scholarly journals Green Synthesis Nanoparticle ZnO Sargassum sp. Extract and The Products Charactheristic

2017 ◽  
Vol 20 (2) ◽  
pp. 238 ◽  
Author(s):  
Rodiah Nurbaya Sari ◽  
N. Nurhasni ◽  
M. Ainul Yaqin
Keyword(s):  
Particle Size ◽  
Green Synthesis ◽  
Calcination Temperature ◽  
Zno Nanoparticles ◽  
Food Packaging ◽  
Xrd Analysis ◽  
Research Area ◽  
Zinc Nitrate ◽  
Wide Range ◽  
Size Of Particles

The synthesis of zinc oxide (ZnO) nanoparticles is an emerging research area due to its wide range of applications, such as electronics, pharmaceuticals, optics and food packaging. In this study, described <br />the green synthesis of ZnO nanoparticles and their characteristics using Sargassum sp. extract and 0.1 M zinc nitrate as the precursors. The variations include Sargassum sp. extracts volume of 5, 10, and 20<br />mL and the calcination temperature of 400, 500, and 600 oC. The characterization had been done such as the role of Sargassum sp. extract as a reducing agent for Zn2+ → Zn0 confirmed by Fourier Transform <br />Infrared Spectroscopy (FTIR) spectra due to 450-4000 cm-1 wavelength, the size of particles using Particle Size Analyzer (PSA), image and chemical composition using Scanning Electron Microscopy with X-ray microanalysis (SEM-EDS) and crystallinity using ray powder diffraction (XRD) with Cu anode at 1.54187 Å. Analysis with PSA instrument showed that ZnO particle size increased from 607 up to 649 nm along with increasing of extract concentration from 5 up to 20% (v/v). SEM imaging showed the formation of ZnO to be predominantly spherical and EDS data confirmed the existence of zinc and oxygen in the particles obtained. XRD analysis revealed hexagonal crystal system of ZnO nanoparticles and decreased in crystallite size was observed from 31.4 to 14.7 nm with increased in calcination temperature from 400 to 600 oC.

scholarly journals Synthesis of ZnO and CuO nanoparticles via Sol gel method and Its Characterization by using XRD and FT-IR Analysis

2022 ◽  
Author(s):  
Monika Patel ◽  
Sunita Mishra ◽  
Ruchi Verma ◽  
Deep Shikha
Keyword(s):  
Particle Size ◽  
Zno Nanoparticles ◽  
Sol Gel ◽  
Broad Band ◽  
Zinc Nitrate ◽  
Zno Nanoparticle ◽  
Absorption Bands ◽  
Characteristic Absorption ◽  
Sol Gel Process ◽  
Ft Ir

Abstract Nanotechnology is a completely unique branch of technology that offers with substances in a very small size between (1-100 nm) with various crystal shapes which include spherical nanoparticles, flower shaped, Nano rods, Nano ribbons, and Nano platelets. Metals have ability to produce large number of oxides. These metal oxides play an major role in many areas of chemistry, physics, material science and food science. In this research, Zinc Oxide (ZnO) and Copper (II) oxide nanoparticles were synthesized via sol-gel process using zinc nitrate and copper (II) nitrate as precursor respectively. The characterization of CuO and ZnO nanoparticles was done by using various techniques. X-ray Diffraction (XRD) indicates the crystallinity and crystal size of CuO and ZnO nanoparticle. Fourier transform infrared spectroscopy (FT-IR) was used to get the infrared spectrum of the sample indicating composition of the sample which contains various functional groups. XRD result shows the particle size of CuO at highest peak 29.40140 was 61.25 nm and the particle size of ZnO at highest peak 36.24760 was 21.82 nm. FT-IR spectra peak at 594.56 cm-1 indicated characteristic absorption bands of ZnO nanoparticles and the broad band peak at 3506.9 cm-1 can be attributed to the characteristic absorption of O-H group. The analysis of FT-IR spectrum of CuO shows peaks at 602.09, 678.39, and 730.19cm−1 which refer to the formation of CuO. A broad absorption peak noticed at 3308.2 cm−1 attributed to O–H stretching of the moisture content.

