Microstructure and Mechanical Property of Mg-Sn-Al Wrought Magnesium Alloys

2017 ◽  
Vol 898 ◽  
pp. 97-103 ◽  
Author(s):  
Zheng Hua Huang ◽  
Nan Zhou ◽  
Jing Xu ◽  
Yang De Li ◽  
Wei Rong Li

The microstructures, phase constitutions and mechanical properties of as-cast samples, extruded rods and plates of Mg-3.52Sn-3.32Al and Mg-6.54Sn-4.78Al alloys were investigated by optical microscopy, scanning electron microscopy, X-ray diffraction and mechanical testing. The results show that as-cast microstructure consists of α-Mg matrix, Mg2Sn and a few dispersed β-Mg17Al12 phases. The two as-cast alloys exhibit good tensile mechanical properties. After hot extrusion, dynamic recrystallization occurs. Average grain size reaches 6 μm ~ 8 μm for rods, and a lot of fine micro-scaled particles exist, resulting in significant enhancement of tensile mechanical properties. The extruded Mg-3.52Sn-3.32Al rod exhibits better comprehensive tensile mechanical property than AZ31B alloy, with tensile strength σb of 295 MPa, yield strength of 200 MPa and elongation of 21.5% at ambient temperature. The extruded Mg-6.54Sn-4.78Al rod exhibits equivalent comprehensive tensile mechanical properties with ZK60 alloy, achieving tensile strength of 355 MPa, yield strength of 275 MPa and elongation of 11% at ambient temperature. The extruded plates at ambient temperature performed a tensile strength of 270 MPa.

2012 ◽  
Vol 472-475 ◽  
pp. 707-711
Author(s):  
Guan Lu ◽  
Ya Qin Yang ◽  
Bao Cheng Li ◽  
Zhi Min Zhang

In this paper, the effects of hot extrusion and T5、T6 heat treatment on the microstructures and mechanical properties of ZK60 magnesium alloys are investigated by optical microscope, electronic scanning microscope and mechanical testers. The result shows that both the tensile strength and the elongation of the ZK60 alloy extruded at 380°Care much higher than that of the as-cast alloys, as there are much granular second phases precipitated during the extrusion. The tensile strength of the extruded and T5 treated alloy increases while the elongation decreases faster than that of the extruded alloy. The strengthening effect of the T6 treatment is inferior to that of the T5 treatment. The tensile fracture of the as-cast alloy is brittle fractured while that of the extruded and T5 treated alloy is ductile fractured with lots of deep and even dimples.


2013 ◽  
Vol 747-748 ◽  
pp. 443-448
Author(s):  
Feng Wang ◽  
Ji Bao Li ◽  
Ping Li Mao ◽  
Zheng Liu

A high strength and toughness extruded Mg-Zn-Y alloy based on quasicrystal-strengthening has been studied. The effect of extrusion and heat treatment on the microstructures and mechanical properties of Mg-Zn-Y alloy were studied by optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectrum (EDS), X-ray diffraction (XRD) and tensile testing. The experimental results indicated that the coarse dendrite crystals were broken through the hot extrusion, and dynamic recrystallization appeared during the hot extrusion, which obviously refined the hot-extruded microstructure to the average grain size about 20μm. A large amount of strengthening phases such as Mg3Zn6Y(I-Phase), Mg12ZnY(X-Phase) and MgZn2, which were massive, grainy and clavate, dispersedly precipitated from the matrix along grain boundary during ageing treatment at 225 after extrusion, and made the sliding of grain boundaries restrained, which resulted in an enhancement for mechanical properties to a great extent. At the same time, the tensile strength and yield strength increased after ageing treatment. After ageing treatment of 225×24h, the highest tensile strength and yield strength of the extruded Mg-Zn-Y alloy were obtained: σb=506.7MPa, σ0.2=373.5MPa, which were increased by 104.8% and 120.4%, respectively, compared with the extruded Mg-Zn-Y alloy, however the elongation decreased to 16.52%.


