scholarly journals Electrospinning on 3D Printed Polymers for Mechanically Stabilized Filter Composites

Polymers ◽  
2019 ◽  
Vol 11 (12) ◽  
pp. 2034 ◽  
Author(s):  
Tomasz Kozior ◽  
Al Mamun ◽  
Marah Trabelsi ◽  
Martin Wortmann ◽  
Sabantina Lilia ◽  
...  
Keyword(s):  
3D Printing ◽  
Thermoplastic Polyurethane ◽  
High Surface ◽  
Antimicrobial Properties ◽  
Mechanical Damage ◽  
Volume Ratio ◽  
Electrospun Nanofiber ◽  
Polymer Nanofiber ◽  
3D Printed ◽  
Nanofiber Mats

Electrospinning is a frequently used method to prepare air and water filters. Electrospun nanofiber mats can have very small pores, allowing for filtering of even the smallest particles or molecules. In addition, their high surface-to-volume ratio allows for the integration of materials which may additionally treat the filtered material through photo-degradation, possess antimicrobial properties, etc., thus enhancing their applicability. However, the fine nanofiber mats are prone to mechanical damage. Possible solutions include reinforcement by embedding them in composites or gluing them onto layers that are more mechanically stable. In a previous study, we showed that it is generally possible to stabilize electrospun nanofiber mats by 3D printing rigid polymer layers onto them. Since this procedure is not technically easy and needs some experience to avoid delamination as well as damaging the nanofiber mat by the hot nozzle, here we report on the reversed technique (i.e., first 3D printing a rigid scaffold and subsequently electrospinning the nanofiber mat on top of it). We show that, although the adhesion between both materials is insufficient in the case of a common rigid printing polymer, nanofiber mats show strong adhesion to 3D printed scaffolds from thermoplastic polyurethane (TPU). This paves the way to a second approach of combining 3D printing and electrospinning in order to prepare mechanically stable filters with a nanofibrous surface.

scholarly journals Stabilization of Electrospun Nanofiber Mats Used for Filters by 3D Printing

Polymers ◽  
2019 ◽  
Vol 11 (10) ◽  
pp. 1618 ◽  
Author(s):  
Kozior ◽  
Trabelsi ◽  
Mamun ◽  
Sabantina ◽  
Ehrmann
Keyword(s):  
3D Printing ◽  
Fused Deposition Modeling ◽  
Water Pressure ◽  
Volume Ratio ◽  
Fused Deposition ◽  
Rigid Objects ◽  
Deposition Modeling ◽  
3D Printed ◽  
Printed Materials ◽  
Nanofiber Mats

Electrospinning is a well-known technology used to create nanofiber mats from diverse polymers and other materials. Due to their large surface-to-volume ratio, such nanofiber mats are often applied as air or water filters. Especially the latter, however, have to be mechanically highly stable, which is challenging for common nanofiber mats. One of the approaches to overcome this problem is gluing them on top of more rigid objects, integrating them in composites, or reinforcing them using other technologies to avoid damage due to the water pressure. Here, we suggest another solution. While direct 3D printing with the fused deposition modeling (FDM) technique on macroscopic textile fabrics has been under examination by several research groups for years, here we report on direct FDM printing on nanofiber mats for the first time. We show that by choosing the proper height of the printing nozzle above the nanofiber mat, printing is possible for raw polyacrylonitrile (PAN) nanofiber mats, as well as for stabilized and even more brittle carbonized material. Under these conditions, the adhesion between both parts of the composite is high enough to prevent the nanofiber mat from being peeled off the 3D printed polymer. Abrasion tests emphasize the significantly increased mechanical properties, while contact angle examinations reveal a hydrophilicity between the original values of the electrospun and the 3D printed materials.

scholarly journals Mechanical Characterization and Thermodynamic Analysis of Laser-Polished Landscape Design Products Using 3D Printing

Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2601
Author(s):  
Yue Ba ◽  
Yu Wen ◽  
Shibin Wu
Keyword(s):  
Surface Roughness ◽  
3D Printing ◽  
Fused Deposition Modeling ◽  
High Surface ◽  
Landscape Design ◽  
Laser Polishing ◽  
Fused Deposition ◽  
Design Structure ◽  
3D Printed ◽  
Stability And Accuracy

