrum of physical and mechanical properties presented by a single dome-forming eruption at a dacitic volcano, Mount Unzen (Japan) by testing a number of isotropic and anisotropic lavas in tension and compression and using monitored acoustic emission (AE) analysis. The lava dome was erupted as a series of 13 lobes between 1991–1995, and its ongoing instability means much of the volcano and its surroundings remain within an exclusion zone today. During a field campaign in 2015, we selected 4 representative blocks as the focus of this study. The core samples from each block span range in porosity from 9.14 to 42.81 %, and permeability ranges from 1.54 × 10−14 to 2.67 × 10−10 m2 (from 1065 measurements). For a given porosity, sample permeability varies by > 2 orders of magnitude is lower for macroscopically anisotropic samples than isotropic samples of similar porosity. An additional 379 permeability measurements on planar block surfaces ranged from 1.90 × 10−15 to 2.58 × 10−12 m2, with a single block having higher standard deviation and coefficient of variation than a single core. Permeability under confined conditions showed that the lowest permeability samples, whose porosity largely comprises microfractures, are most sensitive to effective pressure. The permeability measurements highlight the importance of both scale and confinement conditions in the description of permeability. The uniaxial compressive strength (UCS) ranges from 13.48 to 47.80 MPa, and tensile strength (UTS) using the Brazilian disc method ranges from 1.30 to 3.70 MPa, with crack-dominated lavas being weaker than vesicle-dominated materials of equivalent porosity. UCS is lower in saturated conditions, whilst the impact of saturation on UTS is variable. UCS is between 6.8 and 17.3 times higher than UTS, with anisotropic samples forming each end member. The Young's modulus of dry samples ranges from 4.49 to 21.59 GPa and is systematically reduced in water-saturated tests. The interrelation of porosity, UCS, UTS and Young's modulus was modelled with good replication of the data. Acceleration of monitored acoustic emission (AE) rates during deformation was assessed by fitting Poisson point process models in a Bayesian framework. An exponential acceleration model closely replicated the tensile strength tests, whilst compressive tests tended to have relatively high early rates of AEs, suggesting failure forecast may be more accurate in tensile regimes, though with shorter warning times. The Gutenberg-Richter b-value has a negative correlation with connected porosity for both UCS and UTS tests which we attribute to different stress intensities caused by differing pore networks. b-value is higher for UTS than UCS, and typically decreases (positive Δb) during tests, with the exception of cataclastic samples in compression. Δb correlates positively with connected porosity in compression, and negatively in tension. Δb using a fixed sampling length may be a more useful metric for monitoring changes in activity at volcanoes than b-value with an arbitrary starting point. Using coda wave interferometry (CWI) we identify velocity reductions during mechanical testing in compression and tension, the magnitude of which is greater in more porous samples in UTS but independent of porosity in UCS, and which scales to both b-value and Δb. Yet, saturation obscures velocity changes caused by evolving material properties, which could mask damage accrual or source migration in water-rich environments such as volcanoes. The results of this study highlight that heterogeneity and anisotropy within a single system not only add uncertainty but also have a defining role in the channelling of fluid flow and localisation of strain that dictate a volcano's hazards and the geophysical indicators we use to interpret them.


2021 ◽  
Vol 32 (2) ◽  
pp. 87-104
Author(s):  
Pui-Voon Yap ◽  
Ming-Yeng Chan ◽  
Seong-Chun Koay

This research work highlights the mechanical properties of multi-material by fused deposition modelling (FDM). The specimens for tensile and flexural test have been printed using polycarbonate (PC) material at different combinations of printing parameters. The effects of varied printing speed, infill density and nozzle diameter on the mechanical properties of specimens have been investigated. Multi-material specimens were fabricated with acrylonitrile butadiene styrene (ABS) as the base material and PC as the reinforced material at the optimum printing parameter combination. The specimens were then subjected to mechanical testing to observe their tensile strength, Young’s modulus, percentage elongation, flexural strength and flexural modulus. The outcome of replacing half of ABS with PC to create a multi-material part has been examined. As demonstrated by the results, the optimum combination of printing parameters is 60 mm/s printing speed, 15% infill density and 0.8 mm nozzle diameter. The combination of ABS and PC materials as reinforcing material has improved the tensile strength (by 38.46%), Young’s modulus (by 23.40%), flexural strength (by 23.90%) and flexural modulus (by 37.33%) while reducing the ductility by 14.31% as compared to pure ABS. The results have been supported by data and graphs of the analysed specimens.


