Effects of grain size and temperature on mechanical properties of Fe–20Mn–0.7C TWIP steel

The typical Fe-25Mn-3Si-3Al TWIP steel with different microstructure scale were investigated. It was found When the grains size is up to 35μm in the 25Mn-3Si-3Al TWIP steel samples, the twinning induced plasticity (TWIP) effect can fully developed and results in above 80% elongation. grain size had a strong effect on the mechanical properties. It was concluded that with increasing grain size ultimate tensile strength decreases, while elongation increases obviously.The annealing twin has the twin’s orientation, during deformation the annealing twin has get orientation ready for deformation twins

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Influence of Grain Size on Mechanical Properties in a Fe-9Ni-12Mn-2.5Si-1.0C TWIP Steel

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.197-198.655 ◽

2011 ◽

Vol 197-198 ◽

pp. 655-661

Author(s):

Ze Bin Yang ◽

Ding Yi Zhu ◽

Wei Fa Yi ◽

Shu Mei Lin ◽

Cheng Mei Du

Keyword(s):

Mechanical Properties ◽

Grain Size ◽

Tensile Strength ◽

Strain Hardening ◽

Twip Steel ◽

Optical Microscope ◽

Coarse Grained ◽

Microstructure Observation ◽

Transmission Electron ◽

Average Grain Size

We investigate the influence of grain size on mechanical properties in a Fe-9Ni-12Mn-2.5Si-1.0C TWIP steel by unidirectional tensile. Meanwhile the microstructures of the TWIP steel were observed and analyzed by optical microscope (OM) and transmission electron microscope (TEM). The experimental results show that the TWIP steel’s yield strength and tensile strength decrease with the increasing of grain size, whereas the plasticity increases with it. When the average grain size reaches to 27μm, the tensile strength is 1080MPa, the elongation percentage is 77%, and the strength-plasticity product achieves the 83160MPa•%. Steel’s strain hardening rate can be changed from three-stage to four-stage with the increasing of grain sizes, the areas of strain hardening by twin deformation mechanism are expanded. Through the microstructure observation we found that, coarse-grained TWIP steel conducts to twinning formation, the high density twins can increase the alloy’s ductility by splitting the grain.

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Ultrafine-Grained Structure and Mechanical Properties of a High-Mn Twinning Induced Plasticity Steel

Materials Science Forum ◽

10.4028/www.scientific.net/msf.838-839.392 ◽

2016 ◽

Vol 838-839 ◽

pp. 392-397 ◽

Cited By ~ 2

Author(s):

Pavel Kusakin ◽

Andrey Belyakov ◽

Rustam Kaibyshev ◽

Dmitri Molodov

Keyword(s):

Mechanical Properties ◽

Grain Size ◽

Tensile Strength ◽

Ultimate Tensile Strength ◽

Yield Strength ◽

Cold Rolling ◽

Twip Steel ◽

True Strain ◽

Total Elongation ◽

Recrystallization Annealing

The influence of thermo-mechanical treatment consisting of cold rolling followed by recrystallization annealing on the grain size and mechanical properties of a high-Mn TWIP steel was studied. An Fe-23Mn-0.3C-1.5Al TWIP steel (wt. %) was subjected to extensive cold rolling with a reduction of 80% (true strain of ∼1.6) and then annealed in the temperature interval ranging from 400 to 900 °C during 20 minutes. Recovery processes took place below 500 °C, partial recrystallization was evident at ~550°C and fully recrystallized structure evolved after annealing at 600 °C and higher. The static recovery resulted in a slight decrease in the yield strength from 1400 MPa to 1250 MPa and the ultimate tensile strength from 1540 MPa to 1400 MPa whereas the total elongation of 4% did not changed. The recrystallization development led to a drastic drop of strength and an increase in ductility. The yield strength of 225 MPa, the ultimate tensile strength of 700 MPa and the total elongation of 79% was obtained after annealing at 900 °C. Correspondingly, the grain size increased from 0.2 μm to 6.2 μm with increase in anneal temperature from 550 to 900°C.

