Influence of nozzle temperature and volumetric filling on the mechanical properties of 3D-printed PEEK

2020 ◽  
Vol 62 (4) ◽  
pp. 351-356
Author(s):  
Danny Vogel ◽  
Volker Weißmann ◽  
Leo Rührmund ◽  
Harald Hansmann ◽  
Rainer Bader
Keyword(s):  
Mechanical Properties ◽  
Fused Deposition Modeling ◽  
Bending Strength ◽  
Layer By Layer ◽  
Bending Properties ◽  
Filling Degree ◽  
Fused Deposition ◽  
3D Printed ◽  
Injection Molded ◽  
Nozzle Temperature

Abstract Fused deposition modeling is a layer-by-layer 3D printing technology used to additively manufacture polymers. A major benefit of 3D-printed polymers is the option of tailoring their mechanical properties by varying the process parameters. In addition, the present study investigates the influence of the filling degree (50 % or 100 %) and the nozzle temperature during manufacturing on the mechanical properties of 3D-printed poly-ether-ether-ketone (PEEK) material. PEEK samples were built either compact (filling degree 100 %) or closed-cell porous (filling degree 50 %), using three different nozzle temperatures (390 °C, 430 °C and 470 °C). In static bending tests, the bending properties were evaluated and compared with injection molded PEEK samples. Bending strength and modulus increased up to 21.1 %, when the nozzle temperature was increased and up to 40.8 % when the volumetric filling was altered. The results indicate that nozzle temperature and volumetric filling can be altered to tailor the bending properties of 3D-printed PEEK for particular applications. However, the mechanical properties of the 3D-printed samples determined in the current study could not achieve those of the properties of the injection molded PEEK.

Physical property of 3D-printed sinusoidal pattern using shape memory TPU filament

2020 ◽  
Vol 90 (21-22) ◽  
pp. 2399-2410 ◽  
Author(s):  
Shahbaj Kabir ◽  
Hyelim Kim ◽  
Sunhee Lee
Keyword(s):  
Mechanical Properties ◽  
Tensile Test ◽  
Shape Memory ◽  
Fused Deposition Modeling ◽  
Loss Modulus ◽  
Thermoplastic Polyurethane ◽  
Heating Process ◽  
Fused Deposition ◽  
3D Printed ◽  
Sinusoidal Pattern

This study has investigated the physical properties of 3D-printable shape memory thermoplastic polyurethane (SMTPU) filament and its 3D-printed sinusoidal pattern obtained by fused deposition modeling (FDM) technology. To investigate 3D filaments, thermoplastic polyurethane (TPU) and SMTPU filament were examined by conducting infrared spectroscopy, x-ray diffraction (XRD), dynamic mechanical thermal analysis (DMTA), differential scanning calorimetry (DSC) and a tensile test. Then, to examine the 3D-printed sinusoidal samples, a sinusoidal pattern was developed and 3D-printed. Those samples went through a three-step heating process: (a) untreated state; (b) 5 min heating at 70°C, cooling for 30 min at room temperature; and (c) a repeat of step 2. The results obtained by the three different heating processes of the 3D-printed sinusoidal samples were examined by XRD, DMTA, DSC and the tensile test to obtain the effect of heating or annealing on the structural and mechanical properties. The results show significant changes in structure, crystallinity and thermal and mechanical properties of SMTPU 3D-printed samples due to the heating steps. XRD showed the increase in crystallinity with heating. In DMTA, storage modulus, loss modulus and the tan σ peak position also changed for various heating steps. The DSC result showed that the Tg for different steps of the SMTPU 3D-printed sample remained almost the same at around 51°C. The tensile property of the TPU 3D-printed sinusoidal sample decreased in terms of both load and elongation with increased heating processes, while for the SMTPU 3D-printed sinusoidal sample, the load decreased but elongation increased about 2.5 times.

Assessing the effect of FDM processing parameters on mechanical properties of PLA parts using Taguchi method

2021 ◽  
pp. 089270572110530
Author(s):  
Nagarjuna Maguluri ◽  
Gamini Suresh ◽  
K Venkata Rao
Keyword(s):  
Mechanical Properties ◽  
Tensile Properties ◽  
Fused Deposition Modeling ◽  
Fracture Strain ◽  
Processing Parameters ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Nozzle Temperature ◽  
Experimental Runs ◽  
Printing Speed

