scholarly journals A Facile Method to Fabricate Anisotropic Extracellular Matrix with 3D Printing Topological Microfibers

Materials ◽  
2019 ◽  
Vol 12 (23) ◽  
pp. 3944 ◽  
Author(s):  
Zhen Gu ◽  
Zili Gao ◽  
Wenli Liu ◽  
Yongqiang Wen ◽  
Qi Gu
Keyword(s):  
Mechanical Properties ◽  
Extracellular Matrix ◽  
Mechanical Characteristics ◽  
Fiber Direction ◽  
Gelatin Matrix ◽  
Simple Method ◽  
Elongation At Break ◽  
Anisotropic Mechanical Properties ◽  
The Matrix ◽  
3D Printed

Natural tissues and organs have different requirements regarding the mechanical characteristics of response. It is still a challenge to achieve biomaterials with anisotropic mechanical properties using an extracellular matrix with biological activity. We have improved the ductility and modulus of the gelatin matrix using 3D printed gelatin microfibers with different concentrations and topologies and, at the same, time achieved anisotropic mechanical properties. We successfully printed flat microfibers using partially cross-linked gelatin. We modified the 10% (w/v) gelatin matrix with microfibers consisting of a gelatin concentration of 14% (w/v), increasing the modulus to about three times and the elongation at break by 39% in parallel with the fiber direction. At the same time, it is found that the microfiber topology can effectively change the matrix ductility, and changing the modulus of the gelatin used in the microfiber can effectively change the matrix modulus. These findings provide a simple method for obtaining active biological materials that are closer to a physiological environment.

scholarly journals Investigation of Effective Mechanical Characteristics of Nanomodified Carbon-Epoxide Composite by Numerical and Analytical Methods

2021 ◽  
Vol 12 (5) ◽  
pp. 535-541
Author(s):  
M.O. Kaptakov
Keyword(s):  
Mechanical Properties ◽  
Numerical Modeling ◽  
Fracture Surface ◽  
Mechanical Characteristics ◽  
Modeling Methods ◽  
Fullerene Soot ◽  
The Matrix ◽  
Numerical And Analytical Methods ◽  
Composite Samples

In this work, the mechanical properties of composite samples prepared using a conventional and nanomodified matrix were studied. The thickness of the monolayers in the samples was 0,2 μm. It was found in experiments, that the addition of fullerene soot as a nanomodifierled to an increase in the mechanical properties of the samples along the direction of reinforcement. At the same time, an improvement in the quality of the contact of the matrix with the fibers in the samples with the nanomodifier was observed: on the fracture surface, the nanomodified matrix envelops the fibers, while the usual matrix completely exfoliates. The obtained effects of changing the strength of composites can be associated, among other things, with a change in the level of residual stresses arising in composites during nanomodification. Analytical and numerical modeling methods are used to explain these effects.

Studies on the Mechanical Properties of Foam CB-PVC Composite

2013 ◽  
Vol 681 ◽  
pp. 256-259
Author(s):  
Xiu Qi Liu ◽  
He Qin Xing ◽  
Li Li Zhao ◽  
Dan Wang
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Mechanical Index ◽  
Melt Blending ◽  
Elongation At Break ◽  
Foam Composite ◽  
The Matrix ◽  
System Prototype ◽  
Made In

In our study, a new kind of foam composite was prepared by melt blending with PVC as the matrix and carbon black (CB) as the filler, the standard-spline was made in the dumbbell system prototype. Tensile strength and elongation at break were measured at 25°C。When the CB was added greater than 2.0%, with the increase of CB added, the determination of sample mechanical index began to decline, when the CB content was greater than 9%, tensile strength and elongation at break of the composites remained basically unchanged.

Anisotropic Mechanical Properties of Rapid Prototyping Parts Fabricated by Stereolithography

2021 ◽  
Vol 13 (9) ◽  
pp. 1812-1819
Author(s):  
Na-Na Yang ◽  
Hao-Rui Liu ◽  
Ning Mi ◽  
Qi Zhou ◽  
Li-Qun He ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Elastic Modulus ◽  
Brittle Fracture ◽  
Fracture Surface ◽  
Elongation At Break ◽  
Build Orientation ◽  
Range Distribution ◽  
Anisotropic Mechanical Properties ◽  
Orientation Experiment

