The Gas Permeability of Plasma Sprayed Ceramic Coatings

Author(s):  
A.C. Fox ◽  
T.W. Clyne

Abstract A simple test procedure, based on steady state flow through a membrane, has been developed for measurement of the gas permeability of specimens over a range of temperature. The reliability of this equipment has been verified by testing solid disks containing single perforations and comparing the measured flow rates with those expected on the basis of laminar flow. Coatings of yttria-stabilised zirconia have been produced by plasma spraying in vacuum and in air. The specific permeability of these coatings has been measured at temperatures ranging up to 600°C, using hydrogen gas. It has been found that permeability is increased for coatings produced with longer stand-off distances and at higher pressures. Porosity levels have been measured using densitometry and microstructural features have been examined using SEM. A model has been developed for prediction of the permeability from such microstructural features, based on percolation theory. Agreement between predicted and measured permeabilities is good, although it is clear that more comprehensive data are needed in order to validate the model systematically.

Author(s):  
Aaron J. Knobloch ◽  
Joell R. Hibshman ◽  
George Wu ◽  
Rich Saia

This study summarizes a fundamental investigation of flow through an array of silicon micromachined rectangular slots. The purpose of the study is to evaluate the effect of entrance pressure, flow area, orifice thickness, slot length, and slot width of the orifice on flow rate. These orifices were fabricated using a simple frontside through wafer DRIE process on a 385 μm thick wafer and wafer bonding to create thicker orifices. The dies were then packaged as part of a TO8 can and flow tested. To complement the results of this experimental work, two simple flow models were developed to predict the effect of geometrical and entrance conditions on the flow rate. These models were based on macroscale assumptions that were not necessarily true in the case of thin orifices. One relationship was based on Pouiselle flow which assumes fully developed flow conditions. Calculation of the entry length required for fully developed flow indicate that in the low Reynolds Number regime (32-550) evaluated, the entry flow development requires 2-8 times the thickness of the thickest orifices used for this study. Therefore, calculations of orifice flow based on a Pouiselle model are an overestimate of the actual measured flow rates. Another model examined typical orifice relationships using head loss at the entrance and exit of the slots did not accurately capture the particular flow rates since it overestimated the expansion or constriction losses. A series of experiments where the pressure was varied between 75 and 1000 Pa were performed. A comparison of the Pouiselle flow solution with experimental results was made which showed that the Pouiselle flow model overpredicts the flow rates and more specifically, the effect of width on the flow rates. The results of these tests were used to develop a transfer function which describes the dependence of flow rate on orifice width, thickness, length, and inlet pressure.


1985 ◽  
Vol 107 (1) ◽  
pp. 92-98 ◽  
Author(s):  
E. S. Tillman ◽  
E. O. Hartel ◽  
H. F. Jen

A method for predicting cooling air flow rates using tests on cylindrical models of typical turbine blade leading edges has been extended to include blades with inserts and blades with reversed-angled holes. When an insert is used, the pressure loss across the insert can be determined from flow tests and added to other losses in the flow path to determine cooling flow rates. Calculated and experimentally determined flow rates are compared with good agreement. The second experiment was performed to determine internal loss coefficients for reverse-angled holes oriented so the flow makes a reverse turn to enter the holes. The reversed flow case produced significantly greater internal loss coefficients than when the same holes were oriented in the direction of flow. These results were used to predict flow from arrays of reverse- angled holes and from a cylinder containing both reverse-angled holes and nonreversed holes. In all cases, good agreement was found between predicted and measured flow rates.


Author(s):  
K.R. Subramanian ◽  
A.H. King ◽  
H. Herman

Plasma spraying is a technique which is used to apply coatings to metallic substrates for a variety of purposes, including hardfacing, corrosion resistance and thermal barrier applications. Almost all of the applications of this somewhat esoteric fabrication technique involve materials in hostile environments and the integrity of the coatings is of paramount importance: the effects of process variables on such properties as adhesive strength, cohesive strength and hardness of the substrate/coating system, however, are poorly understood.Briefly, the plasma spraying process involves forming a hot plasma jet with a maximum flame temperature of approximately 20,000K and a gas velocity of about 40m/s. Into this jet the coating material is injected, in powder form, so it is heated and projected at the substrate surface. Relatively thick metallic or ceramic coatings may be speedily built up using this technique.


Coatings ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 643
Author(s):  
Xiaoyu Wu ◽  
Shufeng Xie ◽  
Kangwei Xu ◽  
Lei Huang ◽  
Daling Wei ◽  
...  