Recent innovations in 3D printing technologies and processes have influenced how landscape products are designed, built, and developed. In landscape architecture, reduced-size models are 3D-printed to replicate full-size structures. However, high surface roughness usually occurs on the surfaces of such 3D-printed components, which requires additional post-treatment. In this work, we develop a new type of landscape design structure based on the fused deposition modeling (FDM) technique and present a laser polishing method for FDM-fabricated polylactic acid (PLA) mechanical components, whereby the surface roughness of the laser-polished surfaces is reduced from over Ra 15 µm to less than 0.25 µm. The detailed results of thermodynamics and microstructure evolution are further analyzed during laser polishing. The stability and accuracy of the results are evaluated based on the standard deviation. Additionally, the superior tensile and flexural properties are examined in the laser-polished layer, in which the ultimate tensile strength (UTS) is increased by up to 46.6% and the flexural strength is increased by up to 74.5% compared with the as-fabricated components. Finally, a real polished landscape model is simulated and optimized using a series of scales.

scholarly journals Electrospun Nanofibers for Sensing and Biosensing Applications—A Review

2021 ◽  
Vol 22 (12) ◽  
pp. 6357
Author(s):  
Kinga Halicka ◽  
Joanna Cabaj
Keyword(s):  
High Surface ◽  
High Surface Area ◽  
Toxic Metal ◽  
Volume Ratio ◽  
Electrospun Nanofibers ◽  
Clinical Diagnostics ◽  
Loading Capacity ◽  
Electrospun Nanofiber ◽  
Sensing Platforms ◽  
Different Types

Sensors and biosensors have found applications in many areas, e.g., in medicine and clinical diagnostics, or in environmental monitoring. To expand this field, nanotechnology has been employed in the construction of sensing platforms. Because of their properties, such as high surface area to volume ratio, nanofibers (NFs) have been studied and used to develop sensors with higher loading capacity, better sensitivity, and faster response time. They also allow to miniaturize designed platforms. One of the most commonly used techniques of the fabrication of NFs is electrospinning. Electrospun NFs can be used in different types of sensors and biosensors. This review presents recent studies concerning electrospun nanofiber-based electrochemical and optical sensing platforms for the detection of various medically and environmentally relevant compounds, including glucose, drugs, microorganisms, and toxic metal ions.

scholarly journals DESIGN OF A 3D-PRINTED THREE-CLAW ROBOTIC GRIPPER END-EFFECTOR

2021 ◽  
Vol 11 (4) ◽  
pp. 70-79
Author(s):  
Dino Dominic Forte Ligutan ◽  
Argel Alejandro Bandala ◽  
Jason Limon Española ◽  
Richard Josiah Calayag Tan Ai ◽  
Ryan Rhay Ponce Vicerra ◽  
...  
Keyword(s):  
3D Printing ◽  
Polylactic Acid ◽  
Grip Force ◽  
Thermoplastic Polyurethane ◽  
Robotic Arm ◽  
End Effector ◽  
Design Considerations ◽  
3D Printed ◽  
Materials Used ◽  
Metal Work

The development of a novel 3D-printed three-claw robotic gripper shall be described in this paper with the goal of incorporating various design considerations. Such considerations include the grip reliability and stability, grip force maximization, wide object grasping capability. Modularization of its components is another consideration that allows its parts to be easily machined and reusable. The design was realized by 3D printing using a combination of tough polylactic acid (PLA) material and thermoplastic polyurethane (TPU) material. In practice, additional tolerances were also considered for 3D printing of materials to compensate for possible expansion or shrinkage of the materials used to achieve the required functionality. The aim of the study is to explore the design and eventually deploy the three-claw robotic gripper to an actual robotic arm once its metal work fabrication is finished.

scholarly journals Investigating the Potential of Commercial-Grade Carbon Black-Filled TPU for the 3D Printing of Compressive Sensors

Micromachines ◽  
2019 ◽  
Vol 10 (1) ◽  
pp. 46 ◽  
Author(s):  
Claudio Manganiello ◽  
David Naso ◽  
Francesco Cupertino ◽  
Orazio Fiume ◽  
Gianluca Percoco
Keyword(s):  
3D Printing ◽  
Carbon Black ◽  
Thermoplastic Polyurethane ◽  
Hollow Structure ◽  
Soft Or ◽  
Commercial Grade ◽  
Displacement Sensors ◽  
Commercial Carbon ◽  
3D Printed ◽  
Mechanical Devices