Role of ZnO Nanoparticles for improvement of Antibacterial Activity in Food Packaging

2021 ◽  
pp. 128-131
Author(s):  
Saira Sehar ◽  
Amiza Amiza ◽  
I. H Khan
Keyword(s):  
Antimicrobial Activity ◽  
Particle Size ◽  
Surface Area ◽  
Zno Nanoparticles ◽  
Food Packaging ◽  
Antimicrobial Agents ◽  
Uv Light ◽  
Zno Nps ◽  
Long Time

Nanotechnology advancement leads to development of antimicrobial agents like ZnO nanoparticles. These nanoparticle have their main applications in food packaging. when these nanoparticles incorporate into the food surface, it will kill all bacterias residing on the surface and food become free of bacteria. In this way, food can be stored for a long time because its shelf life is improved. Antimicrobial activity of ZnO nanoparticles can be improved by increasing surface area, reducing particle size and large concentration of ZnO –NPS. Antimicrobial activity increases by increasing intensity of UV light. As UV light fall on ZnO nanoparticles, it increases ZnO surface area and hence anrtimicrobial activity will be increased. Exact mechanism of Antimicrobial activity is still unknown but some processes have been presented.

scholarly journals Synthesis of ZnO Nanoparticles by Precipitation Method with Their Antibacterial Effect

2018 ◽  
Vol 16 (2) ◽  
pp. 117 ◽  
Author(s):  
Muhammad Fajri Romadhan ◽  
Nurgaha Edhi Suyatma ◽  
Fahim Muchammad Taqi
Keyword(s):  
Antimicrobial Activity ◽  
Particle Size ◽  
Average Particle Size ◽  
Spherical Shape ◽  
Xrd Analysis ◽  
Zinc Nitrate ◽  
Sem Analysis ◽  
Precipitation Method ◽  
Average Particle ◽  
Zno Nps

The aim of this study was to synthesize and characterize Zinc oxide nanoparticles (ZnO-NPs) prepared by precipitation method. Zinc nitrate and sodium hydroxide was used as starting materials with biopolymer pectin as capping agent. ZnO-NPs were synthesized at three levels of temperatures (60, 80 and 100 °C) without or with calcinations (500 °C). Particle size analyzer (PSA) analysis results showed that the samples without calcination (T60, T80 and T100) having an average particle size respectively 105.13, 78.53, and 76.43 nm, whereas at the samples by calcination (T60C, T80C and T100C) each have average particle size of 88.73, 44.30 and 543.77 nm. The results showed that preparation of ZnO-NPs by using heating at 80 °C followed with calcinations at 500 °C (T80C) produced the smallest size. T80C samples further were analyzed using XRD, SEM and the antimicrobial activity compared with the ZnO-NPs commercials. XRD analysis confirmed that ZnO-NPs were successfully obtained and have form of pure nanostructure. SEM analysis showed that ZnO-NPs obtained has a spherical shape. Furthermore, this ZnO-NPs (T80C) has a better antimicrobial activity compared than commercial ZnO-NPs in market.

Inactivation of Salmonella typhi Using Fe3+ Doped TiO2/3SnO2 Photocatalytic Powders and Films

2010 ◽  
Vol 12 ◽  
pp. 89-97 ◽  
Author(s):  
Lek Sikong ◽  
Budsabakorn Kongreong ◽  
Duangporn Kantachote ◽  
Weerawan Sutthisripok
Keyword(s):  
Visible Light ◽  
Calcination Temperature ◽  
Food Packaging ◽  
Sol Gel ◽  
Xrd Analysis ◽  
Salmonella Typhi ◽  
Conidial Suspension ◽  
Bacterial Inactivation ◽  
Doped Tio2 ◽  
Antibacterial Performance

The aim of the present study is to synthesize Fe3+-doped TiO2/3SnO2 powder and evaluate its antibacterial performance coated on polyvinylchloride films for fresh food packaging. Fe3+-doped TiO2/3SnO2 nanoparticles were prepared as a photocatalyst through the sol-gel method with concentrations of 0.3-1.2 mol% and a calcination temperature of 400°C. It was found that calcination temperatures strongly affect the phases and phase transformation of TiO2. According to XRD analysis, the anatase crystalline was formed at the calcination temperature of 400°C. In the present work, the photocatalytic performance was determined through methylene blue degradation. The antibacterial activity against Salmonella typhi was investigated with a vitro test, from which the mixture of conidial suspension and Fe3+-doped TiO2/3SnO2 powder was added to Nutrient agar (NA) plates under UV and visible light irradiation, respectively. It was found that Fe3+-doped TiO2/3SnO2 nanoparticles enhance photocatalytic activity and bacterial inactivation efficiency. In addition, Fe3+-doped TiO2/3SnO2 thin films can destroy the cell walls of bacteria within 240 min. Furthermore, the disinfection efficiency of TiO2/3SnO2/0.5 Fe3+ is greater under UV irradiation than it is under visible light.