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The Study of Type Twin Annealing in High Mn Steel

Applied Mechanics and Materials ◽

10.4028/www.scientific.net/amm.148-149.1085 ◽

2011 ◽

Vol 148-149 ◽

pp. 1085-1088

Author(s):

Gholam Reza Razavi

Keyword(s):

Mechanical Properties ◽

Heat Treatment ◽

Grain Size ◽

Room Temperature ◽

Twip Steel ◽

Manganese Steel ◽

High Manganese ◽

High Manganese Steel ◽

Twip Steels ◽

Mn Steel

TWIP steels are high manganese steel (Mn: 17% - 35%) which are used for shaping car bodies. The structure of this kind of steels remains austenite even in room temperature. Due to low SFE (Stacking Fault Energy) twinning of grains is governing reformation mechanism in this kind of steels which strengthen TWIP steel. Regarding heat treatment influences on mechanical properties of TWIP steels, in this paper we discuss twinning phenomenon resulting from this kind of treatment. For this, following casting and hot rolling processes, we anneal the steel at 1100°C and different time cycles and study its microstructure using light microscope. The results showed that with decreasing grain size the number of twin annealing added And four types of annealing twin in the microstructure, in the end they all become one twin and then turn into grain.

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Microstructural and Mechanical Characterization of Autogenous GTAW Weld in High-Manganese Austenitic Steel Ti-Containing with Thermal Analysis

MRS Advances ◽

10.1557/adv.2019.10 ◽

2018 ◽

Vol 3 (64) ◽

pp. 3963-3969

Author(s):

V. García-García ◽

I. Mejía ◽

F. Reyes-Calderón

Keyword(s):

Mechanical Properties ◽

Grain Size ◽

Weld Joint ◽

Heat Input ◽

Thermal Field ◽

Twip Steel ◽

Experimental Results ◽

Butt Weld ◽

Average Grain Size ◽

Gtaw Process

ABSTRACTThe welding heat input has been pointed out as a main limiting factor for TWinnig Induced Plasticity (TWIP) steel weldability. Scarce research works have been focused on the study of application and effects of the Gas Tungsten Arc Welding (GTAW) process in the TWIP steel, especially in higher thickness plate. In this research work was conducted a detailed analysis of a butt weld joint performed in plates of TWIP steel microalloyed with titanium (TWIP-Ti) of 6.3 mm thickness. The autogenous GTAW process with low heat input was applied. The analysis considered grain size measurements, second phases identification, post-weld mechanical properties (microhardness) and the welding thermal field. A Finite Element Model (FEM), validated through experimental results, allowed correlating metallurgical results with the thermal field. Likewise, the phases prediction carried out by means of JMatPro 9.0 software during solidification process as well as the estimation of particle precipitation were in good agreement with the experimental results. These predictive diagrams were calculated taking into account the TWIP-Ti steel chemical composition, the grain size measured in critical weld regions and experimental cooling rates. The low heat input improved the microstructural conditions in the heat affected zone (HAZ) whose average grain size and precipitate particles, like (C, N)Ti, promoted good mechanical properties as compared to the base material (as-solution condition). Some particles like Al2O3 y MnS produced microporosities in the HAZ. Despite this, the weld joint did not present hot cracking in the FZ-HAZ interface.

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Surface Modification and its Influence on the Microstructure and Creep Resistance of Nickel Based Superalloy René 77 / Modyfikacja Powierzchniowa Oraz Jej Wpływ Na Mikrostrukture I Wytrzymałosc Na Pełzanie Odlewów Z Nadstopu Niklu Ren´E 77

Archives of Metallurgy and Materials ◽

10.2478/v10172-012-0157-6 ◽

2013 ◽

Vol 58 (1) ◽

pp. 95-98 ◽

Cited By ~ 2

Author(s):

M. Zielinska ◽

J. Sieniawski

Keyword(s):