2018 ◽  
Vol 917 ◽  
pp. 52-56
Author(s):  
Jirapornchai Suksaeree

Recently, Thai herbs are widely used as medicine to treat some illnesses. Zingiber cassumunar Roxb., known by the Thai name “Plai”, is a popular anti-inflammatory, antispasmodic herbal body and muscle treatment. This research aimed to prepare herbal patches that incorporated the 3 g of crude Z. cassumunar oil. The herbal patches made from different polymer blends were 2 g of 3.5%w/v chitosan and 5 g of 20%w/v hydroxypropyl methylcellulose (HPMC), or 2 g of 3.5%w/v chitosan and 5 g of 20%w/v polyvinyl alcohol (PVA) using 2 g of glycerin as a plasticizer. They were prepared by mixing all ingredients in a beaker and produced by solvent casting method in hot air oven at 70±2oC. The completed herbal patches were evaluated for their mechanical properties including Young’s modulus, ultimate tensile strength, elongation at break, T-peel strength, and tack adhesion. The thickness of blank and herbal patches was 0.263-0.282 mm and 0.269-0.275 mm, respectively. Young’s modulus, ultimate tensile strength, elongation at break, T-peel strength, and tack adhesion were 104.73-142.71 MPa, 87.92-93.28 MPa, 154.39-174.98 %, 3.43-4.88 MPa, and 5.29-7.02 MPa, respectively, for blank patches, and 116.83-147.28 MPa, 89.49-100.47 MPa, 133.78-159.27 %, 2.01-3.98 MPa, and 4.03-5.19 MPa, respectively, for herbal patches. We prepared herbal blended patches made from chitosan/PVA or chitosan/HPMC polymer matrix blends incorporating the crude Z. cassumunar oil. They had good mechanical properties that might be developed for herbal medicinal application.


2018 ◽  
Vol 2018 ◽  
pp. 1-8
Author(s):  
Toan Duy Nguyen ◽  
Chinh Thuy Nguyen ◽  
Van Thanh Thi Tran ◽  
Giang Vu Nguyen ◽  
Hai Viet Le ◽  
...  

Plasticized polyvinyl chloride (PVC) was fabricated using epoxidized soybean oil (ESBO) as a secondary bioplasticizer with dioctyl phthalate (DOP). The PVC/MFA/CB composites were prepared by melt mixing of the plasticized PVC with modified fly ash (MFA), carbon black N330 (CB), and polychloroprene (CR) in a Haake Rheomix mixer using a rotation speed of 50 rpm at 175°C for 6 min and then compressed by Toyoseiki pressure machine under 15 MPa. The effect of ESBO content on morphology, melt viscosity, tensile properties, and flame retardancy of PVC/MFA/CB composites was investigated. The obtained results showed that the incorporation of ESBO has significantly enhanced the processing ability, Young’s modulus, tensile strength, and elongation at break of the PVC/MFA/CB composites. The torque of PVC/MFA/CB composites was increased to approximately 12% when 50 wt% of DOP was replaced by ESBO. When ESBO was 20 wt% in comparison with DOP weight, the elongation at break, tensile strength, and Young’s modulus of the composites were increased to 48%, 24%, and 4.5%, respectively. Correspondingly, thermogravimetric analysis results confirmed that ESBO had improved the thermostability of the PVC composites. The ESBO have potential as a secondary bioplasticizer replacement material for DOP owing to their better thermomechanical stability.


2018 ◽  
Vol 36 (4) ◽  
pp. 2171-2187 ◽  
Author(s):  
Naguleswaran Niroshan ◽  
Ling Yin ◽  
Nagaratnam Sivakugan ◽  
Ryan Llewellyn Veenstra

Author(s):  
Mohammadreza Kamali ◽  
Mahmoud Khalifeh ◽  
Arild Saasen ◽  
Laurent Delabroy

Abstract Integrated zonal isolation is well-known as a key parameter for safe drilling operation and well completion of oil and gas wells. An extensive research on alternative materials has been conducted in the past concerning primary cementing, overcoming annular leaks, and permanent well abandonment. The present article focuses on geopolymers, expansive cement, pozzolan based sealant and thermosetting resins. The viscous behavior and the pumpability of the different materials have been investigated and benchmarked with the properties of neat class G Portland cement. The current study includes short-term mechanical properties of the above-mentioned materials. These properties include compressive strength development, Young’s modulus, indirect tensile strength, and sonic strength. The tests are performed in accordance with API 10B-2 and ASTM D3967-16 for all the materials for 1, 3, 5, and 7-day of curing at 90°C and elevated (172 bar) and atmospheric pressures. Our results show a mixed behavior from the materials. According to uniaxial compressive test results, all the candidate barrier materials developed strength during the considered period; however, the geopolymer and pozzolanic-based mixture did not develop early strength. The expansive cement showed an acceptable early compressive strength, but strength reduction was noticed after some time. The strength reduction of expansive cement was also observed for the indirect tensile strength. All the materials become stiffer overtime as they made more strength. For the neat class G cement and expansive cement, the Young’s modulus showed a minimum after 5 days, but it was increased.


2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
Qing-Sheng Yang ◽  
Bing-Qi Li ◽  
Xiao-Qiao He ◽  
Yiu-Wing Mai

This investigation focuses on the design of functionalization configuration at the atomic level to determine the influence of atomic structure on the mechanical properties of functionalized carbon nanotubes (F-CNTs) and their composites. Tension and compressive buckling behaviors of different configurations of CNTs functionalized by H atoms are studied by a molecular dynamics (MD) method. It is shown that H-atom functionalization reduces Young’s modulus of CNTs, but Young’s modulus is not sensitive to the functionalization configuration. The configuration does, however, affect the tensile strength and critical buckling stress of CNTs. Further, the stress-strain relations of composites reinforced by nonfunctionalized and various functionalized CNTs are analyzed.


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