scholarly journals Die Attach Process Optimization with Enhanced Epoxy Control on Leadframe Package

Author(s):  
Rennier S. Rodriguez ◽  
Edwin M. Graycochea Jr ◽  
Rammil A. Seguido ◽  
Frederick Ray I. Gomez

The paper presents a practical procedure in selecting the best candidate for die attach epoxy control or anti-epoxy bleed-out (anti-EBO) concentration during the introduction of new leadframe configuration. Three different criteria were implemented to measure the relative impact of the anti-EBO into the different interfaces inside a quad-flat no-leads multi-row (QFN-mr) leadframe unit. Die shear test is performed to measure the shear strength and the compatibility of the anti-EBO to the adhesive material. EBO measurement is performed herewith to study the propagation of epoxy bleed-out on the surface of the leadframe with reference to the different level of anti-EBO concentration. Package reliability is employed study the response of different interfaces directly in-contact with anti-EBO through thermal-cycling scenario. Ultimately, understanding the effect of anti-EBO into different set of tests provided a systematic way of selecting appropriate leadframe parameters for QFN-mr leadframe product.

Author(s):  
Brandon Prior

This paper will focus on emerging and fast growth package solutions to meet mobile products' density and cost requirements. A short review of where package miniaturization and modularization has taken us so far, and where it will lead in the next 5 years. Teardowns of high density systems and packages will be used to illustrate key points. Low temperature Ag sintering technology provides a lead-free die attachment compatible with high temperature (300°C) applications. Previous work with Ag sintering has required some pressure during the sintering process or been limited to small area die. In this paper, a pressureless sintering of micro-scale silver paste procedure is presented for large (8mm x 8mm) area die. Experimental combinations included: Ag metallized Si die, Au metallized Si die, Ag thick film substrate metallization, Au thick film substrate metallization, PdAg thick film metallization and sintering temperature. For Au metallization (die and/or substrate), the initial shear strength results were good with 8mm x 8mm die sintered at lower temperatures (200°C). The shear strength was out range of our shear test machine (100 kg), corresponding to >15.3 MPa. However, after aging for 24 hours at 300°C, the shear strength dropped significantly to 40.38 Kg (6.183 MPa). An SEM was used to characterize cross sections of as-built and aged sample. The decrease in die shear strength with high temperature sintering (250°C and 300°C) or high temperature aging is attributed to surface diffusion of Ag along the Au surface resulting in a dense Ag layer adjacent to the Au surface and a depletion layer within the die attach on the opposite side of the the dense Ag layer. Shear failures occurred through the depleted region. For Ag metallization, no decrease in shear strength was observed with 300°C aging. Shear strength of 8x8cm2 dies was out range of our shear test machine (>100 kg, >15.3 MPa) as-built. The shear strength remained out of range (>15.3MPa) after more than 2000 hours of 300C aging.


2016 ◽  
Vol 2016 (HiTEC) ◽  
pp. 000128-000133 ◽  
Author(s):  
Hongwen Zhang ◽  
Jonathan Minter ◽  
Ning-Cheng Lee

Abstract BiAgX® paste with the remelting temperature around 262°C has been tested and adopted successfully for die attach applications [1–5]. BiAgX® HT pastes with the enhanced remelting temperature above 265°C have been designed for the application of 200°C or even higher. The joint strength has been well maintained for most of the tested pastes after thermal aging @ 200°C for 1000hrs. The thermal cycling test (from −55°C to 200°C) degrades the bond shear strength but some of the tested pastes can still keep the joint strength well above IEC standard (IEC 60749-19) required. The melting temperature and the reliability have been observed to closely associate with the alloying elements Z%wt. The BiAgX® pastes have also been modified for board level assembly application. BiAgX® solder wire is under development too.


2011 ◽  
Vol 2011 (HITEN) ◽  
pp. 000139-000144
Author(s):  
Fengqun Lang ◽  
Hiroshi Yamaguchi ◽  
Hiroshi Sato

To evaluate the package reliability of the SiC power modules in harsh environments, the SiC Schottky Barrier Diodes (SBDs) were die bonded to the Si3N4/Cu/Ni(P) substrate with Au-Ge eutectic solder using a vacuum reflow furnace. The Si3N4/Cu/Ni(P) substrates are active metalized copper (AMC). The bonded samples were isothermally aged at 330°C and tested under thermal cycling conditions in the temperature range of −40–300°C in air. During the isothermal aging, cracks of the Ni(P) layer developed, resulting in oxidation of the Cu power path. Decrease in the die bond strength and increase in the electrical resistivity were observed due to the Cu power path oxidation and the growth of the Ni-Ge intermetalic compound (IMC) in the joint. Under the thermal cycling conditions, the metallization of the substrate suffers from serious surface roughness, which greatly degrades the die-attach reliability. The Al electrode was found to seriously exfoliate from the SiC-SBDs due to the thermal stress. After 521 cycles, almost all the Al electrode exfoliated form the anode. Benefit from the excellent mechanical properties of Si3N4, no detachment of the Cu layer was observed from the Si3N4 substrate after 1079 cycles, while the Cu layer detached from the AlN substrate only after 12 cycles.


