scholarly journals Recovery wooden beams impregnating polymer composition based on epoxy resins

2015 ◽  
Vol 5 (3) ◽  
pp. 183-190
Author(s):  
Лукина ◽  
Anastasiya Lukina ◽  
Лукин ◽  
Mikhail Lukin ◽  
Рощина ◽  
...  

This paper proposes a method of restoration of wooden structures by impregnating polymer composition based on epoxy resin, locally weakened destruction. Objective - research and development of technology for site remediation of wooden structures with areas of locally de-graded wood. We analyzed the causes of the destruction of wooden building structures. The pa-per sets out the methodology and the engineering based on the example of a wooden beam, the destruction of locally weakened in the core zone. Engineering calculations were confirmed by numerical experiments carried out in the program complex "Lira 9.6".

Author(s):  
J. G. Adams ◽  
M. M. Campbell ◽  
H. Thomas ◽  
J. J. Ghldonl

Since the introduction of epoxy resins as embedding material for electron microscopy, the list of new formulations and variations of widely accepted mixtures has grown rapidly. Described here is a resin system utilizing Maraglas 655, Dow D.E.R. 732, DDSA, and BDMA, which is a variation of the mixtures of Lockwood and Erlandson. In the development of the mixture, the Maraglas and the Dow resins were tested in 3 different volumetric proportions, 6:4, 7:3, and 8:2. Cutting qualities and characteristics of stability in the electron beam and image contrast were evaluated for these epoxy mixtures with anhydride (DDSA) to epoxy ratios of 0.4, 0.55, and 0.7. Each mixture was polymerized overnight at 60°C with 2% and 3% BDMA.Although the differences among the test resins were slight in terms of cutting ease, general tissue preservation, and stability in the beam, the 7:3 Maraglas to D.E.R. 732 ratio at an anhydride to epoxy ratio of 0.55 polymerized with 3% BDMA proved to be most consistent. The resulting plastic is relatively hard and somewhat brittle which necessitates trimming and facing the block slowly and cautiously to avoid chipping. Sections up to about 2 microns in thickness can be cut and stained with any of several light microscope stains and excellent quality light photomicrographs can be taken of such sections (Fig. 1).


Author(s):  
Georgel MIHU ◽  
Claudia Veronica UNGUREANU ◽  
Vasile BRIA ◽  
Marina BUNEA ◽  
Rodica CHIHAI PEȚU ◽  
...  

Epoxy resins have been presenting a lot of scientific and technical interests and organic modified epoxy resins have recently receiving a great deal of attention. For obtaining the composite materials with good mechanical proprieties, a large variety of organic modification agents were used. For this study gluten and gelatin had been used as modifying agents thinking that their dispersion inside the polymer could increase the polymer biocompatibility. Equal amounts of the proteins were milled together and the obtained compound was used to form 1 to 5% weight ratios organic agents modified epoxy materials. To highlight the effect of these proteins in epoxy matrix mechanical tests as three-point bending and compression were performed.


Materials ◽  
2021 ◽  
Vol 14 (9) ◽  
pp. 2205
Author(s):  
Qian Li ◽  
Yujie Li ◽  
Yifan Chen ◽  
Qiang Wu ◽  
Siqun Wang

A novel liquid phosphorous-containing flame retardant anhydride (LPFA) with low viscosity was synthesized from 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) and methyl tetrahydrophthalic anhydride (MeTHPA) and further cured with bisphenol-A epoxy resin E-51 for the preparation of the flame retardant epoxy resins. Both Fourier transform infrared spectroscopy (FT-IR), mass spectrometry (MS) and nuclear magnetic resonance (NMR) measurements revealed the successful incorporation of DOPO on the molecular chains of MeTHPA through chemical reaction. The oxygen index analysis showed that the LPFA-cured epoxy resin exhibited excellent flame retardant performance, and the corresponding limiting oxygen index (LOI) value could reach 31.2%. The UL-94V-0 rating was achieved for the flame retardant epoxy resin with the phosphorus content of 2.7%. With the addition of LPFA, the impact strength of the cured epoxy resins remained almost unchanged, but the flexural strength gradually increased. Meanwhile, all the epoxy resins showed good thermal stability. The glass transition temperature (Tg) and thermal decomposition temperature (Td) of epoxy resin cured by LPFA decreased slightly compared with that of MeTHPA-cured epoxy resin. Based on such excellent flame retardancy, low viscosity at room temperature and ease of use, LPFA showed potential as an appropriate curing agent in the field of electrical insulation materials.


2014 ◽  
Vol 1053 ◽  
pp. 263-267 ◽  
Author(s):  
Xiu Juan Tian

Thermal stability and thermal degradation kinetics of epoxy resins with 2-(Diphenylphosphinyl)-1, 4-benzenediol were investegated by thermogravimetric analysis (TGA) at different heating rates of 5 K/min, 10 K/min, 20 K/min and 40 K/min. The thermal degradation kinetic mechanism and models of the modified epoxy resins were determined by Coast Redfern method.The results showed that epoxy resins modified with the flame retardant had more thermal stability than pure epoxy resin. The solid-state decomposition mechanism of epoxy resin and the modified epoxy resin corresponded to the controlled decelerating ځ˽̈́˰̵̳͂͆ͅ˼˰̴̱̾˰̸̵̈́˰̵̸̳̱̹̽̾̓̽˰̶̳̹̾̈́̿̾̓ͅ˰̶˸ځ˹˰̵̵͇͂˰̃˸́˽ځ˹2/3. The introduction of phosphorus-containing flame retardant reduced thermal degradation rate of epoxy resins in the primary stage, and promote the formation of carbon layer.