Stereolithography (SLA)-manufactured parts behave with anisotropic properties due to the varying interface orientations generated by the layer-based manufacturing process. Part build orientation is a very important factor of anisotropic mechanical properties. In this paper, the build orientation experiment was designed to study the anisotropic behaviour of the mechanical properties of the SLA parts based on the orientation relationship between the force and the layer. The results show that there are obvious brittle characteristics on the fracture surface of the specimens and microcracks perpendicular to the direction of the layer distributed on the side of the fracture. The mechanical properties under brittle fracture have different degrees of sensitivity to the build orientation. Among all the build orientations, whether a specimen is built flat or on an edge shows obvious difference in tensile strength, and the relative range distribution reaches 35%. The changes in elastic modulus and the elongation at break are the most obvious in different angles relative to the XY plane, and the relative range distribution reaches 62% and 56% respectively. In all the build orientations designed, the tensile strength is the largest when it is placed on the edge at 0° with Y-axis in the XY plane, the elastic modulus is the largest when it was placed vertically, and the elongation at break is the largest when it is placed flat at 45° with Y-axis in the XY plane.

Anisotropy Evaluation of Different Raster Directions, Spatial Orientations, and Fill Percentage of 3D Printed PETG Tensile Test Specimens

2019 ◽  
Vol 821 ◽  
pp. 167-173 ◽  
Author(s):  
Muammel M. Hanon ◽  
Róbert Marczis ◽  
László Zsidai
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Tensile Test ◽  
Fused Deposition Modelling ◽  
Elongation At Break ◽  
Know How ◽  
Fused Deposition ◽  
Test Pieces ◽  
3D Printed ◽  
Fill Percentage

In this paper, the mechanical properties of Polyethylene terephthalate-glycol (PETG) tensile test specimens have been investigated. The test pieces were prepared using fused deposition modelling (FDM) 3D printing technology. Three print settings were examined which are: raster direction angles, print orientations, and infill percentage and patterns in order to evaluate the anisotropy of objects when employing FDM print method. The variations in stress-strain curves, tensile strength values and elongation at break among the tested samples were studied and compared. Illustration for the broken specimens after the tensile test was accomplished to know how the test pieces printed with various parameters were fractured. A comparison with some previous results regarding the elongation at break has been carried out.

PLA-Based Biodegradable Copolyester Nanocomposites: Preparation, Characterization and Mechanical Properties

2011 ◽  
Vol 380 ◽  
pp. 290-293
Author(s):  
Bing Tao Wang ◽  
Ping Zhang ◽  
De Gao
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Lactic Acid ◽  
Interfacial Adhesion ◽  
Polyhedral Oligomeric Silsesquioxanes ◽  
Elongation At Break ◽  
Butylene Terephthalate ◽  
The Matrix ◽  
Different Characteristics

In situ melt copolycondensation was proposed to prepare biodegradable copolyester nanocomposites based on degradable components poly(L-lactic acid) (PLA), rigid segments poly(butylene terephthalate) (PBT), and nanoparticles polyhedral oligomeric silsesquioxanes (POSS). The morphologies and dispersions of two POSS nanoparticles (POSS-NH2 and POSS-PEG) in the copolyester PLABT matrix and their effects on the mechanical properties were investigated. The results demonstrated that the morphologies and dispersions of POSS-NH2 and POSS-PEG showed quite different characteristics. POSS-PEG took better dispersion in the PLABT, while POSS-NH2 had poor dispersions and formed crystalline microaggregates. Due to the good dispersion and strong interfacial adhesion of POSS-PEG with the matrix, the tensile strength and Young’s modulus were greatly improved from 6.4 and 9.6 MPa for neat PLABT up to 11.2 and 70.7 MPa for PLABT/POSS-PEG nanocomposite. Moreover, the incorporation of POSS-PEG could impart macromolecular chains good flexibility and improve the mobility of the chains, so the the elongation at break of PLABT/POSS-PEG nanocomposite dramatically increased from 190 to 350 % compared with neat PLABT.

scholarly journals Mechanical Properties of Thermoplastic Starch Biocomposite Films with Hybrid Fillers

2021 ◽  
Vol 2080 (1) ◽  
pp. 012011
Author(s):  
Di Sheng Lai ◽  
Sinar Arzuria Adnan ◽  
Azlin Fazlina Osman ◽  
Ismail Ibrahim ◽  
Hazrul Haq
Keyword(s):  
Mechanical Properties ◽  
Food Packaging ◽  
Corn Starch ◽  
Composite Films ◽  
Thermoplastic Starch ◽  
Elongation At Break ◽  
Biocomposite Films ◽  
Hybrid Fillers ◽  
The Matrix ◽  
Dry Food