2018 ◽  
Vol 2018 (1) ◽  
pp. 000167-000172
Author(s):  
Guangyu Fan ◽  
Christine Labarbera ◽  
Ning-Cheng Lee ◽  
Colin Clark

Abstract Ag sintering has been paid attention as an alternative to soldering in die attach for decades, especially for high temperature power electronics packages because of its high melting temperature, highly thermal and electrical conductivity of the sintered silver joints, and low process temperature less than 275°C. The coefficient of thermal expansion (CTE) of silver (19.1ppm/°C), however, is much higher than the silicon die (2.6ppm/°C) and the commonly used alumina substrate (7.2ppm/°C). CTE mismatch of the different materials in the various components in a power electronics package lead to the delamination at the interface between interconnection layer and chips or substrate, and/or cracking of the interconnection layer is one of the mostly common causes of failure of power electronics device during thermal cycling or high temperature operation. In recent years we have been developing a series of silver sinter pastes containing low CTE non-metal particles to reduce or adjust CTE of the sintered joints so as to extend the lifetime and reliability of power electronics device in high temperature applications. In the present paper, we will report a new set of silver sinter pastes containing micro scale non-metal particles, a sintering process, microstructural morphologies, thermo-mechanical reliability of the sintered joint and effect of the contents of non-metal particles on shear strength of the sintered silver joints bonding an Ag silicon die on Ni/Au DBC substrates. Shear tests on the sintered joints with and/or without the low CTE non-metal additives have been conducted at room temperature, 200, 250, and 300°C. Thermo-mechanical reliability of the sintered joints was evaluated by thermal cycling, thermal shock, high temperature storage tests (HTS), respectively. X-ray inspection and scanning electronic microscopy (SEM) were used to characterize void, crack and microstructure morphologies of the sintered joints with and/or without the additives.


Author(s):  
Edwin Graycochea Jr. ◽  
Rennier Rodriguez ◽  
Frederick Ray Gomez ◽  
Bryan Christian Bacquian

The paper is focused on the reliability performance of quad-flat no-leads (QFN) package evaluated on different die attach machine platforms. Reliability tests were done to check the difference in the quality and reliability performance of the device that undergone die attach process on two different machines. Thermal cycling resulted in significant difference on the two machines, with the device processed in Machine 1 showing reliability failures while on Machine 2 it passed the 1000 thermal cycle. For future works, Machine 2 could be used for devices with critical package reliability requirement.


2017 ◽  
Vol 2017 (HiTEN) ◽  
pp. 000177-000192
Author(s):  
Siyuan Qi ◽  
Chris Powley ◽  
Maria Mirgkizoudi ◽  
Adele Pliscott ◽  
Peter Collier

Abstract The development of novel high temperature die attach methods for semiconductor packaging enables use in harsh environments and unique opportunities for demanding industrial applications such as controls and monitoring for next generation engine and airframe platforms. Traditional die attach materials including lead solders and conductive adhesives cannot meet requirements of operation temperatures up to and exceeding 300°C due to their limited melting and glass transition temperatures [1]. The Manufacturing Technology Centre Ltd (MTC) has evaluated a range of high temperature die attach materials and processes for silicon and silicon carbide (SiC) semiconductors. Assembly processes were explored for bonding components with and without a back metallisation and with capability to support electrical back contact if required. Die attach methods evaluated include:Sinterable silver materials for back metallised semiconductor componentsSilver glass for non-back metallised semiconductor componentsGold-silicon near eutectic preforms for non-back metallised semiconductor components Two types of substrates were selected including high temperature co-fired ceramic (HTCC) packages and gold or silver plated Kovar substrates. Test assemblies were subjected to accelerated life tests consisting of thermal ageing at 400°C and thermal cycling of −40°C to 200°C. These tests enabled the evaluation of the die attach materials after accelerated conditions of use. Reliability performance of the die attach materials was assessed using visual and X-ray inspection, mechanical shear testing and microstructure analysis. For sinterable silver materials, the test assemblies constructed using HTCC packages showed no significant reduction in shear strength after 1,008 hours ageing at 400°C. However shear strengths of the test assemblies constructed using Kovar substrates reduced by 95% of the initial values after ageing at 400°C for 336 hours. All test assemblies showed no significant reduction in adhesion after thermal cycling of −40°C to 200°C for 1,000 cycles. In addition, no apparent differences in shear strengths could be detected for sintered silver interconnections for gold and silver metallised semiconductor components. Gold-silicon bonding as performed using a near eutectic preform had limited performance as aged at 400°C. Silver glass test assemblies constructed using HTCC packages showed a 50% reduction in shear strength compared to the initial values after thermal ageing at 400°C for 1,000 hours. A similar reduction in adhesion was presented after thermal cycling of −40°C to 200°C for 1,000 cycles.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Jianguo Cui ◽  
Keke Zhang ◽  
Di Zhao ◽  
Yibo Pan

