Effect of Ag additions on the microstructure and phase transformations of Zn-22Al-2Cu (wt.%) alloy

Author(s):  
Carlos Ferreira-Palma ◽  
Héctor J. Dorantes-Rosales ◽  
Víctor M. López-Hirata ◽  
Alberto A. Torres-Castillo

Abstract The relationship between microstructure and mechanical properties is studied for eutectoid Zn-22Al (wt.%) alloys modified with Cu and Ag. Three alloys with a Cu content of 2 wt.% and varying amounts of Ag were cast and hot-extruded. Different microstructural characteristics were induced by heat treatments: natural aging, artificial aging and furnace cooling. Structural and microstructural characterizations were carried out with X-ray diffraction and scanning electron microscopy. Mechanical properties were determined by tensile testing. Dilatometry was used for determining the effects of composition on the transformation points. The addition of Ag increased the ε phase fraction and provided solid solution strengthening, improving the mechanical strength and reducing ductility. Ag additions also displaced the eutectoid reaction to higher temperatures. The microstructure of the matrix has proven to have a strong impact on mechanical properties. The naturally aged specimens presented the highest ductility and tensile strength; however, these properties are severely affected by aging. Lamellar microstructures present the lowest ductility and values of tensile strength between those of the natural and artificially-aged specimens.

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 548 ◽  
Author(s):  
Leonid Agureev ◽  
Valeriy Kostikov ◽  
Zhanna Eremeeva ◽  
Svetlana Savushkina ◽  
Boris Ivanov ◽  
...  

The article presents the study of alumina nanoparticles’ (nanofibers) concentration effect on the strength properties of pure nickel. The samples were obtained by spark plasma sintering of previously mechanically activated metal powders. The dependence of the grain size and the relative density of compacts on the number of nanofibers was investigated. It was found that with an increase in the concentration of nanofibers, the average size of the matrix particles decreased. The effects of the nanoparticle concentration (0.01–0.1 wt.%) on the elastic modulus and tensile strength were determined for materials at 25 °C, 400 °C, and 750 °C. It was shown that with an increase in the concentration of nanofibers, a 10–40% increase in the elastic modulus and ultimate tensile strength occurred. A comparison of the mechanical properties of nickel in a wide range of temperatures, obtained in this work with materials made by various technologies, is carried out. A description of nanofibers’ mechanisms of influence on the structure and mechanical properties of nickel is given. The possible impact of impurity phases on the properties of nickel is estimated. The tendency of changes in the mechanical properties of nickel, depending on the concentration of nanofibers, is shown.


2005 ◽  
Vol 475-479 ◽  
pp. 317-320 ◽  
Author(s):  
Jing Pei Xie ◽  
Ji Wen Li ◽  
Zhong Xia Liu ◽  
Ai Qin Wang ◽  
Yong Gang Weng ◽  
...  

The in-situ Ti alloying of aluminium alloys was fulfilled by electrolysis, and the material was made into A356 alloy and used in automobile wheels. The results show that the grains of the A356 alloy was refined and the second dendrites arm was shortened due to the in-situ Ti alloying. Trough 3-hour solution treatment and 2-hour aging treatment for the A356 alloy, the microstructures were homogeneous, and Si particles were spheroid and distribute in the matrix fully. The outstanding mechanical properties with tensile strength (σb≥300Mpa) and elongation values (δ≥10%) have been obtained because the heat treatment was optimized. Compared with the traditional materials, tensile strength and elongation were increased by 7.6~14.1% and 7.4~44.3% respectively. The qualities of the automobile wheels were improved remarkably.


2014 ◽  
Vol 2014 ◽  
pp. 1-10 ◽  
Author(s):  
Fakhim Babak ◽  
Hassani Abolfazl ◽  
Rashidi Alimorad ◽  
Ghodousi Parviz

We investigate the performance of graphene oxide (GO) in improving mechanical properties of cement composites. A polycarboxylate superplasticizer was used to improve the dispersion of GO flakes in the cement. The mechanical strength of graphene-cement nanocomposites containing 0.1–2 wt% GO and 0.5 wt% superplasticizer was measured and compared with that of cement prepared without GO. We found that the tensile strength of the cement mortar increased with GO content, reaching 1.5%, a 48% increase in tensile strength. Ultra high-resolution field emission scanning electron microscopy (FE-SEM) used to observe the fracture surface of samples containing 1.5 wt% GO indicated that the nano-GO flakes were well dispersed in the matrix, and no aggregates were observed. FE-SEM observation also revealed good bonding between the GO surfaces and the surrounding cement matrix. In addition, XRD diffraction data showed growth of the calcium silicate hydrates (C-S-H) gels in GO cement mortar compared with the normal cement mortar.


Author(s):  
S C Sharma

A well-consolidated composite of Al alloy 6061 reinforced with 4, 8 and 12 wt% garnet was prepared by a liquid metallurgy technique, the composite was heat treated for different ageing durations (T6 treatment), and its mechanical properties were determined by destructive testing. The results of the study indicated that, as the garnet particle content in the composites increased, there were marked increases in the ultimate tensile strength, compressive strength and hardness but there was a decrease in the ductility. There was an improvement in the tensile strength, compressive strength, and hardness with ageing due to precipitation. Precipitation in Al alloy 6061, with and without garnet particulate reinforcement, was studied using transmission electron microscopy. The fracture behaviour of the composites was altered significantly by the presence of garnet particles and the crack propagation through the matrix, and the reinforcing particle clusters resulted in final fracture.