Green synthesis of zinc oxide nanoparticles using Hibiscus subdariffa leaf extract: effect of temperature on synthesis, anti-bacterial activity and anti-diabetic activity

RSC Advances ◽  
2015 ◽  
Vol 5 (7) ◽  
pp. 4993-5003 ◽  
Author(s):  
Niranjan Bala ◽  
S. Saha ◽  
M. Chakraborty ◽  
M. Maiti ◽  
S. Das ◽  
...  
Keyword(s):  
Particle Size ◽  
Zinc Oxide ◽  
Green Synthesis ◽  
Zno Nanoparticles ◽  
Zinc Oxide Nanoparticles ◽  
Leaf Extract ◽  
Bacterial Activity ◽  
Effect Of Temperature ◽  
Oxide Nanoparticles ◽  
Size Dependent

Particle size dependent anti-bacterial and anti-diabetic activities of green synthesized ZnO nanoparticles.

scholarly journals Strategy Towards Active Food Packaging Material From Cellulose Nanoparticles and its Characterization

2021 ◽  
Vol 11 (4) ◽  
pp. 4255-4262
Keyword(s):  
Particle Size ◽  
Food Packaging ◽  
Particle Size Analysis ◽  
Industrial Wastes ◽  
Size Analysis ◽  
Cellulose Nanoparticles ◽  
Active Food Packaging ◽  
Wide Range ◽  
The Rich ◽  
Soluble Base

The utilization of agro-industrial wastes such as sugarcane bagasse (SCB) as a source of cellulose has influenced a wide range of interest in various applications such as food packaging, drug delivery, paper production, etc. Owing to the rich source of cellulose in SCB, the nanoparticle was prepared efficiently. The pure form of cellulose was isolated from SCB by eliminating the remaining components such as hemicellulose and lignin by treating SCB with a soluble base and a bleaching agent. Cellulose nanoparticles were synthesized from the purified cellulose by acid hydrolysis using H2SO4 followed by dialysis to remove sulfate ions and attain neutrality. The obtained nanoparticles were characterized using FTIR spectroscopy that helped to confirm the exclusion of lignin and hemicellulose. The crystalline nature of the cellulose nanoparticles (CNPs) was confirmed using X-Ray Diffraction (XRD). The morphology of CNPs was studied by scanning electron microscopy (SEM), and the particle size of CNPs was found to be 189 nm by particle size analysis (PSA). Further, this study proved the nanomaterial preparation from agro-wastes can be utilized to develop food packaging film in food industries.

scholarly journals The potential of green seaweed (Caulerpa sp.) extract to synthesis ZnO nanoparticles with zinc nitrate as a precursor and pH variations

2021 ◽  
Vol 924 (1) ◽  
pp. 012088
Author(s):  
R N Sari ◽  
E Sinurat ◽  
D L Ayudiarti ◽  
D A Oktavia
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Zno Nanoparticles ◽  
Zinc Nitrate ◽  
Wave Number ◽  
Capping Agent ◽  
Solution Ph ◽  
Green Seaweed ◽  
Ph Variations

Abstract The potential of green seaweed Caulerpa sp. as a reducing agent, stabilizer, and capping agent and the benefits of zinc oxide (ZnO) nanoparticles in the food and non-food is exciting to be developed. The research was aimed to understand the potential of green seaweed (Caulerpa sp.) to become ZnO nanoparticles capping agent with ten mM zinc nitrate as a precursor and pH variations of 8-12. The analysis included function groups, particle size distribution, and % mass O and Zn composition. The result found that spectra at wave number 574 cm−1 were Zn-O stretching vibration from solution pH synthesis of 11. Size distribution was homogeneous, but it still had not met the size of nano. The average particle size ranged from 992.37-1369.36 nm, and the smallest particle size was obtained at a ZnO synthesized at a pH of 8. The composition from ZnO synthesis at solution pH of 9 was 7.68% O and 92.32% Zn. Caulerpa sp. extract could produce a synthesis of ZnO with ten mM zinc nitrate as a precursor and solution pH variations. Although the biosynthesis had not produced a ZnO with nanoparticles size yet, the particle size distribution had been homogeneous. The biosynthesis at pH 9, %mass Zn and O for ZnO produced had been similar to the ZnO standard.