The present research aims to exploit commercially available materials and machines to fabricate multilayer, topologically designed transducers, which can be embedded into mechanical devices, such as soft or rigid grippers. Preliminary tests on the possibility of fabricating 3D-printed transducers using a commercial conductive elastomeric filament, carbon black-filled thermoplastic polyurethane, are presented. The commercial carbon-filled thermoplastic polyurethane (TPU), analyzed in the present paper, has proven to be a candidate material for the production of 3D printed displacement sensors. Some limitations in fabricating the transducers from a 2.85 mm filament were found, and comparisons with 1.75 mm filaments should be conducted. Moreover, further research on the low repeatability at low displacements and the higher performance of the hollow structure, in terms of repeatability, must be carried out. To propose an approach that can very easily be reproduced, only commercial filaments are used.

Simulation and Validation of Fully 3D Printed Soft Actuators

2020 ◽  
Author(s):  
Steffi Torres ◽  
Julio San Martin ◽  
Brittany Newell ◽  
Jose Garcia
Keyword(s):  
3D Printing ◽  
Thermoplastic Polyurethane ◽  
Pharmaceutical Products ◽  
Element Analysis ◽  
Strain Behavior ◽  
Fea Model ◽  
First Case ◽  
3D Printed ◽  
Soft Actuators ◽  
Robotic Applications

Abstract Flexible actuators are a growing class of devices implemented in soft robotic applications, medical devices and processes involving food and pharmaceutical products. Such actuators have traditionally been manufactured using casting processes or other conventional methods requiring more than one fabrication step. The arrival of flexible 3D printing materials and 3D printing techniques has facilitated the creation of these flexible actuators via additive manufacturing. The work presented in this article displays the analytical characterization and experimental validation of two materials and two actuator designs. The first case presents a finite element analysis (FEA) simulated model of a bellows actuator using a photocurable flexible resin (TangoPlus FLX930) and studies the effect of printing orientation on the simulation. The simulation used a 5 parameter Mooney-Rivlin model to predict the strain behavior of the actuator under hydrostatic pressure. A second case is presented where a Thermoplastic Polyurethane actuator was 3D printed and simulated using the same FEA model and a second calibration of the Mooney-Rivlin 5 parameter model. In both cases experimental data was used to calibrate and validate the simulation. The resulting simulated strain was consistent when the printing orientation of actuators was parallel (0 degrees) to the strain direction of the actuators. Results were less consistent when a print orientation of 45 degrees was applied.

scholarly journals 3D Printing of a Self-Healing Thermoplastic Polyurethane through FDM: From Polymer Slab to Mechanical Assessment

Polymers ◽  
2021 ◽  
Vol 13 (2) ◽  
pp. 305
Author(s):  
Linda Ritzen ◽  
Vincenzo Montano ◽  
Santiago J. Garcia
Keyword(s):  
3D Printing ◽  
Room Temperature ◽  
Thermoplastic Polyurethane ◽  
The Self ◽  
Added Value ◽  
Fused Deposition Modelling ◽  
Full Potential ◽  
Self Healing ◽  
Fused Deposition ◽  
3D Printed

The use of self-healing (SH) polymers to make 3D-printed polymeric parts offers the potential to increase the quality of 3D-printed parts and to increase their durability and damage tolerance due to their (on-demand) dynamic nature. Nevertheless, 3D-printing of such dynamic polymers is not a straightforward process due to their polymer architecture and rheological complexity and the limited quantities produced at lab-scale. This limits the exploration of the full potential of self-healing polymers. In this paper, we present the complete process for fused deposition modelling of a room temperature self-healing polyurethane. Starting from the synthesis and polymer slab manufacturing, we processed the polymer into a continuous filament and 3D printed parts. For the characterization of the 3D printed parts, we used a compression cut test, which proved useful when limited amount of material is available. The test was able to quasi-quantitatively assess both bulk and 3D printed samples and their self-healing behavior. The mechanical and healing behavior of the 3D printed self-healing polyurethane was highly similar to that of the bulk SH polymer. This indicates that the self-healing property of the polymer was retained even after multiple processing steps and printing. Compared to a commercial 3D-printing thermoplastic polyurethane, the self-healing polymer displayed a smaller mechanical dependency on the printing conditions with the added value of healing cuts at room temperature.