2016 ◽  
Vol 61 (2) ◽  
pp. 475-480
Author(s):  
K. Bolanowski

Abstract The paper analyzes the influence of different heat treatment processes on the mechanical properties of low-alloy high-strength steel denoted by Polish Standard (PN) as 10MnVNb6. One of the findings is that, after aging, the mechanical properties of rolled steel are high: the yield strength may reach > 600 MPa, and the ultimate tensile strength is > 700 MPa. These properties are largely dependent on the grain size and dispersion of the strengthening phase in the ferrite matrix. Aging applied after hot rolling contributes to a considerable rise in the yield strength and ultimate tensile strength. The process of normalization causes a decrease in the average grain size and coalescence (reduction of dispersion) of the strengthening phase. When 10MnVNb6 steel was aged after normalization, there was not a complete recovery in its strength properties.


2018 ◽  
Vol 37 (1) ◽  
pp. 97-103 ◽  
Author(s):  
Hansong Xue ◽  
Xinyu Li ◽  
Weina Zhang ◽  
Zhihui Xing ◽  
Jinsong Rao ◽  
...  

AbstractThe effects of Bi on the microstructure and mechanical properties of AZ80-2Sn alloy were investigated. The results show that the addition of Bi within the as-cast AZ80-2Sn alloy promotes the formation of Mg3Bi2 phase, which can refine the grains and make the eutectic phases discontinuous. The addition of 0.5 % Bi within the as-extruded AZ80-2Sn alloy, the average grain size decreases to 12 μm and the fine granular Mg17Al12 and Mg3Bi2 phases are dispersed in the α-Mg matrix. With an increase in Bi content, the Mg17Al12 and Mg3Bi2 phases become coarsened and the grain size increases. The as-extruded AZ80-2Sn-0.5 %Bi alloy has the optimal properties, and the ultimate tensile strength, yield strength and elongation are 379.6 MPa, 247.1 MPa and 14.8 %, respectively.


2011 ◽  
Vol 682 ◽  
pp. 49-54
Author(s):  
Bin Chen ◽  
Chen Lu ◽  
Dong Liang Lin ◽  
Xiao Qin Zeng

The Mg96Y3Zn1 alloy processed by equal channel angular pressing has been investigated. It was found that the Mg96Y3Zn1 alloy processed by ECAP obtained ultrafine grains and exhibits excellent mechanical properties. After ECAP, the average grain size of Mg96Y3Zn1 alloy refined to about 400 nm. The highest strengths with yield strength of 381.45MPa and ultimate tensile strength of 438.33MPa were obtained after 2 passes at 623K. It was found that cracks were preferentially initiated and propagated in the interior of X-phase during the tensile test. As a result, the elongation of alloy is decreased with pass number increasing.


2020 ◽  
Vol 39 (1) ◽  
pp. 200-208
Author(s):  
Tao Lin ◽  
Ji-Xue Zhou ◽  
Cai-Nian Jing ◽  
Yun-Teng Liu ◽  
Lin-Lin Zhang ◽  
...  

AbstractFew studies of cryogenic treatment were focused on nonferrous alloys, such as magnesium alloy. In this work, the effect of cryogenic treatment (77 K) before extrusion on microstructure and mechanical properties of ZK60 alloy was investigated. The results showed that many fine G.P. zones were formed during the cryogenic treatment and then grew to short fine {\beta }_{1}^{^{\prime} } precipitates when heating before extrusion. These precipitates pinned dynamic recrystallized grain boundaries in the subsequent extrusion, resulting in fine gains and dispersed spherical precipitates. By the cryogenic treatment before extrusion, the extruded ZK60 alloy showed good tensile strength and elongation balance. Especially, elongation was improved by 29%.


2011 ◽  
Vol 704-705 ◽  
pp. 892-896
Author(s):  
Bao Hong Zhang ◽  
Zhi Min Zhang

In order to study the effect of plastic deformation on microstructure and mechanical properties of as-cast AZ91 magnesium alloy, experiments of hot direct extrusion were performed at different extrusion temperatures and different extrusion ratios. The microstructure and mechanical properties of extruded billets and extrudate were measured. Experimental results show that the grain size of as-cast AZ91 magnesium alloy can be dramatically refined by extrusion. Hot extrusion can obviously improve the mechanical properties of as-cast AZ91 magnesium Alloy, comparing with the pre-extruded billet, the tensile strength, yield strength and elongation of extrudate can be improved by at least 69%, 117% and 150% respectively. As the extrusion temperature increases, the tensile strength and yield strength of extrudate will increase. As the extrusion ratio increases, the tensile strength and yield strength of extrudate will increase at first and then fall. At the time of extrusion temperature of 420°C and extrusion ratio of 45, the highest tensile strength of 381Mpa and yield strength of 303MPa can be achieved for the extrudate.