Abstract Thermoplastic starch (TPS) was studied extensively to replace conventional plastic in packaging application. In this study, granule corn starch was first plasticized with water and glycerol to form TPS films and two different fillers were incorporated with TPS to form hybrid biocomposite films (TPSB). Two different fillers: Microcrystalline cellulose (MC) and Nano bentonite (NB) fixed at 1: 4 ratios in various loading (1wt%-6wt%) were incorporated in TPS to study effect of hybrid fillers on the mechanical properties of TPSB films. The effect of different loading of MC/NB on TPSB films was investigated through the structural, morphological and mechanical testing. Fourier Transform Infrared Spectroscopy (FTIR) shows TPS matrix and hybrid fillers are highly compatible due to hydroxyl bonding and verified through the shifting of spectra band. Scanning Electron Microscope (SEM) showed even distribution of fillers in the matrix of TPS. The TPSB films exhibited significant improvement 40% in elongation at break compared to pure TPS films. In this study, 5wt% is best loading of the hybrid fillers to incorporated in TPSB films as it achieved the highest value of tensile strength (8.52MPa), Young’s Modulus (42.0 MPa) and elongation at break (116.3%). Generally, previous studies showed flexibility of TPS composite films reduced with incorporating filler, however in this study, the flexibility TPSB show significant improvement compared to previous studies and exhibit promising potential in dry food packaging application.

Evaluation of mechanical properties of fiber reinforced composites filled with hollow spheres: A micromechanics approach

2020 ◽  
pp. 002199832094964
Author(s):  
Mojde Biarjemandi ◽  
Ehsan Etemadi ◽  
Mojtaba Lezgy-Nazargah
Keyword(s):  
Mechanical Properties ◽  
Elastic Constants ◽  
Volume Fraction ◽  
Hollow Spheres ◽  
Matrix Phase ◽  
Fiber Reinforced Composites ◽  
Fiber Direction ◽  
Reinforced Composites ◽  
Fiber Reinforced ◽  
The Matrix

Recent researches show that the embedment of hollow spheres in the matrix phase of composite materials improves the strength of these structures against crack propagations. Rare studies are reported for calculating equivalent elastic constants of fiber reinforced composites containing hollow spheres. In this paper, the effects of hollow spheres on mechanical characteristics of fiber reinforced composite are studied for the first time. To achieve this aim, a micromechanics based finite element method is employed. Representative volume elements (RVEs) including hollow spheres with different radius, thickness and volume fraction of hollow spheres, are modeled by using 3D finite elements. The equivalent elastic constants are calculated through homogenization technique. The results are compared with available experimental works. Good agreements find between two sets of results. Also, the volume fraction, number and thickness of hollow spheres as effective parameters on mechanical properties of composite were investigated. The results show the equivalent elastic properties increase with increasing the volume fraction and number of hollow spheres and decrease with increasing the number of hollow spheres. Furthermore, the equivalent Young’s modulus in transverse directions to the fiber direction and shear modulus of the composite increase with increasing the thickness of hollow spheres. As a final result, the presence of hollow spheres in the matrix phase generally increases the equivalent elastic constants without significant changes in the weight of structures.

scholarly journals Polyimide-Based Nanocomposites with Binary CeO2/Nanocarbon Fillers: Conjointly Enhanced Thermal and Mechanical Properties

Polymers ◽  
2020 ◽  
Vol 12 (9) ◽  
pp. 1952
Author(s):  
Alexandra L. Nikolaeva ◽  
Iosif V. Gofman ◽  
Alexander V. Yakimansky ◽  
Elena M. Ivan’kova ◽  
Ivan V. Abalov ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Thermal Stability ◽  
Carbon Nanoparticles ◽  
Mechanical Characteristics ◽  
Functional Performance ◽  
Polymer Materials ◽  
Thermal And Mechanical Properties ◽  
Binary Blends ◽  
Working Temperature ◽  
The Matrix