Mechanical Properties ◽

Grain Size ◽

Surface Modification ◽

Turbine Blades ◽

Processing Parameters ◽

Grain Structure ◽

Creep Tests ◽

Cobalt Aluminate ◽

Nickel Based Superalloy ◽

Average Grain Size

Superalloy René 77 is very wide used for turbine blades, turbine disks of aircraft engines which work up to 1050°C. These elements are generally produced by the investment casting method. Turbine blades produced by conventional precision casting methods have coarse and inhomogeneous grain structure. Such a material often does not fulfil basic requirements, which concern mechanical properties for the stuff used in aeronautical engineering. The incorporation of controlled grain size improved mechanical properties. This control of grain size in the casting operation was accomplished by the control of processing parameters such as casting temperature, mould preheating temperature, and the use of grain nucleates in the face of the mould. For nickel and cobalt based superalloys, it was found that cobalt aluminate (CoAl2O4) has the best nucleating effect. The objective of this work was to determine the influence of the inoculant’s content (cobalt aluminate) in the surface layer of the ceramic mould on the microstructure and mechanical properties at high temperature of nickel based superalloy René 77. For this purpose, the ceramic moulds were made with different concentration of cobalt aluminate in the primary slurry was from 0 to 10% mass. in zirconium flour. Stepped and cylindrical samples were casted for microstructure and mechanical examinations. The average grain size of the matrix ( phase), was determined on the stepped samples. The influence of surface modification on the grain size of up to section thickness was considered. The microstructure investigations with the use of light microscopy and scanning electron microscopy (SEM) enable to examine the influence of the surface modification on the morphology of ’ phase and carbides precipitations. Verification of the influence of CoAl2O4 on the mechanical properties of castings were investigated on the basis of results obtained form creep tests.

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MICROCAST-X MAR-M-247

Alloy Digest ◽

10.31399/asm.ad.ni0481 ◽

1995 ◽

Vol 44 (5) ◽

Keyword(s):

Mechanical Properties ◽

Grain Size ◽

Tensile Properties ◽

Negative Impact ◽

Rupture Properties

Abstract The Microcast-X process produces a substantially finer grain size that improves mechanical properties in MAR-M-247 with modest negative impact on rupture properties above 1600 F (871 C). This datasheet provides information on composition, microstructureand tensile properties as well as creep and fatigue. It also includes information on casting. Filing Code: Ni-481. Producer or source: Howmet Corporation.

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Grain Size Evolution and Mechanical Properties of Nb, V–Nb, and Ti–Nb Boron Type S1100QL Steels

Metals ◽

10.3390/met11030492 ◽

2021 ◽

Vol 11 (3) ◽

pp. 492

Author(s):

Jan Foder ◽

Jaka Burja ◽

Grega Klančnik

Keyword(s):

Mechanical Properties ◽

Heat Treatment ◽

Grain Size ◽

Hot Forging ◽

Size Control ◽

High Strength ◽

Fatigue Properties ◽

Titanium Addition ◽

Austenite Grain Size ◽

Size Evolution

Titanium additions are often used for boron factor and primary austenite grain size control in boron high- and ultra-high-strength alloys. Due to the risk of formation of coarse TiN during solidification the addition of titanium is limited in respect to nitrogen. The risk of coarse nitrides working as non-metallic inclusions formed in the last solidification front can degrade fatigue properties and weldability of the final product. In the presented study three microalloying systems with minor additions were tested, two without any titanium addition, to evaluate grain size evolution and mechanical properties with pre-defined as-cast, hot forging, hot rolling, and off-line heat-treatment strategy to meet demands for S1100QL steel. Microstructure evolution from hot-forged to final martensitic microstructure was observed, continuous cooling transformation diagrams of non-deformed austenite were constructed for off-line heat treatment, and the mechanical properties of Nb and V–Nb were compared to Ti–Nb microalloying system with a limited titanium addition. Using the parameters in the laboratory environment all three micro-alloying systems can provide needed mechanical properties, especially the Ti–Nb system can be successfully replaced with V–Nb having the highest response in tensile properties and still obtaining satisfying toughness of 27 J at –40 °C using Charpy V-notch samples.

