scholarly journals Effect of Deformation Path on the Microstructure and Mechanical Behavior of TWIP980 Steel

2019 ◽  
Vol 3 (1) ◽  
pp. 12 ◽  
Author(s):  
António Pereira ◽  
Fábio Fernandes ◽  
Bruno Filipe
Keyword(s):  
Electron Microscopy ◽  
Yield Stress ◽  
Microstructural Analysis ◽  
Rolling Direction ◽  
High Strength ◽  
Deformation Path ◽  
Technological Advances ◽  
Transmission Electron ◽  
Twip Steels ◽  
Permanent Softening

Recent technological advances have made it possible to manufacture steels with both high strength and high ductility. This is the case for Twinning-Induced Plasticity (TWIP) steels which are characterized by a twinning deformation mechanism, which is responsible for its excellent properties. In this work, TWIP980 steel was tested under tensile loading along the rolling direction until pre-deformations of 10%, 20%, and 30% were reached. In order to assess the effect of the deformation path, the pre-deformed samples were reloaded in directions of 0°, 45° and 90° against the rolling direction. Microstructural analysis was performed by means of optical microscopy, scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The yield stress increased with the imposed deformation for all the tested directions. As the strain path changed from 0° to 90°, the yield stress for reload decreased, and the Bauschinger effect and permanent softening was observed. The yield plateau was observed as being directly influenced by deformation path without influence by strain rate and temperature.

Microstructural Analysis of SiO2-Al2O3 Glasses

1982 ◽  
Vol 40 ◽  
pp. 562-563
Author(s):  
C. M. Jantzen ◽  
D. G. Howitt
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Microstructural Analysis ◽  
Liquid Immiscibility ◽  
Metastable Region ◽  
Transmission Electron ◽  
Liquidus Temperatures

The mullite-SiO2 liquidus has been extensively studied, and it has been shown that the flattening of the liquidus is related to the existence of a metastable region of liquid immiscibility at sub-liquidus temperatures which is detectable by transmission electron microscopy (TEM) (Fig. 1).

scholarly journals Investigation of Interfacial Layer for Friction Stir Scribe Welded Aluminum to Steel Joints

2018 ◽  
Vol 140 (11) ◽  
Author(s):  
Kaifeng Wang ◽  
Piyush Upadhyay ◽  
Yuxiang Wang ◽  
Jingjing Li ◽  
Xin Sun ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Driving Force ◽  
Bond Formation ◽  
Welding Process ◽  
High Strength ◽  
Bimaterial Interface ◽  
Joint Interface ◽  
Friction Stir ◽  
Transmission Electron ◽  
Steel Joints

Friction stir scribe (FSS) welding as a recent derivative of friction stir welding (FSW) has been successfully used to fabricate a linear joint between automotive Al and steel sheets. It has been established that FSS welding generates a hook-like structure at the bimaterial interface. Beyond the hook-like structure, there is a lack of fundamental understanding on the bond formation mechanism during this newly developed FSS welding process. In this paper, the microstructures and phases at the joint interface of FSS welded Al to ultra-high-strength steel were studied using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). It was found that both mechanical interlocking and interfacial bonding occurred simultaneously during the FSS welding process. Based on SEM observations, a higher diffusion driving force in the advancing side was found compared to the retreating side and the scribe swept zone, and thermally activated diffusion was the primary driving force for the interfacial bond formation in the scribe swept region. The TEM energy-dispersive X-ray spectroscopy (EDXS) revealed that a thin intermetallic compound (IMC) layer was formed through the interface, where the thickness of this layer gradually decreased from the advancing side to the retreating side owing to different material plastic deformation and heat generations. In addition, the diffraction pattern (or one-dimensional fast Fourier transform (FFT) pattern) revealed that the IMC layer was composed of Fe2Al5 or Fe4Al13 with a Fe/Al solid solution depending on the weld regions.

Effect of Processing Route on Mechanical Behavior of C-Mn Multiphase High Strength Cold Rolled Steel

2007 ◽  
Vol 539-543 ◽  
pp. 4375-4380
Author(s):  
Dagoberto Brandão Santos ◽  
Élida G. Neves ◽  
Elena V. Pereloma
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Mechanical Behavior ◽  
Quantitative Relationship ◽  
High Strength ◽  
Microstructural Characterization ◽  
Processing Route ◽  
Accelerated Cooling ◽  
Microstructural Parameters ◽  
Transmission Electron

The multiphase steels have complex microstructures containing polygonal ferrite, martensite, bainite, carbide and a small amount of retained austenite. This microstructure provides these steels with a high mechanical strength and good ductility. Different thermal cycles were simulated in the laboratory in order to create the microstructures with improved mechanical properties. The samples were heated to various annealing temperatures (740, 760 or 780°C), held for 300 s, and then quickly cooled to 600 or 500°C, where they were soaked for another 300 s and then submitted to the accelerated cooling process, with the rates in the range of 12-30°C/s. The microstructure was examined at the end of each processing route. The mechanical behavior evaluation was made by microhardness testing. The microstructural characterization involved optical microscopy (OM), X-ray diffraction (XRD), scanning electron microscopy (SEM) with electron backscattering diffraction (EBSD) and transmission electron microscopy (TEM). The use of multiple regression analysis allowed the establishment of quantitative relationship between the microstructural parameters, cooling rates and mechanical properties of the steel.