scholarly journals Preparation and Characterization Of Co3O4 Nano Powder

2015 ◽  
pp. 124-129
Author(s):  
Pepi Helza Yanti ◽  
Akmal Mukhtar ◽  
. Astarina
Keyword(s):  
Particle Size ◽  
Calcination Temperature ◽  
Xrd Analysis ◽  
Precipitation Method ◽  
Molar Ratio ◽  
Temperature Influence ◽  
Mineral Phase ◽  
Nano Powder

Synthesis of Co3O4 has been done using Co(NH3)4.6H2O and KOH as precursors with molar ratio 1:1 M with precipitation method. Several of calcination temperature were done to learn type of mineral phase and crystalinity of Co3O4 synthesized. The XRD analysis revealed that calcination temperature influence crystalinity and mineral phase of Co3O4 prepared and calcination temperature at 700 oC has highest intensity and crystalinity that others. Analysis of particle size was examined using Schererr equation, and the results showed that particle size decrease with calcination temperature. The particle size at  700 oC was = 32.387 nm. Analysis morphology of Co3O4 was examined using SEM technique, and the result revelaed Co3O4 have nearly spherical.DOI :http://dx.doi.org/10.15408/jkv.v0i0.3176.

Microstructural characterization of laser-melted/roller-quenched dicalcium silicate

1988 ◽  
Vol 46 ◽  
pp. 582-583
Author(s):  
C. J. Chan ◽  
K. R. Venkatachari ◽  
W. M. Kriven ◽  
J. F. Young
Keyword(s):  
Particle Size ◽  
Raw Materials ◽  
Shape Change ◽  
Microstructural Characterization ◽  
Particle Size Effect ◽  
Dicalcium Silicate ◽  
Laser Melting ◽  
Uniform Size ◽  
Cell Shape Change ◽  
Wide Range

Dicalcium silicate (Ca2SiO4) is a major component of Portland cement. It has also been investigated as a potential transformation toughener alternative to zirconia. It has five polymorphs: α, α'H, α'L, β and γ. Of interest is the β-to-γ transformation on cooling at about 490°C. This transformation, accompanied by a 12% volume increase and a 4.6° unit cell shape change, is analogous to the tetragonal-to-monoclinic transformation in zirconia. Due to the processing methods used, previous studies into the particle size effect were limited by a wide range of particle size distribution. In an attempt to obtain a more uniform size, a fast quench rate involving a laser-melting/roller-quenching technique was investigated.The laser-melting/roller-quenching experiment used precompacted bars of stoichiometric γ-Ca2SiO4 powder, which were synthesized from AR grade CaCO3 and SiO2xH2O. The raw materials were mixed by conventional ceramic processing techniques, and sintered at 1450°C. The dusted γ-Ca2SiO4 powder was uniaxially pressed into 0.4 cm x 0.4 cm x 4 cm bars under 34 MPa and cold isostatically pressed under 172 MPa. The γ-Ca2SiO4 bars were melted by a 10 KW-CO2 laser.

Pharmaceutical Co-Crystals - Design, Development and Applications

2020 ◽  
Vol 10 (3) ◽  
pp. 169-184
Author(s):  
Rachna Anand ◽  
Arun Kumar ◽  
Arun Nanda
Keyword(s):  
Physicochemical Properties ◽  
Crystal Engineering ◽  
Pharmacological Action ◽  
Physicochemical Characteristics ◽  
Research Area ◽  
Dissolution Profile ◽  
Design Development ◽  
Drug Molecule ◽  
Wide Range ◽  
Major Factors

Background: Solubility and dissolution profile are the major factors which directly affect the biological activity of a drug and these factors are governed by the physicochemical properties of the drug. Crystal engineering is a newer and promising approach to improve physicochemical characteristics of a drug without any change in its pharmacological action through a selection of a wide range of easily available crystal formers. Objective: The goal of this review is to summarize the importance of crystal engineering in improving the physicochemical properties of a drug, methods of design, development, and applications of cocrystals along with future trends in research of pharmaceutical co-crystals. Co-crystallization can also be carried out for the molecules which lack ionizable functional groups, unlike salts which require ionizable groups. Conclusion: Co-crystals is an interesting and promising research area amongst pharmaceutical scientists to fine-tune the physicochemical properties of drug materials. Co-crystallization can be a tool to increase the lifecycle of an older drug molecule. Crystal engineering carries the potential of being an advantageous technique than any other approach used in the pharmaceutical industry. Crystal engineering offers a plethora of biopharmaceutical and physicochemical enhancements to a drug molecule without the need of any pharmacological change in the drug.

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