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Development of Al–Mg–Si alloy performance by addition of grain refiner Al–5Ti–1B alloy

Science Progress ◽

10.1177/00368504211029469 ◽

2021 ◽

Vol 104 (2) ◽

pp. 003685042110294

Author(s):

Khaled Abd El-Aziz ◽

Emad M Ahmed ◽

Abdulaziz H Alghtani ◽

Bassem F Felemban ◽

Hafiz T Ali ◽

...

Keyword(s):

Mechanical Properties ◽

Grain Size ◽

Corrosion Resistance ◽

Testing Machine ◽

Dendritic Structure ◽

Grain Refiner ◽

Corrosion Properties ◽

Average Grain Size ◽

Structural Applications ◽

Alloy Addition

Aluminum alloys are the most essential part of all shaped castings manufactured, mainly in the automotive, food industry, and structural applications. There is little consensus as to the precise relationship between grain size after grain refinement and corrosion resistance; conflicting conclusions have been published showing that reduced grain size can decrease or increase corrosion resistance. The effect of Al–5Ti–1B grain refiner (GR alloy) with different percentages on the mechanical properties and corrosion behavior of Aluminum-magnesium-silicon alloy (Al–Mg–Si) was studied. The average grain size is determined according to the E112ASTM standard. The compressive test specimens were made as per ASTM: E8/E8M-16 standard to get their compressive properties. The bulk hardness using Vickers hardness testing machine at a load of 50 g. Electrochemical corrosion tests were carried out in 3.5 % NaCl solution using Autolab Potentiostat/Galvanostat (PGSTAT 30).The grain size of the Al–Mg–Si alloy was reduced from 82 to 46 µm by the addition of GR alloy. The morphology of α-Al dendrites changes from coarse dendritic structure to fine equiaxed grains due to the addition of GR alloy and segregation of Ti, which controls the growth of primary α-Al. In addition, the mechanical properties of the Al–Mg–Si alloy were improved by GR alloy addition. GR alloy addition to Al–Mg–Si alloy produced fine-grained structure and better hardness and compressive strength. The addition of GR alloy did not reveal any marked improvements in the corrosion properties of Al–Mg–Si alloy.

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Influence of Post Weld Heat Treatment on the Grain Size, and Mechanical Properties of the Alloy-800H Rotary Friction Weld Joints

Materials ◽

10.3390/ma14164366 ◽

2021 ◽

Vol 14 (16) ◽

pp. 4366

Author(s):

Saqib Anwar ◽

Ateekh Ur Rehman ◽

Yusuf Usmani ◽

Ali M. Al-Samhan

Keyword(s):

Mechanical Properties ◽

Heat Treatment ◽

Grain Size ◽

Heat Affected Zone ◽

Tensile Testing ◽

Weld Zone ◽

Alloy 800H ◽

Weld Joints ◽

Heat Treated ◽

Friction Weld

This study evaluated the microstructure, grain size, and mechanical properties of the alloy 800H rotary friction welds in as-welded and post-weld heat-treated conditions. The standards for the alloy 800H not only specify the composition and mechanical properties but also the minimum grain sizes. This is because these alloys are mostly used in creep resisting applications. The dynamic recrystallization of the highly strained and plasticized material during friction welding resulted in the fine grain structure (20 ± 2 µm) in the weld zone. However, a small increase in grain size was observed in the heat-affected zone of the weldment with a slight decrease in hardness compared to the base metal. Post-weld solution heat treatment (PWHT) of the friction weld joints increased the grain size (42 ± 4 µm) in the weld zone. Both as-welded and post-weld solution heat-treated friction weld joints failed in the heat-affected zone during the room temperature tensile testing and showed a lower yield strength and ultimate tensile strength than the base metal. A fracture analysis of the failed tensile samples revealed ductile fracture features. However, in high-temperature tensile testing, post-weld solution heat-treated joints exhibited superior elongation and strength compared to the as-welded joints due to the increase in the grain size of the weld metal. It was demonstrated in this study that the minimum grain size requirement of the alloy 800H friction weld joints could be successfully met by PWHT with improved strength and elongation, especially at high temperatures.

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