AbstractThrough ultrasonic wave assisted Sn2.5Ag0.7Cu0.1RExNi/Cu (x = 0, 0.05, 0.1) soldering test and − 40 to 125 °C thermal shock test, the microstructure and shear properties of Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints under thermal cycling were studied by the SEM, EDS and XRD. The results show that the Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints with high quality and high reliability can be obtained by ultrasonic assistance. When the ultrasonic vibration power is 88 W, the ultrasonic-assisted Sn2.5Ag0.7Cu0.1RE0.05Ni/Cu solder joints exhibits the optimized performance. During the thermal cycling process, the shear strength of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints had a linear relationship with the thickness of interfacial intermetallic compound (IMC). Under the thermal cycling, the interfacial IMC layer of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints consisted of (Cu,Ni)6Sn5 and Cu3Sn. The thickness of interfacial IMC of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints was linearly related to the square root of equivalent time. The growth of interfacial IMC of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints had an incubation period, and the growth of IMC was slow within 300 cycles. And after 300 cycles, the IMC grew rapidly, the granular IMC began to merge, and the thickness and roughness of IMC increased obviously, which led to a sharp decrease in the shear strength of the solder joints. The 0.05 wt% Ni could inhibit the excessive growth of IMC, improve the shear strength of solder joints and improve the reliability of solder joints. The fracture mechanism of ultrasonic-assisted Sn2.5Ag0.7Cu0.1RExNi/Cu solder joints changed from the ductile–brittle mixed fracture in the solder/IMC transition zone to the brittle fracture in the interfacial IMC.


2018 ◽  
Vol 2018 ◽  
pp. 1-7 ◽  
Author(s):  
Yanhui Cheng ◽  
Weijun Yang ◽  
Dongliang He

Structural plane is a key factor in controlling the stability of rock mass engineering. To study the influence of structural plane microscopic parameters on direct shear strength, this paper established the direct shear mechanical model of the structural plane by using the discrete element code PFC2D. From the mesoscopic perspective, the research on the direct shear test for structural plane has been conducted. The bonding strength and friction coefficient of the structural plane are investigated, and the effect of mesoscopic parameters on the shear mechanical behavior of the structural plane has been analyzed. The results show that the internal friction angle φ of the structural plane decreases with the increase of particle contact stiffness ratio. However, the change range of cohesion is small. The internal friction angle decreases first and then increases with the increase of parallel bond stiffness ratio. The influence of particle contact modulus EC on cohesion c is relatively small. The internal friction angle obtained by the direct shear test is larger than that obtained by the triaxial compression test. Parallel bond elastic modulus has a stronger impact on friction angle φ than that on cohesion c. Under the same normal stress conditions, the shear strength of the specimens increases with particle size. The shear strength of the specimen gradually decreases with the increase of the particle size ratio.


2013 ◽  
Vol 353-356 ◽  
pp. 735-739
Author(s):  
Xiao Ming Zhang ◽  
Shu Wen Ding ◽  
Shuang Xi Li

Development of slope disintegration is close to soil mechanic characteristics such as shear strength indices. Soil grain diameter and water content were tested. Soil direct shear test was conducted to analyze the relationship between shear strength indices and the influencing factors. The experimental data indicate that clay content and the range affect soil cohesion value and the scope. Soil cohesion increases with bulk density before 1.6g/cm3. But it decreases when the bulk after that. The results could provide a scientific basis for control of slope disintegration.


Author(s):  
Fei Qin ◽  
Shuai Zhao ◽  
Yanwei Dai ◽  
Lingyun Liu ◽  
Tong An ◽  
...  

Abstract Thermo-mechanical reliability assessment for sintered silver is a crucial issue as sintered silver is a promising candidate of die-attachment materials for power devices. In this paper, the nano-indentation tests are performed for sintered silver in typical die-attach interconnection under different thermal cycles. Based on thermal cycling test, the Young's modulus and hardness of sintered silver layer have been presented. It is found that the Young's modulus and hardness of sintered silver layer changes slightly although the microstructure of sintered silver also presents some variations. The stress and strain curves for different thermal cycling tests for sintered silver based on reverse analysis of nano-indentation are also given. The results show that the elastoplastic constitutive equations change significantly after thermal cycling tests, and the yielding stress decreases remarkably after 70 thermal cycles. The experimental investigation also show that the cracking behaviors of sintered silver depends on its geometry characteristics, which implies that the possible optimization of sintered silver layer could enhance its thermo-mechanical performance.


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