Fused deposition modeling (FDM) is a fast-expanding additive manufacturing technique for fabricating various polymer components in engineering and medical applications. The mechanical properties of components printed with the FDM method are influenced by several process parameters. In the current work, the influence of nozzle temperature, infill density, and printing speed on the tensile properties of specimens printed using polylactic acid (PLA) filament was investigated. With an objective to achieve better tensile properties including elastic modulus, tensile strength, and fracture strain; Taguchi L8 array has been used for framing experimental runs, and eight experiments were conducted. The results demonstrate that the nozzle temperature significantly influences the tensile properties of the FDM printed PLA products followed by infill density. The optimum processing parameters were determined for the FDM printed PLA material at a nozzle temperature of 220°C, infill density of 100%, and printing speed of 20 mm/s.

scholarly journals Effect of Porosity on Mechanical Properties of 3D Printed Polymers: Experiments and Micromechanical Modeling Based on X-Ray Computed Tomography Analysis

Polymers ◽  
2019 ◽  
Vol 11 (7) ◽  
pp. 1154 ◽  
Author(s):  
Wang ◽  
Zhao ◽  
Fuh ◽  
Lee
Keyword(s):  
Computed Tomography ◽  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Fused Deposition Modeling ◽  
Micromechanical Model ◽  
Micromechanical Modeling ◽  
X Ray ◽  
Fused Deposition ◽  
3D Printed ◽  
X Ray Computed

Additive manufacturing (commonly known as 3D printing) is defined as a family of technologies that deposit and consolidate materials to create a 3D object as opposed to subtractive manufacturing methodologies. Fused deposition modeling (FDM), one of the most popular additive manufacturing techniques, has demonstrated extensive applications in various industries such as medical prosthetics, automotive, and aeronautics. As a thermal process, FDM may introduce internal voids and pores into the fabricated thermoplastics, giving rise to potential reduction on the mechanical properties. This paper aims to investigate the effects of the microscopic pores on the mechanical properties of material fabricated by the FDM process via experiments and micromechanical modeling. More specifically, the three-dimensional microscopic details of the internal pores, such as size, shape, density, and spatial location were quantitatively characterized by X-ray computed tomography (XCT) and, subsequently, experiments were conducted to characterize the mechanical properties of the material. Based on the microscopic details of the pores characterized by XCT, a micromechanical model was proposed to predict the mechanical properties of the material as a function of the porosity (ratio of total volume of the pores over total volume of the material). The prediction results of the mechanical properties were found to be in agreement with the experimental data as well as the existing works. The proposed micromechanical model allows the future designers to predict the elastic properties of the 3D printed material based on the porosity from XCT results. This provides a possibility of saving the experimental cost on destructive testing.

scholarly journals EFFECT OF EXTRUSION PROCESS PARAMETERS ON MECHANICAL PROPERTIES OF 3D PRINTED PLA PRODUCT

2021 ◽  
Vol 6 (2) ◽  
pp. 119
Author(s):  
Nanang Ali Sutisna ◽  
Rakha Amrillah Fattah
Keyword(s):  
Mechanical Properties ◽  
Additive Manufacturing ◽  
Fused Deposition Modeling ◽  
Extrusion Process ◽  
Experimental Procedure ◽  
Fused Deposition ◽  
Novel Approach ◽  
Deposition Modeling ◽  
3D Printed ◽  
3D Digital Models

The method of producing items through synchronously depositing material level by level, based on 3D digital models, is named Additive Manufacturing (AM) or 3D-printing. Amongs many AM methods, the Fused Deposition Modeling (FDM) technique along with PLA (Polylactic acid) material is commonly used in additive manufacturing. Until now, the mechanical properties of the AM components could not be calculated or estimated until they've been assembled and checked. In this work, a novel approach is suggested as to how the extrusion process affects the mechanical properties of the printed component to obtain how the parts can be manufactured or printed to achieve improved mechanical properties. This methodology is based on an experimental procedure in which the combination of parameters to achieve an optimal from a manufacturing experiment and its value can be determined, the results obtained show the effect of the extrusion process affects the mechanical properties.

Deposition-induced effects of isotactic polypropylene and polycarbonate composites during fused deposition modeling

2017 ◽  
Vol 23 (5) ◽  
pp. 869-880 ◽  
Author(s):  
Ying-Guo Zhou ◽  
Bei Su ◽  
Lih-sheng Turng
Keyword(s):  
Mechanical Properties ◽  
Design Methodology ◽  
Fused Deposition Modeling ◽  
Content Type ◽  
Fused Deposition ◽  
Close Relationship ◽  
Molded Parts ◽  
Deposition Modeling ◽  
Injection Molded ◽  
First Time