To design novel polymer materials with optimal properties relevant to industrial usage, it would seem logical to modify polymers with reportedly good functionality, such as polyimides (PIs). We have created a set of PI-based nanocomposites containing binary blends of CeO2 with carbon nanoparticles (nanocones/discs or nanofibres), to improve a number of functional characteristics of the PIs. The prime novelty of this study is in a search for a synergistic effect amidst the nanofiller moieties regarding the thermal and the mechanical properties of PIs. In this paper, we report on the structure, thermal, and mechanical characteristics of the PI-based nanocomposites with binary fillers. We have found that, with a certain composition, the functional performance of a material can be substantially improved. For example, a PI containing SO2-groups in its macrochains not only had its thermal stability enhanced (by ~20 °C, 10% weight loss up to 533 °C) but also had its stiffness increased by more than 10% (Young’s modulus as high as 2.9–3.0 GPa) in comparison with the matrix PI. In the case of a PI with no sulfonic groups, binary fillers increased stiffness of the polymer above its glass transition temperature, thereby widening its working temperature range. The mechanisms of these phenomena are discussed. Thus, this study could contribute to the design of new composite materials with controllable and improved functionality.

Investigation of future 3D printed brace design parameters: evaluation of mechanical properties and prototype outcomes

2019 ◽  
Vol 3 (4) ◽  
pp. 171-184
Author(s):  
Kenwick JL Ng ◽  
Kajsa Duke ◽  
Edmond Lou
Keyword(s):  
Mechanical Properties ◽  
Mechanical Characteristics ◽  
Treatment Effectiveness ◽  
Design Parameters ◽  
Wear Comfort ◽  
Polypropylene Material ◽  
Spinal Brace ◽  
3D Printed ◽  
Opening And Closing

Aim: Spinal brace wear time affects treatment effectiveness of adolescent idiopathic scoliosis but remains challenging with the brace’s bulkiness. This study aims to determine the appropriate material and thickness to improve wear comfort. Materials & methods: Thirty-one specimens were tested with 13 ULTEM1010 and 13 Nylon12 potential materials and 5 standard polypropylene material in 2.5, 3.25 and 4 mm thicknesses to evaluate mechanical properties. Donning tests of ULTEM1010 and Nylon12 printed braces were conducted. Results: Nylon12 with 2.5–3.25 mm thickness had higher flexibility and the closest mechanical characteristics as 4-mm thick polypropylene. ULTEM1010 brace fractured after 615-times and Nylon12 brace handled 2920-times of opening and closing. Conclusion: Nylon12, 2.5–3.25 mm are appropriate design parameters. Further clinical study can validate long term brace effectiveness.

scholarly journals Modification of nitrile butadiene rubber at the stage of its allocation

2018 ◽  
Vol 80 (3) ◽  
pp. 323-329
Author(s):  
V. A. Sedykh ◽  
O. V. Karmanova ◽  
E. V. Koroleva
Keyword(s):  
Mechanical Properties ◽  
Wear Resistance ◽  
Mechanical Characteristics ◽  
Physical And Mechanical Properties ◽  
Butadiene Rubber ◽  
Rubber Latex ◽  
Retention Capacity ◽  
Elongation At Break ◽  
Dry Mixing ◽  
Selection Of

Search for additives that increase the wear resistance of rubbers is relevant. It is known that the introduction of hollow corundum microspheres (NCM) into rubber reduces the wear of rubber products. The uniform distribution of small amounts of microspheres in rubber by traditional "dry" mixing in a rubber mixer or on rollers is difficult. Microspheres were introduced into rubber at the stage of its separation from latex. The work consisted in the selection of thickeners capable of holding the NSM in rubber latex SCN-18SNT at the stage of its coagulation, and evaluation of physical and mechanical properties of rubbers in the presence of NCM. The retention capacity of thickeners of polyacrylamide (PAA), carboxymethylcellulose (CMC) and polyvinyl alcohol (PVA) was determined. Thickened latex was coagulated in the presence of microspheres with polymeric coagulant and sulfuric acid. When filling the polymer with microspheres, it is preferable to use a PAA thickener. The yield of microspheres in rubber using thickeners PAA, CMC and PVA was 71.1, 66.5 and 38.7% , respectively. The physico-mechanical characteristics of rubbers based on SKN-18SNT in the presence of microspheres introduced both as a "dry" method in rubber and at the stage of its isolation from latex are determined. The presence of microspheres in an amount of 4.4-4.7% by weight. on rubber, did not affect the hardness and elasticity of rebound rubbers. It has been confirmed that the presence of microspheres, especially those introduced from the latex rubber release stage, provides an increase in abrasion resistance. In turn, the presence of microspheres in rubber with traces of polyacrylamide provided an increase in the resistance of rubbers to tearing, the modulus at 100 and 200% elongation with a decrease in the elongation at break.

Sign in / Sign up

Export Citation Format

Share Document