scholarly journals USE OF TRAINING DISCUSSION AT LABORATORY AND PRACTICAL LESSONS WHILE IMPLEMENTING COMPETENCY BASED APPROACH

Author(s):  
Olga P. Sazhina ◽  
Oxana V. Glazkova ◽  
Alexandr A. Shabarin ◽  
Yulia I. Matyushkina

An approach implemented in a higher school education system requires use of interactive forms in learning process. Using the example of organisation of laboratory and practical lessons "Methods of quality control with respect to raw materials and products of chemistry manufacture" the effectiveness of training discussions as an interactive form of learning while implementing a competency based approach was demonstrated. Analysis of natural magnetite, used as a raw material for production of iron by the pyrometallurgical method, was chosen as a subject of the discussion. Initially, students analyse State Standard (GOST) N 32517.1-2013 on their own. In class they analyse the Standard from the perspective of use of potentiometric titration instead of visual one under the supervision of instructors. They do modernization of technique for determining: correct a list of specimen used, solution strength, mass of magnetite sample, volume of a sample for titration; suggest a list of laboratory dishes and devices, make preliminary calculations and find out the calculation formula. In the course of discussion, the most preferable method of experiment is elaborated on and recorded. Upon completion a public discussion of the results is held. Each group analyses the obtained data, indicates the positive and negative sides of the suggested method for potentiometric determination of iron content in naturally occurring magnetite. Based on results of questionnaire survey having been held among students who took part in the pedagogic experiment, it was discovered that the proposed way of holding laboratory and practical lessons is more effective in comparison to the traditional one, while serving to unlock the students’ research potential. This way requires applying theoretical skills learned earlier to perform a particular research task. They also learn to work in a team, to sum up results of the common activity and hold responsibility for the results received. Moreover, public speaking is also an important point of learning process. The proposed methods of gaining skills for solution of training tasks facilitate development of intellectual, speaking and communicative students’ competences; they make future specialists more prepared for resolving real production issues.For citation:Sazhina O.P., Glazkova O.V., Shabarin A.A., Matyushkina Yu.I. Use of training discussion at laboratory and practical lessons while implementing competency based approach. Izv. Vyssh. Uchebn. Zaved. Khim. Khim. Tekhnol. 2017. V. 60. N 7. P. 97-101.

1994 ◽  
Vol 77 (6) ◽  
pp. 1447-1453 ◽  
Author(s):  
Pauline M Lacrok ◽  
Norman M Curran ◽  
Wing-Wah Sy ◽  
Dennis K J Goreck ◽  
Pierre Thibault ◽  
...  

Abstract A liquid chromatographic method for the determination of amiodarone hydrochloride and 10 related compounds in drug raw material and for assay of drug in tablets was developed. The method specifies a 3 jxm Hypersil nitrile column (150 × 4.6 mm), a mobile phase of 1 + 1 acetonitrile–ammonium acetate buffer (0.1 M adjusted to pH 6.0 with 0.1 M acetic acid), a flow rate of 1 mL/min, and detection at 240 nm. The lower limit of quantitation of the related compounds is 0.02% or less. Drug contents in 2 raw material samples were 100.1 and 99.9% and ranged from 98.2 to 99.4% in 3 tablet formulations. Impurity levels in 2 samples of raw material from different manufacturers were ca 0.4%. The presence of 3 of the known related compounds in these samples was confirmed by liquid chromatographymass spectrometry. The method applied to raw materials was evaluated by a second laboratory and found to be satisfactory.


2019 ◽  
Vol 9 (2) ◽  
pp. 12-20
Author(s):  
Julio Warmansyah ◽  
Dida Hilpiah

 PT. Cahaya Boxindo Prasetya is a company engaged in the manufacture of carton boxes or boxes. The company's activities also include cutting and printing services using machinery and human power. The problem faced in this company is the difficulty of predicting the amount of inventory of raw materials that will be  included in the production. The remaining raw materials for production will be used as the final stock to get the minimum, the goal is to reduce excess stock Overcoming this problem, fuzzy logic is used to predict raw material inventories by focusing on the final stock. In this study using Fuzzy Sugeno, with three input variables, namely: initial inventory, purchase, production, while the output is the final stock. Determination of prediction results using defuzzification using the average concept of MAPE (Mean Absolute Percentage Error). The results obtained, using the Fuzzy Sugeno method can predict the inventory of raw materials with a MAPE value of 38%. 


