Effect of Heat Treatment on the Tensile Strength of Glass Fibre Reinforced Polypropylene

2003 ◽  
Vol 11 (5) ◽  
pp. 369-381
Author(s):  
Jeng-Shyong Lin

Improvement of the interfacial adhesion by heat treatment of glass fibre reinforced polypropylene composite was studied. Polypropylene blended with glass fibres was injection-molded. The molded parts were heat treated at various temperatures for various times. Characterization of the mechanical properties of the resulting samples was performed including measurement of the critical fibre length, and differential scanning calorimetry. The results show that the critical fibre length increases while the tensile strength decreases with increasing testing temperature. At 25 and 80°C, heat treatment can improve the tensile strength. At or above 120°C, certain treatment conditions cause the tensile strength to drop significantly.

2002 ◽  
Vol 10 (8) ◽  
pp. 607-618 ◽  
Author(s):  
Jeng-Shyong Lin

The improvement of the interfacial adhesion of glass fibre reinforced polypropylene composites by heat treatment was studied. Polypropylene blended with short glass fibres was injection moulded. The moulded specimens were heat treated at various temperatures and for various times. Characterization of the mechanical properties of the samples was performed, including measurement of the critical fibre length. Impact tests were performed. The fracture surfaces were examined using a scanning electron microscope. The results show that the impact strength increased with the testing temperature. At 25°C, the impact strength was dominated by the fibre fracture mechanism. At temperatures above 120°C, it was strongly influenced by the PP matrix. At higher temperatures, the impact strength increased significantly because of the formation of extra cracks.


2002 ◽  
Vol 10 (3) ◽  
pp. 211-218
Author(s):  
Jeng-Shyong Lin ◽  
Sheng-Kuen Wu

In this work, the effect of heat treatment on the fracture toughness of glass fibre reinforced polypropylene was studied. Polypropylene blended with short glass fibres was injection-moulded. The moulded parts were heat treated at 150°C for 30 min. The crack growth resistance curve (R-curve) was measured to evaluate the effect of heat treatment on the fracture toughness, and to determine the stress intensity factor at the point of instability, KR(ins). The fracture surface was examined using scanning electron microscope to analyze the fracture mechanism. The results show that the stress intensity factor at the unstable fracture point KR(ins) increases with the initial crack length.


2021 ◽  
pp. 152808372110649
Author(s):  
Ajay Jayswal ◽  
Sabit Adanur

Fused Deposition Modeling (FDM) is a widely used 3D printing technique, which works based on the principle of melted polymer extrusion through nozzle(s) and depositing them on a build plate layer by layer. However, products manufactured with this method lack proper mechanical strength. In this work, 2/1 twill weave fabric structures are 3D printed using poly (lactic) acid (PLA). The ultimate tensile strength in the warp and weft directions and the modulus (stiffnesses) are measured for non-heat-treated (NHT) samples. The printed samples were heat-treated (HT) to improve the strength and stiffness. The variation in ultimate tensile strength is statistically insignificant in warp direction at all temperatures; however, the tensile strength in weft direction decreased after heat treatment. The modulus in warp direction increased by 31% after heat treatment while in the weft direction it decreased after heat treatment. Differential scanning calorimetry (DSC) tests showed the highest crystallinity at 125°C. The properties of the twill fabrics were compared with a standard dog-bone (DB) specimen using uniaxial tensile tests, Differential scanning calorimetry tests, and optical microscope (OM). For dog-bone specimens, the maximum values of crystallinity, ultimate tensile strength, and modulus were found to be at 125°C. The maximum crystallinity percentages are higher than that of the NHT samples. The ultimate tensile strength of NHT DB specimen 3D printed in horizontal orientation improved after heat treatment. The ultimate tensile strength of DB samples in vertical directions increased after heat treatment as well. The stiffness increased in both directions for DB samples.


Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1036
Author(s):  
Eduardo Colin García ◽  
Alejandro Cruz Ramírez ◽  
Guillermo Reyes Castellanos ◽  
José Federico Chávez Alcalá ◽  
Jaime Téllez Ramírez ◽  
...  