2021 ◽  
Vol 410 ◽  
pp. 686-691
Author(s):  
Evgeniy S. Bochkarev ◽  
Dmitriy S. Vostrikov ◽  
Oleg O. Tuzhikov

The paper represents ozone resistance of rubbers based on carboxylated nitrile butadiene rubber cured with epoxy resins and magnesium oxide. Ozone resistance was investigated using the express-method at a flow rate of the ozone-air mixture of 9 l/h and ozone content of 9 mg/l. In the method used, the “time to cracking start” indicator was taken as the basic indicator of ozone resistance. The second indicator characterizing the ozone resistance of elastomeric materials was the "rate of destruction" in the main period of destruction. There has been evaluated the effect of dissolved polyvinyl chloride in epoxy resin ED-20 on the properties of vulcanizates. There has been investigated the Increase in destruction time under the action of ozone.


2012 ◽  
Vol 263-266 ◽  
pp. 1304-1309
Author(s):  
Jia Si Wang ◽  
Ying Zhang ◽  
Di Ming Ai ◽  
Feng Pan

The micro-Extended-Analog-Computater(uEAC) is a newly emergent unconventional computing model under research and development. Although, a single uEAC unit can achieve some classic pattern classification problem, the slop of the classification face generated by uEAC is a constant and moves parallely. So a feedforward array structure is proposed for the improvement of uEAC, and Particle Swarm Optimizer(PSO) is utilized to configure the uEAC array. The analysis of the mapping characteristics and numerical experiments both illustrate the effectiveness of the improvement.


Author(s):  
M.A. Serekpayeva ◽  
◽  
G.А. Kokayeva ◽  
R.K. Niyazbekova ◽  
S. Kardybai ◽  
...  

The outcomes of studying epoxy-based composite materials supplemented with microsilica are provided in the article. Microsilica was used as a filler. The samples were produced on the epoxy ED-20 basis supplemented with 2, 5 and 10 mas. % of microsilica. The structure and size of finely dispersed filler particles were defined. The obtained composites were tested for resistance to the effect of variable temperatures, corrosive, and abrasion. The study outcomes proved that samples supplemented with 2% of microsilica are more resistant to acid and alkali as well as to petrol than those ones supplemented with 25% of microsilica. Besides the amount of the filler from 2 to 10% doesn’t sufficiently affect the resistance to variable temperatures. When microsilica is added to epoxy resin, it causes scuff resistance increase. The conducted testing proved that the developed composite materials are resistant to the effect of variable temperatures, corrosive, and abrasion. This enables to use these materials as coatings and anti-corrosion protection during machine maintenance.


2021 ◽  
Vol 17 ◽  
pp. 55-67
Author(s):  
Aija Grietena

In the search for balancing factors in the art of environmental design between architecture, landscape architecture, and interiors needed to improve interdisciplinary collaborative planning and enhance the psycho-emotional quality of the environment, the study of landscape space-indoor interaction through comparative analysis and inductive reference is continued. On the Latvian scale, the new, 21st-century technological capabilities in the design and production of wooden structures in the architecture of the open air concert hall “Mītava”, constructed in 2019 on Pasta Island. The importance of the structure on the Baltic scale is emphasized by the unique design, which resembles a shell washed on the bank of the Lielupe River, large (<60m) arched timber continuous roof structures and high acoustic characteristics. Original building structures have opened up new opportunities for interaction between landscape space and indoor space, creating a broad, spatial synthesis. The realization of an artistically stylistic concept in the open-air concert hall “Mītava”, which is subordinated to the existing landscape space and supplemented with appropriate greenery, is considered a valuable contribution to the urban environment. The specific case study analyzed in detail underlines the importance of successful interdisciplinary collaboration in the harmonious interaction between landscape space and indoor.


Author(s):  
J. Murray Wilson

Epoxy resins are not just replacements for concrete and cement grouts, they offer the opportunity for completely new foundation/gas turbine interface designs. As a substitute for steel chocks, epoxy resin ones give perfect fit, high holding force and good thermal insulation, while eliminating the need for soleplates or rails.


2021 ◽  
Author(s):  
Heba Mansour ◽  
Ahmed M.R. Fath El-Bab ◽  
Emad A. Soliman ◽  
Ahmed L. Abdel-Mawgood

Abstract Microfluidic devices are a rising technology to automatize chemical and biological operations. In this context, laser ablation has significant potential for polymer-based microfluidic platforms' fast and economical manufacturing. Nevertheless, the manufacturing of epoxy-based microfluidic chips is considered highly cost full due to demand for cleanroom facilities that utilize expensive equipment and lengthy processes. Therefore, this study targeted investigating the feasibility of epoxy resins to be fabricated as a lab-on-chip using carbon dioxide laser ablation. The chemical structural properties and thermal stability of the plain epoxy resins were characterized by Fourier transform infrared spectral analysis (FT-IR) and thermogravimetric analysis (TGA). Moreover, a specific migration test was performed to quantify potential migrants by gas chromatography coupled to mass spectrometry (GC-MS) to prove that the cured epoxy resin would not release unreacted monomers to the biological solution test, which caused inhibition of the sensitive biological reactions. By investigating the impact of this process on microchannels' dimensions and quality, a laser technique using CO2 laser was used in vector mode to engrave into a transparent epoxy resin chip. The resulting microchannels were characterized using 3D Laser microscopy. The outcomes of this study showed considerable potential for laser ablation in machining the epoxy-based chips, whereas the microchannels were produced with minor bulges' height (0.027 µm) with no clogging. Moreover, a reasonable depth of 99.31 µm with roughness (Ra) of 14.52 µm was obtained at a laser speed of 5 mm/s and laser power of 1.8 W. This process can produce epoxy resin-based microfluidic chips without the need for cleanroom facilities that require expensive equipment and lengthy process.


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