2017 ◽  
Vol 12 (2) ◽  
Author(s):  
Monika Handayani ◽  
Eka Kusuma Dewi

<p>CV. Baja Utama Landasan Ulin is a business entity that manufactures various products using the basic ingredients of iron. In the management of raw materials for the production of common regulatory process raw materials into sections for further processing. This setting is often done manually without doing careful planning, so that at the end of each production process there are many remaining pieces of the raw materials that should be used in production. In addition to the determination of the production is necessary to reference how the product should be made for each type of existing products. This is often an important factor that pushed for the optimization of production planning in determining the number of products for each type of product and raw material consumption.Linear Programming is one of the methods used in production planning to regulate the use of raw materials is limited. Simplex method is part of the linear programming method that can be used in the production planning system implementation. Simplex method identifies an initial basic solution and then move systematically to other basic solution that has the potential to improve the value of the objective function.The calculation result of production planning using the simplex method can be used as a reference in the decision making production planning. By building an application using the simplex method can assist in the calculation of production peencanaan more efficiently and effectively. Accuracy testing system constructed show significant results with great value reached 94% level of accuracy.<br />Keywords: simplex, production planning, the maximum gain, linear programming</p>


2021 ◽  
Vol 1 (2) ◽  
Author(s):  
Aula Fajar Iman Sakti ◽  
Wiwik Sulistiyowati

CV. Riki Utama Mandiri is a company in distributing an economic fish frozen product. This company distributed any kind of retail and wholesaler, both domestic and export. They distributing many frozen fish products variant such as Patin Fillet and Shark Fin. The all raw materials of those frozen seafood was obtained by three different suppliers. The common problems found in CV. Riki Utama Mandiri mostly about raw patin fish supplier which often committed delivery delays.  The purpose of this research is to fixing the supply chain management in deciding the more accurate selections of raw materials supplier. To overcome the common problems that happen. Analytical network process (ANP) will simplify the criteria weight values and sub criteria of each supplier. Meanwhile, technique for others reference by similarity to ideal solution (TOPSIS) method is used for giving a rank order of the alternative supplier. This research is expected for being a consideration for the company in obtaining a good and more effective kind of raw supplier. We also expecting the company for tighten supplier selection more effective way so that it can fullfilled the existing standard. Also to overcome the common problems such as delivery delays, competing raw materials with uncertain quality, and difficulty in sort out the raw materials due to size issues.


2021 ◽  
pp. 104-113
Author(s):  
O. P. Deryugina ◽  
E. A. Trapeznikov

The article discusses the issue of industrial compounding, which improves the quality of the raw materials supplied to the main pipelines. Compounding from "to compound" (English) - to mix. When mixing different types of oil obtained, "incompatibility" is possible, which is expressed in the precipitation of a solid sediment and violation of the stability of the colloidal system and due to the differing properties of oils. Attention to this problem is due to the tightening of requirements for the quality of raw materials that must comply with modern standards. The article discusses the causes of the problem of "incompatibility" of oil during compounding and effective ways of solving it, substantiates the need for a preliminary study of the properties of mixed oil in order to identify possible incompatibility of various types of oil. The standard tests for determination of incompatibility indices characterizing the ability of raw materials to mix are considered. The article substantiates the need to develop methods for diagnosing the incompatibility of oils as the most important task of modern chemical science, the solution of which will improve the quality of the raw material obtained and solve many technological problems in the compounding process.


Author(s):  
ARIEF SETIAWAN ROSO ◽  
I KETUT SUAMBA ◽  
NI WAYAN PUTU ARTINI

The Added Value of Processed Red Ginger Product at UD. VisionBali Herbal Indonesia, DenpasarThis research aimed to determine the added value of red ginger as an herbal drink in one production process and to determine the level of profits earned by the company in the red ginger processing in one production process. Determination of the study area was done purposively and the analytical methods used was the method of added value calculation, i.e. the product value is deducted by the value of raw materials and other supporting materials.It can be concluded from the result of the research that the added value of the red ginger processing business obtained in one production process is Rp. 84.600,00/kg. The added value is obtained from the deduction of the value of the product/output of Rp. 175.000,00/kg with the cost of raw material (input prices) Rp. 25.000,00/kg and the contribution of the cost of other inputs of Rp. 65.400,00/kg. It was also found that the profits gained by the manufacturer from the processed red ginger into herbal drink in one production process was Rp. 200.954,06. The suggestion that can be given to the company is to put more attention in the details of its production costs so as not to result in a low ratio of added value and further to improve the marketing of the products, so that people are interested in re-use of herbal medicine that is free of chemical components.