Ductile iron camshafts low alloyed with 0.2 and 0.3 wt % vanadium were produced by one of the largest manufacturers of the ductile iron camshafts in México “ARBOMEX S.A de C.V” by a phenolic urethane no-bake sand mold casting method. During functioning, camshafts are subject to bending and torsional stresses, and the lobe surfaces are highly loaded. Thus, high toughness and wear resistance are essential for this component. In this work, two austempering ductile iron heat treatments were evaluated to increase the mechanical properties of tensile strength, hardness, and toughness of the ductile iron camshaft low alloyed with vanadium. The austempering process was held at 265 and 305 °C and austempering times of 30, 60, 90, and 120 min. The volume fraction of high-carbon austenite was determined for the heat treatment conditions by XRD measurements. The ausferritic matrix was determined in 90 min for both austempering temperatures, having a good agreement with the microstructural and hardness evolution as the austempering time increased. The mechanical properties of tensile strength, hardness, and toughness were evaluated from samples obtained from the camshaft and the standard Keel block. The highest mechanical properties were obtained for the austempering heat treatment of 265 °C for 90 min for the ADI containing 0.3 wt % V. The tensile and yield strength were 1200 and 1051 MPa, respectively, while the hardness and the energy impact values were of 47 HRC and 26 J; these values are in the range expected for an ADI grade 3.


Author(s):  
Abhijit Biswas ◽  
Suman Kalyan Das ◽  
Prasanta Sahoo

The microstructural changes of electroless Ni–P–Cu coating at various heat-treatment conditions are investigated to understand its implications on the tribological behavior of the coating. Coatings are heat-treated at temperatures ranging between 200°C and 800 °C and for 1–4 h duration. Ni–P–Cu coatings exhibit two-phase transformations in the temperature range of 350–450 °C and the resulting microstructural changes are found to significantly affect their thermal stability and tribological attributes. Hardness of the coating doubles when heat-treated at 452 °C, due to the formation of harder Ni3P phase and crystalline NiCu. Better friction and wear performance are also noted upon heat treatment of the coating at the phase transformation regime, particularly at 400 °C. Wear mechanism is characterized by a mixed adhesive cum abrasive wear phenomena. Heat treatment at higher temperature (600 °C and above) and longer duration (4 h) results in grain coarsening phenomenon, which negatively influences the hardness and tribological characteristics of the coating. Besides, diffusion of iron from the ferrous substrate as well as greater oxide formation are noticed when the coating is heat-treated at higher temperatures and for longer durations (4 h).


Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 647 ◽  
Author(s):  
Bingrong Zhang ◽  
Lingkun Zhang ◽  
Zhiming Wang ◽  
Anjiang Gao

In order to obtain high-strength and high-ductility Al–Si–Cu–Mg alloys, the present research is focused on optimizing the composition of soluble phases, the structure and morphology of insoluble phases, and artificial ageing processes. The results show that the best matches, 0.4 wt% Mg and 1.2 wt% Cu in the Al–9Si alloy, avoided the toxic effect of the blocky Al2Cu on the mechanical properties of the alloy. The addition of 0.6 wt% Zn modified the morphology of eutectic Si from coarse particles to fine fibrous particles and the texture of Fe-rich phases from acicular β-Fe to blocky π-Fe in the Al–9Si–1.2Cu–0.4Mg-based alloy. With the optimization of the heat treatment parameters, the spherical eutectic Si and the fully fused β-Fe dramatically improved the ultimate tensile strength and elongation to fracture. Compared with the Al–9Si–1.2Cu–0.4Mg-based alloy, the 0.6 wt% Zn modified alloy not only increased the ultimate tensile strength and elongation to fracture of peak ageing but also reduced the time of peak ageing. The following improved combination of higher tensile strength and higher elongation was achieved for 0.6 wt% Zn modified alloy by double-stage ageing: 100 °C × 3 h + 180 °C × 7 h, with mechanical properties of ultimate tensile strength (UTS) of ~371 MPa, yield strength (YS) of ~291 MPa, and elongation to fracture (E%) of ~5.6%.