Purpose Although the feasibility and effectiveness of the fused deposition modeling (FDM) method have been proposed and developed, studies of applying this technology to various materials are still needed for researching its applicability, especially with regard to polymer blends and composites. The purpose of this paper is to study the deposition-induced effect and the effect of compatibilizers on the mechanical properties of polypropylene and polycarbonate (PP/PC) composites. Design/methodology/approach For this purpose, three different deposition modes for PP/PC composites with or without compatibilizers were used for the FDM method and tested for tensile properties. Also, parts with the same materials were made by injection molding and used for comparison. In addition, different deposition speeds were used to investigate the different deposition-induced effects. Furthermore, the behavior of the mechanical properties was clarified with scanning electron microscope images of the fracture surfaces. Findings The research results suggest that the deposition orientation has a significant influence on the mechanical behavior of PP/PC composite FDM parts. The results also indicate that there is a close relationship between the mechanical properties and morphological structures which are deeply influenced by compatibilization. Compared with injection molded parts, the ductility of the FDM parts can be dramatically improved due to the formation of fibrils and micro-fibrils by the deposition induced during processing. Originality/value This is the first paper to investigate a PP/PC composite FDM process. The results of this paper verified the applicability of PP/PC composites to FDM technology. It is also the first time that the deposition-induced effect during FDM has been investigated and studied.

scholarly journals 3D-Printable PP/SEBS Thermoplastic Elastomeric Blends: Preparation and Properties

Polymers ◽  
2019 ◽  
Vol 11 (2) ◽  
pp. 347 ◽  
Author(s):  
Shib Banerjee ◽  
Stephen Burbine ◽  
Nischay Kodihalli Shivaprakash ◽  
Joey Mead
Keyword(s):  
3D Printing ◽  
Carbon Black ◽  
Computer Aided Design ◽  
Fused Deposition Modeling ◽  
Mechanical Performance ◽  
Polymeric Materials ◽  
Fused Deposition ◽  
3D Printed ◽  
Injection Molded ◽  
Preferential Location

Currently, material extrusion 3D printing (ME3DP) based on fused deposition modeling (FDM) is considered a highly adaptable and efficient additive manufacturing technique to develop components with complex geometries using computer-aided design. While the 3D printing process for a number of thermoplastic materials using FDM technology has been well demonstrated, there still exists a significant challenge to develop new polymeric materials compatible with ME3DP. The present work reports the development of ME3DP compatible thermoplastic elastomeric (TPE) materials from polypropylene (PP) and styrene-(ethylene-butylene)-styrene (SEBS) block copolymers using a straightforward blending approach, which enables the creation of tailorable materials. Properties of the 3D printed TPEs were compared with traditional injection molded samples. The tensile strength and Young’s modulus of the 3D printed sample were lower than the injection molded samples. However, no significant differences could be found in the melt rheological properties at higher frequency ranges or in the dynamic mechanical behavior. The phase morphologies of the 3D printed and injection molded TPEs were correlated with their respective properties. Reinforcing carbon black was used to increase the mechanical performance of the 3D printed TPE, and the balancing of thermoplastic elastomeric and mechanical properties were achieved at a lower carbon black loading. The preferential location of carbon black in the blend phases was theoretically predicted from wetting parameters. This study was made in order to get an insight to the relationship between morphology and properties of the ME3DP compatible PP/SEBS blends.

Influence of Built Orientation on Mechanical Properties in Fused Deposition Modeling

2014 ◽  
Vol 592-594 ◽  
pp. 400-404 ◽  
Author(s):  
Sandeep V. Raut ◽  
Vijaykumar S. Jatti ◽  
T.P. Singh
Keyword(s):  
Mechanical Properties ◽  
Rapid Prototyping ◽  
Fused Deposition Modeling ◽  
Polymer Materials ◽  
Manufacturing Cost ◽  
Layer By Layer ◽  
Total Cost ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
Main Material

Fused deposition modeling (FDM) is one of the thirty techniques of rapid prototyping methods that produce prototypes from polymer materials (natural or with different grades). Acrylonitrile butadiene styrene (ABS) is one of the good material among all polymer materials. It is used in the layer by layer manufacturing of the prototype which is in the semi-molten plastic filament form and built up on the platform from bottom to top. In FDM, one of the critical factor is to select the built up orientation of the model since it affects the different areas of the model like main material, support material, built up time, total cost per part and most important the mechanical properties of the part. In view of this, objective of the present study was to investigate the effect of the built-up orientation on the mechanical properties and total cost of the FDM parts. Experiments were carried out on STRATASYS FDM type rapid prototyping machine coupled with CATALYST software and ABS as main material. Tensile and Impact specimens were prepared as per the ASTM standard with different built-up orientation and in three geometrical axes. It can be concluded from the experimental analysis that built orientation has significant affect on the tensile, impact and total cost of the FDM parts. These conclusions will help the design engineers to decide on proper build orientation, so that FDM parts can be fabricated with good mechanical properties at minimum manufacturing cost.