2019 ◽  
Vol 9 (10) ◽  
pp. 2001
Author(s):  
Vladimir Kochemirovsky ◽  
Svetlanav Kochemirovskaia ◽  
Michael Malygin ◽  
Alexey Kuzmin ◽  
Maxim Novomlinsky ◽  
...  

The development of an algorithm to automate the process of measuring the magnetic properties of macroscopic objects in motion is an important problem in various industries, especially in ferrous metallurgy and at factories where ferrous scrap is a strategic raw material. The parameter that requires work control is the hidden mass fraction of a non-magnetic substance that is present in the ferromagnetic raw material. The solution to this problem has no prototypes. In our work, a simple measuring device and a mathematical algorithm for calculating the mass fraction of the non-magnetic fraction in a strongly magnetic matrix were developed. The device is an inductance coil, in which the angle of the electromagnet losses is related to the mass of the magnetic material moving the coil. The magnitude of the instantaneous values of the lost angle integral was compared with the result of weighing the object on scales. This allowed us to calculate the proportion of the magnetic and non-magnetic fractions. The use of this prototype is herein illustrated. The experimental results of the determination of the magnetic-fractional composition depending on the mass of scrap metal and its bulk and the magnetic characteristics are presented.


Minerals ◽  
2020 ◽  
Vol 10 (2) ◽  
pp. 174 ◽  
Author(s):  
Peter Blistan ◽  
Stanislav Jacko ◽  
Ľudovít Kovanič ◽  
Julián Kondela ◽  
Katarína Pukanská ◽  
...  

A frequently recurring problem in the extraction of mineral resources (especially heterogeneous mineral resources) is the rapid operative determination of the extracted quantity of raw material in a surface quarry. This paper deals with testing and analyzing the possibility of using unconventional methods such as digital close-range photogrammetry and terrestrial laser scanning in the process of determining the bulk density of raw material under in situ conditions. A model example of a heterogeneous deposit is the perlite deposit Lehôtka pod Brehmi (Slovakia). Classical laboratory methods for determining bulk density were used to verify the results of the in situ method of bulk density determination. Two large-scale samples (probes) with an approximate volume of 7 m3 and 9 m3 were realized in situ. 6 point samples (LITH) were taken for laboratory determination. By terrestrial laser scanning (TLS) measurement from 2 scanning stations, point clouds with approximately 163,000/143,000 points were obtained for each probe. For Structure-from-Motion (SfM) photogrammetry, 49/55 images were acquired for both probes, with final point clouds containing approximately 155,000/141,000 points. Subsequently, the bulk densities of the bulk samples were determined by the calculation from in situ measurements by TLS and SfM photogrammetry. Comparison of results of the field in situ measurements (1841 kg∙m−3) and laboratory measurements (1756 kg∙m−3) showed only a 4.5% difference in results between the two methods for determining the density of heterogeneous raw materials, confirming the accuracy of the used in situ methods. For the determination of the loosening coefficient, the material from both large-scale samples was transferred on a horizontal surface. Their volumes were determined by TLS. The loosening coefficient for the raw material of 1.38 was calculated from the resulting values.


1991 ◽  
Vol 74 (3) ◽  
pp. 453-455
Author(s):  
Normand Beaulieu ◽  
Terry D Cyr ◽  
Susan J Graham ◽  
Edward G Lovering

Abstract A liquid chromatographic method has been developed for determination of selegiline hydrochloride and related substances in drug raw material and tablet formulations. The method resolves 3 known related compounds from the drug with a limit of quantitation of less than 0.05%. Drug raw material and tablet samples contained ca 0.2 and 0.6% impurities, respectively. These included some related compounds, the identities of which were confirmed by gas chromatography with a Fourier transform Infrared detector.


2020 ◽  
Vol 839 ◽  
pp. 184-188
Author(s):  
Victoria A. Gurieva ◽  
Anastasia A. Ilyina

The paper considers the existing problems of the production of ceramic products in the territory of the Russian Federation, presents the priority directions of development of this industry. The study includes the determination of the properties of samples based on the raw material base of the Orenburg region, namely, waste generated during the development of brown coal from the Tyulgansk deposit - white and red clays and nickel slag of OJSC Yuzhuralnickel Combine of the Orenburg region. The study presents data from the study of the technological properties of the raw materials, the development of the composition of the ceramic mixture. The influence of the material composition of the clay / slag mixture on the physic mechanical characteristics of the products of the experimental compositions was determined: compressive strength, fire shrinkage, water absorption and density.


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