2010 ◽  
Vol 297-301 ◽  
pp. 1037-1041
Author(s):  
Young Mo Kim ◽  
Soon Sub Park ◽  
Seul Ki Park ◽  
Hyeon Taek Son ◽  
Jae Seol Lee

The microstructure of as-cast Mg-xAl-2Sn alloys consists of an α-Mg matrix, a Mg17Al12 eutectic phase and a Mg2Sn phase. In as-cast alloys, the Mg17Al12 eutectic phase was located at along grain boundaries. The eutectic phase of the extruded alloys was elongated in the extrusion direction and crushed into fine particles because of deformation during hot extrusion, and the grain size was refined with an increased Al content. The maximum values of the yield strength and tensile strength were 240 MPa and 300 MPa at 9 wt.% containing Al element, respectively.


2018 ◽  
Vol 2 (1) ◽  

The as-cast pure magnesium (Mg), with a purity of 99.99%, was hot-extruded at 300 o C to prepare a Mg bar with a diameter of 8 mm. The microstructure and mechanical properties of the sample before and after extrusion weis obviously refined with a large number of subgrains rather than equre investigated. The results show that the asextruded microstructure iaxed grains. (10 1 2) tensile twins can be observed significantly in the microstructure at this temperature. Mechanical properties including yield strength (YS), ultimate tensile strength (UTS) increased greatly but uniform elongation (UE) decreased slightly as a result of work hardening.


Polymers ◽  
2021 ◽  
Vol 13 (3) ◽  
pp. 404
Author(s):  
Nur Sharmila Sharip ◽  
Hidayah Ariffin ◽  
Tengku Arisyah Tengku Yasim-Anuar ◽  
Yoshito Andou ◽  
Yuki Shirosaki ◽  
...  

The major hurdle in melt-processing of ultra-high molecular weight polyethylene (UHMWPE) nanocomposite lies on the high melt viscosity of the UHMWPE, which may contribute to poor dispersion and distribution of the nanofiller. In this study, UHMWPE/cellulose nanofiber (UHMWPE/CNF) bionanocomposites were prepared by two different blending methods: (i) melt blending at 150 °C in a triple screw kneading extruder, and (ii) non-melt blending by ethanol mixing at room temperature. Results showed that melt-processing of UHMWPE without CNF (MB-UHMWPE/0) exhibited an increment in yield strength and Young’s modulus by 15% and 25%, respectively, compared to the Neat-UHMWPE. Tensile strength was however reduced by almost half. Ethanol mixed sample without CNF (EM-UHMWPE/0) on the other hand showed slight decrement in all mechanical properties tested. At 0.5% CNF inclusion, the mechanical properties of melt-blended bionanocomposites (MB-UHMWPE/0.5) were improved as compared to Neat-UHMWPE. It was also found that the yield strength, elongation at break, Young’s modulus, toughness and crystallinity of MB-UHMWPE/0.5 were higher by 28%, 61%, 47%, 45% and 11%, respectively, as compared to the ethanol mixing sample (EM-UHMWPE/0.5). Despite the reduction in tensile strength of MB-UHMWPE/0.5, the value i.e., 28.4 ± 1.0 MPa surpassed the minimum requirement of standard specification for fabricated UHMWPE in surgical implant application. Overall, melt-blending processing is more suitable for the preparation of UHMWPE/CNF bionanocomposites as exhibited by their characteristics presented herein. A better mechanical interlocking between UHMWPE and CNF at high temperature mixing with kneading was evident through FE-SEM observation, explains the higher mechanical properties of MB-UHMWPE/0.5 as compared to EM-UHMWPE/0.5.


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