FDM Prototype Experimental Research of Processing Parameter Optimization to Achieve Higher Tensile Stress

2015 ◽  
Vol 220-221 ◽  
pp. 767-773 ◽  
Author(s):  
Ilmars Brensons ◽  
Svetlana Polukoshko ◽  
Andris Silins ◽  
Natalija Mozga
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Epoxy Resin ◽  
Fused Deposition Modeling ◽  
Low Cost ◽  
Rapid Prototype ◽  
Layer By Layer ◽  
Processing Parameter ◽  
Practical Applications ◽  
Fused Deposition

Fused Deposition Modeling (FDM) is one of most common ways of rapidly producing a part. Heated material (most commonly – plastic) is used to extrude it through a nozzle and deposit on a surface layer by layer until the part is fully produced. FDM has become one of the most popular in rapid production area due to its low cost, available materials and versatility.Due to fact that part is made layer by layer and each additional layer is deposited on top of a layer that is already a little below material melting point, part maintains different mechanical properties in various directions. These varying mechanical properties affect the part usability in practical applications. Critical point is tensile strength.The objective of this paper is to research optimal processing parameters for FDM prototyping to improve tensile strength. Several rapid prototype models (tensile test samples) with various geometry of longitudinal reinforcement channels were built. As reinforcing material, the epoxy resin was used, because it has higher tensile strength when solid and allows filling channels with various geometry. All made samples were tested for tensile strength. Experiment was carried out to confirm the effectiveness of this approach. From the results, it is found how different amount of epoxy resin affects part tensile strength.

scholarly journals Polymer Composites Used in Rapid Prototyping Technology

2020 ◽  
Vol 44 (1) ◽  
pp. 15-20
Author(s):  
Katarzyna Bulanda ◽  
Mariusz Oleksy ◽  
Rafał Oliwa ◽  
Grzegorz Budzik ◽  
Tadeusz Markowski
Keyword(s):  
Mechanical Properties ◽  
3D Printing ◽  
Fused Deposition Modeling ◽  
New Materials ◽  
Fused Deposition ◽  
The Matrix ◽  
Molded Parts ◽  
Deposition Modeling ◽  
Injection Molded ◽  
The Impact

AbstractNew materials and filaments dedicated to 3D printing were obtained using the fused deposition modeling method, and the properties of the produced materials were investigated. Polylactide was used as a polymer base for the assays because of the desired properties of the polymer, mainly biodegradability, and the matrix was refilled by the addition of metallic nanofillers, such as bronze, copper, brass, and steel. For the composites obtained, mechanical properties were investigated to determine the dependence of the obtained results on the content and type of filler used and on the method of fabrication of the fittings. It was found that the additives present in the polymer matrix increased the fluidity of the material. The best results were obtained for the compositions with bronze and steel in which the mass flow rate was 72.97 and 79.99 g/10 min, respectively. The filled material that had lower hardness was measured by Rockwell and the impact strength was measured by Charpy. In addition, it was found that injection-molded parts obtained much better mechanical properties than those obtained by 3D printing.

scholarly journals The Effects of Combined Infill Patterns on Mechanical Properties in FDM Process

Polymers ◽  
2020 ◽  
Vol 12 (12) ◽  
pp. 2792
Author(s):  
Mohammadreza Lalegani Dezaki ◽  
Mohd Khairol Anuar Mohd Ariffin
Keyword(s):  
Mechanical Properties ◽  
Computer Aided Design ◽  
Fused Deposition Modeling ◽  
Strength Analysis ◽  
Element Analysis ◽  
Fused Deposition ◽  
Deposition Modeling ◽  
3D Printed ◽  
Complex Features ◽  
Aided Design

Fused deposition modeling (FDM) is commonly used to print different products with highly complex features. Process parameters for FDM are divided into controllable or uncontrollable parameters. The most critical ones are built orientation, layer thickness, infill pattern, infill density, and nozzle diameter. This study investigates the effects of combined infill patterns in 3D printed products. Five patterns (solid, honeycomb, wiggle, grid, and rectilinear) were combined in samples to analyze their effects on mechanical properties for tensile strength analysis. Polylactic acid (PLA) samples were printed in different build orientations through two directions: flat and on-edge. The limitation was that the software and machine could not combine the infill patterns. Thus, the patterns were designed and assembled in computer aided design (CAD) software. Finite element analysis (FEA) was used to determine the patterns’ features and results showed honeycomb and grid have the highest strength while their weights were lighter compared to solid. Moreover, 0° samples in both flat and on-edge direction had the strongest layer adhesion and the best quality. In contrast, perpendicular samples like 60° and 75° showed poor adhesion and were the weakest specimens in both flat and on-edge, respectively. In brief, by increasing the build orientation, the strength decreases in this study.

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