scholarly journals Influence of washing on the adhesion between 3D-printed TPU and woven fabrics

2021 ◽  
Vol 2 (1) ◽  
pp. 34-39
Author(s):  
Jannik Störmer ◽  
Daniel Görmer ◽  
Andrea Ehrmann
Keyword(s):  
3D Printing ◽  
Strong Correlation ◽  
Thermoplastic Polyurethane ◽  
Cotton Fabrics ◽  
Woven Fabrics ◽  
Textile Fabrics ◽  
Fabric Structure ◽  
High Adhesion ◽  
3D Printed ◽  
Textile Fabric

3D printing on textile fabrics can be used to create composites with position-dependent mechanical, water-resistant, magnetic or other properties. An important prerequisite to use such composites technologically or for design purposes is a sufficient adhesion between both materials. While previous studies revealed that soft, elastic printing polymers were advantageous to prepare connections with a high adhesion, not much research has been performed yet on the dependence of the adhesion on textile fabric structure, heat post-treatment, and the influence of washing, which is necessary for most applications of such composites. Here we investigate composites from thermoplastic polyurethane (TPU) 3D-printed on two different woven cotton fabrics. Besides the expected strong correlation of the adhesion with the distance between nozzle and printing bed, we find a higher adhesion on the thinner fabric and an increase in the adhesion after one washing cycle.

scholarly journals Silver Nanoparticles and Mitochondrial Interaction

2013 ◽  
Vol 2013 ◽  
pp. 1-8 ◽  
Author(s):  
Eriberto Bressan ◽  
Letizia Ferroni ◽  
Chiara Gardin ◽  
Chiara Rigo ◽  
Michele Stocchero ◽  
...  
Keyword(s):  
Silver Nanoparticles ◽  
High Surface ◽  
Specific Interaction ◽  
Antimicrobial Properties ◽  
Chemical Properties ◽  
Volume Ratio ◽  
Clear Understanding ◽  
Different Types ◽  
Physical And Chemical ◽  
And Chemical Properties

Nanotechnology has gone through a period of rapid growth, thus leading to the constant increase in the application of engineered nanomaterials in daily life. Several different types of nanoparticles have been engineered to be employed in a wide array of applications due to their high surface to volume ratio that leads to unique physical and chemical properties. So far, silver nanoparticles (AgNps) have been used in many more different medical devices than any other nanomaterial, mainly due to their antimicrobial properties. Despite the promising advantages posed by using AgNps in medical applications, the possible health effects associated with the inevitable human exposure to AgNps have raised concerns as to their use since a clear understanding of their specific interaction with biological systems has not been attained yet. In light of such consideration, aim of the present work is the morphological analysis of the intracellular behavior of AgNps with a diameter of 10 nm, with a special attention to their interaction with mitochondria.

Characterization of PLA/TPU composite filaments manufactured for 3D printing with FDM

2021 ◽  
pp. 089270572110625
Author(s):  
Ajay Jayswal ◽  
Sabit Adanur
Keyword(s):  
3D Printing ◽  
Fused Deposition Modeling ◽  
Thermoplastic Polyurethane ◽  
Tensile Tests ◽  
Optical Microscope ◽  
Mechanical Analysis ◽  
Uniaxial Tensile ◽  
Scanning Calorimetry ◽  
Fused Deposition ◽  
3D Printed

Polylactic acid (PLA) and thermoplastic polyurethane (TPU) were mixed in different proportions and extruded through twin-screw and single-screw extruders to obtain composite filaments to be used for 3D printing with fused deposition modeling (FDM) method. The properties of the filaments were characterized using uniaxial tensile tests, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), rheology, polarized optical microscope (POM), and scanning electron microscope (SEM). 3D printed samples from composite filaments were tested using dynamic mechanical analysis (DMA). It was found that the tensile strength and modulus of the filaments decrease while elongation at break increases with the increasing TPU content in the composite. The analysis also showed a partial miscibility of the polymer constituents in the solution of composite filaments. Finally, a flexible structure, plain weave fabric, was designed and 3D printed using the composite filaments developed which proved that the filaments are well suited for 3D printing.

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