2019 ◽  
Vol 3 (1) ◽  
Author(s):  
Catur Pramono ◽  
Sri Widodo ◽  
Muhammad Galih Ardiyanto

Composite is a material consisting of two or more components which have characteristics mild and relatively strong. This study used bagasse fiber which is widely produced in sugar industry. Treatment of bagasse fiber by soaked in alkaline solution (NaOH) for 2 hours to remove the cork / wax attached to the fiber. Manufacture of composite by hand lay up. The matrix used in this study is epoxy. The fraction volume of composite between bagasse fiber and epoxy are 4%: 96%, 8%: 92% and 12%: 88%. The mechanical properties tested is tensile strength. The tensile test refers to ASTM D638 type 4. The highest tensile test composite resulted at the fraction volume composite of bagasse fiber with epoxy 12%: 88% i.e. 28.43 MPa.


2010 ◽  
Vol 667-669 ◽  
pp. 457-461
Author(s):  
Wei Guo ◽  
Qu Dong Wang ◽  
Man Ping Liu ◽  
Tao Peng ◽  
Xin Tao Liu ◽  
...  

Cyclic channel die compression (CCDC) of AZ31-1.7 wt.% Si alloy was performed up to 5 passes at 623 K in order to investigate the microstructure and mechanical properties of compressed alloys. The results show that multi-pass CCDC is very effective to refine the matrix grain and Mg2Si phases. After the alloy is processed for 5 passes, the mean grain size decreases from 300 μm of as-cast to 8 μm. Both dendritic and Chinese script type Mg2Si phases break into small polygonal pieces and distribute uniformly in the matrix. The tensile strength increases prominently from 118 MPa to 216 MPa, whereas the hardness of alloy deformed 5 passes only increase by 8.4% compared with as-cast state.


2013 ◽  
Vol 681 ◽  
pp. 256-259
Author(s):  
Xiu Qi Liu ◽  
He Qin Xing ◽  
Li Li Zhao ◽  
Dan Wang

In our study, a new kind of foam composite was prepared by melt blending with PVC as the matrix and carbon black (CB) as the filler, the standard-spline was made in the dumbbell system prototype. Tensile strength and elongation at break were measured at 25°C。When the CB was added greater than 2.0%, with the increase of CB added, the determination of sample mechanical index began to decline, when the CB content was greater than 9%, tensile strength and elongation at break of the composites remained basically unchanged.


2018 ◽  
Vol 941 ◽  
pp. 224-229
Author(s):  
Takahiro Izumi ◽  
Tatsuya Kobayashi ◽  
Ikuo Shohji ◽  
Hiroaki Miyanaga

Microstructures and mechanical properties of lap fillet welded joints of several high and ultra-high tensile strength steel by arc welding were investigated. Steel plates having tensile strength of 400 (SPH400W), 590 (SPC590Y, SPC590R), 980 (SPC980Y) and 1500 MPa (SAC1500HP) class with 2 mm thickness were prepared. Four types of joints were formed by MAG welding; SPH400W/SPH400W, SPC590Y/SPC590Y, SPC980Y/SPC980Y and SAC1500HP/SPC590R. In joints with SPC590Y, SPC980Y and SAC1500HP steel which matrixes are martensitic microstructures, the HAZ softens due to transformation of martensite into ferrite with precipitating cementite. By using high and ultra-high tensile strength steel, the weld metal is strengthened due to dilution of the matrix into the weld metal and thus tensile shear strength of the welded joint increases. In the fatigue test, similar S-N diagrams were obtained in the all welded joints investigated. It seems that the effect of stress concentration due to the shape of the welded joint on fatigue properties is larger than that of the strength of the matrix.


2019 ◽  
Vol 130 ◽  
pp. 01005
Author(s):  
Cindy Retno Putri ◽  
Anne Zulfia Syahrial ◽  
Salahuddin Yunus ◽  
Budi Wahyu Utomo

The goal of this research is to improve the mechanical properties such as strength, hardness and wear resistance for automotive application such as brake shoe and bearings due to high cycle, load and impact during their usage. Therefore, another alloying element or reinforcement addition is necessary. In this work, the composites are made by ADC 12 (Al-Si aluminum alloy) as the matrix and reinforced with micro SiC through stir casting process and TiB is added various from (0.04, 0.06, 0.15, 0.3 and 0.5) wt.% that act as grain refiners and 5 wt.% of Mg is added to improve the wettability of the composites. The addition of TiB improves the mechanical properties because the grain becomes finer and uniform, and the addition of Mg makes the matrix and reinforce have better adhesion. The results obtained that the optimum composition was found by adding 0.15 wt.% of TiB with tensile strength improve from 98 MPa to 136.3 MPa, hardness from 35 to 53 HRB and wear rate reduced from 0.006 2 mm3 s−1 to 0.002 3 mm3 s−1 respectively.


2020 ◽  
pp. 096739112097118
Author(s):  
Mustafa Taşyürek

In this study, process parameters and mechanical properties of the multi-scale composite were investigated experimentally and predictably. Multi-scale material includes boron carbide particles and multi walled carbon nanotubes (MWCNTs) in the epoxy-based matrix. Both reinforcements were reinforced into the matrix with various rates simultaneously. Average three tensile strength and hardness values were determined. The tensile strength and hardness were enhanced thanks to high rate of B4C usage up to 54.09% and 2.54%, respectively. The microstructure of the hybrid composite was investigated by Scanning Electron Microscopy. Also, Fourier Transform Infrared Spectroscopy was used to interpret spectral bands. The experimental data were analyzed using optimization method. Optimal process parameters for tensile strength and interfacial properties were determined. The Analysis of Variance (ANOVA) was used to obtain most significant factor and optimum levels of parameters. Finally, it was observed that B4C ratio is the most dominant factor affecting the mechanical and thermal properties.


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