Burning loss of graphene in the high-temperature plasma-spraying process is a critical issue, significantly limiting the remarkable performance improvement in graphene reinforced ceramic coatings. Here, we reported an effective approach to enhance the graphene retention, and thus improve the performance of plasma-sprayed alumina/graphene nanoplatelets (Al2O3/GNPs) coatings by heat treatment of agglomerated Al2O3/GNPs powders. The effect of powder heat treatment on the microstructure, GNPs retention, and electrical conductivity of Al2O3/GNPs coatings were systematically investigated. The results indicated that, with the increase in the powder heat treatment temperature, the plasma-sprayed Al2O3/GNPs coatings exhibited decreased porosity and improved adhesive strength. Thermogravimetric analysis and Raman spectra results indicated that increased GNPs retention from 12.9% to 28.4%, and further to 37.4%, as well as decreased structural defects, were obtained for the AG, AG850, and AG1280 coatings, respectively, which were fabricated by using AG powders without heat treatment, powders heat-treated at 850 °C, and powders heat-treated at 1280 °C. Moreover, the electrical conductivities of AG, AG850, and AG1280 coatings exhibited 3 orders, 4 orders, and 7 orders of magnitude higher than that of Al2O3 coating, respectively. Powder heat treatment is considered to increase the melting degree of agglomerated alumina particles, eventually leaving less thermal energy for GNPs to burn; thus, a high retention amount and structural integrity of GNPs and significantly enhanced electrical conductivity were achieved for the plasma-sprayed Al2O3/GNPs coatings.


Energies ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2796
Author(s):  
Andrzej Osuch ◽  
Ewa Osuch ◽  
Stanisław Podsiadłowski ◽  
Piotr Rybacki

In the introduction to this paper, the characteristics of Góreckie lake and the construction and operation of the wind-driven pulverizing aerator are presented. The purpose of this manuscript is to determine the efficiency of the pulverizing aerator unit in the windy conditions of Góreckie Lake. The efficiency of the pulverization aerator depends on the wind conditions at the lake. It was necessary to conduct thorough research to determine the efficiency of water flow through the pulverization segment (water pump). It was necessary to determine the rotational speed of the paddle wheel, which depended on the average wind speed. Throughout the research period, measurements of hourly average wind speed were carried out. It was possible to determine the efficiency of the machine by developing a dedicated mathematical model. The latest method was used in the research, consisting of determining the theoretical volumetric flow rates of water in the pulverizing aerator unit, based on average hourly wind speeds. Pulverization efficiency under the conditions of Góreckie Lake was determined based on 6600 average wind speeds for spring, summer and autumn, 2018. Based on the model, the theoretical efficiency of the machine was calculated, which, under the conditions of Góreckie Lake, amounted to 75,000 m3 per year.


Computation ◽  
2021 ◽  
Vol 9 (3) ◽  
pp. 27
Author(s):  
Nattakarn Numpanviwat ◽  
Pearanat Chuchard

The semi-analytical solution for transient electroosmotic flow through elliptic cylindrical microchannels is derived from the Navier-Stokes equations using the Laplace transform. The electroosmotic force expressed by the linearized Poisson-Boltzmann equation is considered the external force in the Navier-Stokes equations. The velocity field solution is obtained in the form of the Mathieu and modified Mathieu functions and it is capable of describing the flow behavior in the system when the boundary condition is either constant or varied. The fluid velocity is calculated numerically using the inverse Laplace transform in order to describe the transient behavior. Moreover, the flow rates and the relative errors on the flow rates are presented to investigate the effect of eccentricity of the elliptic cross-section. The investigation shows that, when the area of the channel cross-sections is fixed, the relative errors are less than 1% if the eccentricity is not greater than 0.5. As a result, an elliptic channel with the eccentricity not greater than 0.5 can be assumed to be circular when the solution is written in the form of trigonometric functions in order to avoid the difficulty in computing the Mathieu and modified Mathieu functions.


Author(s):  
Yilin Lv ◽  
YunLong Chi ◽  
XinYe Mao ◽  
MingMing Xue ◽  
Yanchun Dong ◽  
...  

1989 ◽  
Vol 181 (1-2) ◽  
pp. 407-415 ◽  
Author(s):  
F Beltzung ◽  
G Zambelli ◽  
E Lopez ◽  
A.R Nicoll

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