Effect of Milling Condition on Properties and Microstructure of Copper Reinforced with 1% vol. NbC

2007 ◽  
Vol 539-543 ◽  
pp. 826-831
Author(s):  
Marta López ◽  
José A. Jiménez ◽  
R. Benavente
Keyword(s):  
Fine Particles ◽  
Pure Copper ◽  
Microstructural Analysis ◽  
High Strength ◽  
Milling Process ◽  
X Ray Diffraction ◽  
Mechanical And Electrical Properties ◽  
Composites Materials ◽  
Transmission Electron ◽  
Fine Microstructure

Composites materials consisting of pure copper reinforced with 1 vol.% of NbC were prepared by the powder metallurgy route to determine the influence of the milling process on the mechanical and electrical properties. For comparative purpose different milling times at four different rotational speeds were used. The resulting powders were consolidated by hot uniaxial pressing under 90MPa for 2h at 923K to obtain materials with a fine microstructure without residual porosity. It was found that the microstructure and properties of composite materials could be principally related to the amount of Fe, Cr, C and O incorporated as impurities during the milling process. Therefore, the rotational speeds used for milling has an important influence on the properties of the final product. A lower energy-ball milling is accompanied by a smaller amount of impurities (Fe, C and O) incorporated during milling. Composites materials combine electrical conductivity above 40% IACS with high strength. A detailed microstructural analysis by scanning and transmission electron microscopy and X ray diffraction showed that these properties are related not only to NbC particles, but also to the presence of very fine particles of carbides and oxides.

Scanning Transmission Electron Microscopy Studies of the Microstructure of High Chromium Steel after Long Time Exposure

2013 ◽  
Vol 212 ◽  
pp. 25-28 ◽  
Author(s):  
Kinga B. Rodak ◽  
Adam Hernas
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Scanning Transmission Electron Microscopy ◽  
Microstructural Analysis ◽  
Chromium Steel ◽  
Scanning Transmission Electron ◽  
Transmission Electron ◽  
Δ Ferrite ◽  
Scanning Transmission ◽  
Long Time

The detailed microstructural analysis of HCM12 steel after long time (100 000 hours) exposure at service temperatures around 600°C was investigated by means of scanning transmission electron microscopy. The results show, that the recovery processes of the martensite lath structure and δ ferrite are significantly different. Moreover are differences in particles precipitating at the martensite and δ ferrite. The intensive process intragranular M23C6 and Laves particles precipitating is observed at the martensite/ δ ferrite interfaces.

Microstructural analysis of high-pressure compressed C60

2001 ◽  
Vol 16 (7) ◽  
pp. 1960-1966 ◽  
Author(s):  
K. Miyazawa ◽  
H. Satsuki ◽  
M. Kuwabara ◽  
M. Akaishi
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
High Pressure ◽  
High Resolution ◽  
Microstructural Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Hardness Tests ◽  
Lattice Planes

The structure and hardness of C60 bulk specimens compressed under 5.5 GPa at room temperature to 600 °C are investigated by high-resolution transmission electron microscopy, x-ray diffraction, and micro-Vickers hardness tests. A strong accumulation of the [1 1 0]tr orientation of high-pressure-treated C60 specimens was developed along the compression axis, and stacking faults and nano-sized deformation twins were introduced into the C60 specimens compressed at 450–600 °C. Curved lattice planes indicating a polymerization of C60 were observed by high resolution transmission electron microscopy (HRTEM). The polymerization of the high-pressure-compressed C60 is also supported by the computer simulation of HRTEM images.

Study on the Microstructure and Properties of Low Cost TiFeAl Alloy

2013 ◽  
Vol 477-478 ◽  
pp. 1288-1292
Author(s):  
Bo Long Li ◽  
Tong Liu ◽  
Jie Yuan ◽  
Zuo Ren Nie
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Low Cost ◽  
High Strength ◽  
Al Alloys ◽  
Vacuum Induction Melting ◽  
Induction Melting ◽  
Β Phase ◽  
Transmission Electron ◽  
Solution Strengthening

The high strength and low cost Ti-Fe based alloy was produced by double vacuum induction melting method followed by hot deformation. The microstructure has been investigated by Optical Microscopy, Scanning Electron Microscopy (SEM), and Transmission Electron Microscopy (TEM). The microstructure of as-forged alloy is composed of α and β phase without the precipitation of TiFe intermetallic compound. The Ti-Fe-Al alloys show good comprehensive mechanical properties, demonstrating ultimate tensile strength of 1100MPa and elongation above10%. The results indicate the Fe is a good candidate for solution strengthening and simultaneously increasing ductility in titanium alloys. Effect of the Fe and Al elements on the microstructure and mechanical properties have been discussed.

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