2021 ◽  
Vol 875 ◽  
pp. 203-210
Author(s):  
Talha Ahmed ◽  
Wali Muhammad ◽  
Zaheer Mushtaq ◽  
Mustasim Billah Bhatty ◽  
Hamid Zaigham

In this study, mechanical properties of friction stir welded Aluminum Alloy (AA) 6061 in three different heat treatment conditions i.e. Annealed (O), Artificially aged (T6) and Post Weld Heat Treated (PWHT) were compared. Plates were welded in a butt joint form. Parameters were optimized and joints were fabricated using tool rotational speed and travel speed of 500 rpm and 350 mm/min respectively. Two sets of plates were welded in O condition and out of which one was, later, subjected to post weld artificial aging treatment. Third set was welded in T6 condition. The welds were characterized by macro and microstructure analysis, microhardness measurement and mechanical testing. SEM fractography of the tensile fracture surfaces was also performed. Comparatively better mechanical properties were achieved in the plate with PWHT condition.


Fibers ◽  
2019 ◽  
Vol 7 (4) ◽  
pp. 27 ◽  
Author(s):  
Peter Jenkins ◽  
Liu Yang ◽  
James Thomason

The tensile strength of single water-sized E-glass fibres that were thermally conditioned, either in air or under vacuum, was investigated. The vacuum removed water from the conditioning atmosphere, as well as the fibre surfaces, at room temperature but retained tensile strength of fibres treated in the absence of water were not significantly different from those thermally conditioned in a standard air furnace. The results suggest that water, either in the treatment atmosphere or on the surface of the fibres, is not a significant factor in fundamental glass fibre strength loss at an elevated temperature. It may, therefore, be necessary to consider alternative theories to explain this strength loss.


2010 ◽  
Vol 6 (3) ◽  
pp. 373-382
Author(s):  
Ali Nazari ◽  
Shadi Riahi

PurposeThe aims of this study is to analyze failure of two types of high‐strength low‐alloy (HSLA) steels which are used in wheel bolts 10.9 grade, boron steel and chromium‐molybdenum steel, before and after heat treatment.Design/methodology/approachThe optimum heat treatment to obtain the best tensile behavior was determined and Charpy impact and Rockwell hardness tests were performed on the two steel types before and after the optimum heat treating.FindingsFractographic studies show a ductile fracture for heat‐treated boron steel while indicate a semi‐brittle fracture for heat‐treated chromium‐molybdenum steel. Formation of a small boron carbide amount during heat treating of boron steel results in increment the bolt's tensile strength while the ductility did not changed significantly. In the other hand, formation of chromium and molybdenum carbides during heat treating of chromium‐molybdenum steel increased the bolt's tensile strength with a considerable reduction in the final ductility.Originality/valueThis paper evaluates failure analysis of HSLA wheel bolt steels and compares their microstructure before and after the loading regime.


2014 ◽  
Vol 606 ◽  
pp. 55-59 ◽  
Author(s):  
R. Senthil ◽  
A. Gnanavelbabu

Magnesium alloys are the very progressive materials whereon is due to improve their end-use properties. Especially, wrought Mg alloys attract attention since they have more advantageous mechanical properties than cast Mg alloys. Investigations were carried out the effects of heat treatment on tensile strength and microstructure of AZ61A magnesium alloy. The AZ61A Mg alloy is solution heat treated at the temperature of 6500F (343°C) for various soaking timing such as 120 min, 240 min and 360 minutes and allowed it cool slowly in the furnace itself. Magnesium alloys usually are heat treated either to improve mechanical properties or as means of conditioning for specific fabrication operations. Special attention had been focused on the analysis of mutual relations existing between the deformation conditions, microstructural parameters, grain size and the achieved mechanical properties. The result after the solution heat treatment, showed remarkably improved hardness, tensile strength and yield strength. It would be appropriate for a forming process namely isostatic forming process.


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