Microstructure and Mechanical Properties of Tough Phase Layers of a NiCoCrAl/YSZ Multiscalar Microlaminate

2015 ◽  
Vol 1089 ◽  
pp. 15-19
Author(s):  
Chun Yu Jiang ◽  
Xiao Xiao Tian ◽  
Guo Dong Shi

One multiscalar microlaminate comprising 66 thin strong layer stacks of NiCoCrAl / ZrO2-8wt.%Y2O3 (YSZ) and 5 thick tough phase layers of NiCoCrAl whose thicknesses ranged from 5μm to 25μm was fabricated by Electron Beam Physical Vapor Deposition (EB-PVD) and followed by hot pressing treatment. Scanning electron microscopy was used to characterize the microstructures and failure mode of the tough phase layers. Tensile tests and nanoindentation tests were performed to evaluate the mechanical properties of the tough phase layers. The influence of thicknesses of tough phase layers on their microstructure and mechanical properties was investigated. It was found that with the increasing thicknesses of the tough phase layers, their hardness decreased, but their plasticity increased. There was a critical thickness for the tough phase layers between 13μm and 20μm. The tough phase layers with thickness less than the critical value displayed the different microstructure and failure mode from those with thickness more than the critical value.

2014 ◽  
Vol 988 ◽  
pp. 156-160
Author(s):  
Hong Wei Liu ◽  
Feng Wang ◽  
Bai Qing Xiong ◽  
Yong An Zhang ◽  
Zhi Hui Li ◽  
...  

The microstructure and mechanical properties of the Al-2.24Cu-1.42Mg-0.9Fe-0.9Ni alloy were studied using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and tensile tests. The results indicate that the microstructures of the as cast alloy involve α-Al matrix, Al/Al2CuMg eutectic structure, Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds. The tensile test results indicate that the alloy at elevated temperature (200°C) displays superior tensile strength due to the presence of the thermally stable Al7Cu2Fe, Al7Cu4Ni and Al9FeNi compounds.


2019 ◽  
Vol 38 (2019) ◽  
pp. 892-896 ◽  
Author(s):  
Süleyman Tekeli ◽  
Ijlal Simsek ◽  
Dogan Simsek ◽  
Dursun Ozyurek

AbstractIn this study, the effect of solid solution temperature on microstructure and mechanical properties of the AA7075 alloy after T6 heat treatment was investigated. Following solid solution at five different temperatures for 2 hours, the AA7075 alloy was quenched and then artificially aged at 120∘C for 24 hours. Hardness measurements, microstructure examinations (SEM+EDS, XRD) and tensile tests were carried out for the alloys. The results showed that the increased solid solution temperature led to formation of precipitates in the microstructures and thus caused higher hardness and tensile strength.


2018 ◽  
Vol 284 ◽  
pp. 615-620 ◽  
Author(s):  
R.M. Baitimerov ◽  
P.A. Lykov ◽  
L.V. Radionova

TiAl6V4 titanium base alloy is widely used in aerospace and medical industries. Specimens for tensile tests from TiAl6V4 with porosity less than 0.5% was fabricated by selective laser melting (SLM). Specimens were treated using two heat treatment procedures, third batch of specimens was tested in as-fabricated statement after machining. Tensile tests were carried out at room temperature. Microstructure and mechanical properties of SLM fabricated TiAl6V4 after different heat treatments were investigated.


2010 ◽  
Vol 638-642 ◽  
pp. 3479-3484 ◽  
Author(s):  
Roberta O. Rocha ◽  
Tulio M.F. Melo ◽  
Dagoberto Brandao Santos

The influence of continuous annealing variables on the microstructure and mechanical properties of a C-Mn Dual Phase (DP) steel was studied. The annealing cycles were simulated using a Gleeble machine. Some specimens were quenched at different stages of the annealing cycle in order to evaluate the microstructural evolution during the annealing process. Tensile tests and microstrutural analysis were carried out. The results showed that high heating rates increased the final recrystallization temperature and as a consequence the microstructure obtained was refined. Austenite grain nucleation and growth were also influenced by the heating rates. Soaking temperature was the most influent variable on the mechanical properties, i. e., the yield strength increased and the tensile strength decreased with an increase in the soaking temperature. Microstructural analysis showed that not only martensite, but also bainite and martensite-retained autenite constituent (MA) were formed. Undissolved carbides were also detected by transmission electron microscopy.


2010 ◽  
Vol 150-151 ◽  
pp. 51-55 ◽  
Author(s):  
Jun Du ◽  
Ping Zhang ◽  
Jun Jun Zhao ◽  
Zhi Hai Cai

Titanium alloys are susceptible to sand erosion, hard zirconium nitride coatings have been deposited onto titanium alloys by Physical vapor deposition (PVD) in order to improve erosion resistance. Al and Cu were added into ZrN coatings to strength and toughing the coating. The microstructure and mechanical properties of ZrAlCuN coating were studied. Erosion tests were conducted to evaluate anti-erosion ability. Erosion rates were measured and characteristic damage features were identified on the surface of eroded specimens. The mechanisms of erosion are discussed in order to explain the promising performance of materials in erosive conditions. It was found that there is an significant increase of erosion resistance because of the increase of hardness and toughness.


Materials ◽  
2022 ◽  
Vol 15 (2) ◽  
pp. 603
Author(s):  
Natalia Rońda ◽  
Krzysztof Grzelak ◽  
Marek Polański ◽  
Julita Dworecka-Wójcik

This work investigates the effect of layer thickness on the microstructure and mechanical properties of M300 maraging steel produced by Laser Engineered Net Shaping (LENS®) technique. The microstructure was characterized using light microscopy (LM) and scanning electron microscopy (SEM). The mechanical properties were characterized by tensile tests and microhardness measurements. The porosity and mechanical properties were found to be highly dependent on the layer thickness. Increasing the layer thickness increased the porosity of the manufactured parts while degrading their mechanical properties. Moreover, etched samples revealed a fine cellular dendritic microstructure; decreasing the layer thickness caused the microstructure to become fine-grained. Tests showed that for samples manufactured with the chosen laser power, a layer thickness of more than 0.75 mm is too high to maintain the structural integrity of the deposited material.


2017 ◽  
Vol 54 (1) ◽  
pp. 41-44 ◽  
Author(s):  
Maria Adina Vulcan ◽  
Celina Damian ◽  
Paul Octavian Stanescu ◽  
Eugeniu Vasile ◽  
Razvan Petre ◽  
...  

This paper deals with the synthesis of polyurea and its use as polymer matrix for nanocomposites reinforced with multi-walled carbon nanotubes (MWCNT). Two types of materials were obtained during this research, the first cathegory uses the polyurea as matrix and the second one uses a mixture between epoxy resin and polyurea. The nanocomposites were characterized by Thermogravimetric Analysis (TGA), Dynamic Mechanical Analysis (DMA), Scanning Electron Microscopy (SEM) and Tensile Tests .The elastomeric features of nanocomposites were highlighted by the results which showed low value of Tg. Also higher thermal stability with ~40oC compared with commercial products (M20) were observed, but lower mechanical properties compared to neat polyurea.


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